P4W24O80 Roussel P, Mather G, Domenges B, Groult D, Labbe P Acta Crystallographica B54 (1998) 365-375 Structural investigation of P4W24O80: A new monophosphate tungsten bronze _cod_database_code 1001821 _database_code_amcsd 0009905 CELL PARAMETERS: 5.3120 6.5557 42.1960 90.000 90.000 90.000 SPACE GROUP: P2_12_12_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1469.428 Density (g/cm3): 6.571 MAX. ABS. INTENSITY / VOLUME**2: 109.2073957 RIR: 5.411 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 4.19 65.84 21.0980 0 0 2 2 8.38 12.22 10.5490 0 0 4 2 12.59 5.20 7.0327 0 0 6 2 15.92 2.29 5.5681 0 1 4 4 16.81 2.48 5.2745 0 0 8 2 18.50 6.43 4.7953 0 1 6 4 20.96 1.16 4.2387 1 0 6 4 21.05 1.29 4.2196 0 0 10 2 21.62 33.50 4.1095 0 1 8 4 21.64 13.55 4.1076 1 1 1 4 21.94 4.78 4.0504 1 1 2 4 22.45 16.91 3.9602 1 1 3 4 23.14 85.94 3.8435 1 1 4 4 23.33 63.55 3.8135 0 1 9 4 23.77 2.00 3.7428 1 0 8 4 24.00 100.00 3.7076 1 1 5 4 25.02 36.57 3.5595 1 1 6 4 25.10 28.46 3.5482 0 1 10 4 26.93 2.45 3.3108 0 1 11 4 26.99 3.07 3.3040 1 0 10 4 27.44 4.84 3.2504 1 1 8 4 30.29 1.51 2.9505 1 1 10 4 30.49 2.22 2.9321 1 0 12 4 30.74 1.55 2.9088 0 1 13 4 32.15 2.75 2.7840 0 2 8 4 32.73 5.27 2.7362 1 2 3 4 33.22 34.58 2.6968 1 2 4 4 33.35 16.12 2.6864 0 2 9 4 33.75 35.19 2.6560 2 0 0 2 33.84 30.48 2.6486 1 2 5 4 34.02 1.06 2.6352 2 0 2 4 34.21 63.13 2.6214 1 0 14 4 34.59 2.80 2.5930 1 2 6 4 34.65 15.54 2.5886 0 2 10 4 34.70 2.05 2.5851 0 1 15 4 36.04 2.11 2.4920 0 2 11 4 38.76 1.50 2.3234 2 1 6 4 38.79 1.41 2.3213 0 1 17 4 40.44 6.62 2.2307 2 1 8 4 40.88 4.08 2.2073 0 1 18 4 41.37 12.96 2.1823 0 3 1 4 41.43 12.19 2.1795 2 1 9 4 41.55 1.22 2.1736 0 3 2 4 42.52 6.60 2.1263 2 1 10 4 43.00 4.39 2.1034 0 1 19 4 43.69 1.61 2.0718 2 1 11 4 45.15 3.08 2.0084 0 1 20 4 45.83 1.26 1.9801 2 2 6 4 45.86 2.81 1.9788 0 2 17 4 46.29 1.14 1.9614 2 1 13 4 47.30 4.17 1.9217 2 2 8 4 47.70 11.84 1.9068 0 2 18 4 48.18 19.63 1.8887 2 2 9 4 48.46 1.14 1.8786 1 1 20 4 49.15 17.03 1.8538 2 2 10 4 49.18 1.83 1.8525 2 1 15 4 49.58 8.23 1.8386 0 2 19 4 50.20 1.97 1.8173 2 2 11 4 51.08 2.02 1.7880 1 3 11 4 52.21 1.44 1.7522 1 3 12 4 52.34 2.47 1.7478 2 1 17 4 52.62 7.30 1.7394 1 1 22 4 53.41 28.05 1.7156 1 3 13 4 53.66 1.27 1.7080 3 1 1 4 54.02 7.61 1.6976 2 1 18 4 54.04 1.71 1.6969 3 1 3 4 54.37 7.68 1.6874 3 1 4 4 54.41 21.10 1.6861 2 3 1 4 54.56 1.35 1.6821 2 3 2 4 54.76 11.35 1.6764 1 1 23 4 54.79 1.59 1.6755 2 3 3 4 54.79 9.94 1.6754 3 1 5 4 55.31 4.00 1.6610 3 1 6 4 55.75 7.67 1.6490 2 1 19 4 56.03 16.63 1.6413 1 3 15 4 56.93 3.83 1.6175 1 1 24 4 57.45 1.16 1.6041 1 3 16 4 57.53 3.05 1.6019 2 1 20 4 58.13 1.09 1.5868 2 2 17 4 58.39 1.25 1.5805 1 2 22 4 58.93 1.00 1.5672 1 3 17 4 59.02 1.54 1.5651 0 4 8 4 59.69 3.53 1.5491 1 4 4 4 59.70 6.62 1.5489 2 2 18 4 59.72 1.00 1.5484 3 2 3 4 59.77 3.74 1.5471 0 4 9 4 60.03 6.46 1.5412 3 2 4 4 60.09 7.48 1.5398 1 4 5 4 60.39 5.26 1.5328 1 2 23 4 60.42 6.05 1.5320 3 2 5 4 60.57 2.95 1.5286 1 4 6 4 60.61 1.76 1.5277 0 4 10 4 60.66 12.48 1.5267 3 0 14 4 61.32 5.86 1.5117 2 2 19 4 61.54 5.80 1.5070 0 0 28 2 62.44 5.48 1.4874 1 2 24 4 67.65 1.18 1.3849 2 0 26 4 69.74 2.89 1.3484 2 4 8 4 70.05 1.74 1.3432 0 4 18 4 70.43 6.27 1.3369 2 4 9 4 70.97 5.50 1.3280 4 0 0 2 71.20 2.98 1.3243 2 4 10 4 71.55 2.86 1.3187 0 4 19 4 72.05 9.52 1.3107 2 0 28 4 73.22 1.47 1.2927 1 1 31 4 74.33 2.39 1.2761 3 1 22 4 74.67 4.73 1.2712 0 3 27 4 74.90 1.96 1.2678 1 5 3 4 74.98 8.52 1.2667 3 3 13 4 75.18 3.72 1.2638 1 5 4 4 75.19 1.61 1.2637 4 1 8 4 75.26 1.14 1.2627 0 5 9 4 75.54 2.28 1.2587 1 5 5 4 75.72 3.14 1.2561 1 1 32 4 75.86 3.50 1.2541 4 1 9 4 76.01 1.56 1.2521 0 5 10 4 76.11 4.02 1.2507 3 1 23 4 76.61 1.88 1.2437 4 1 10 4 77.19 5.68 1.2359 3 3 15 4 77.95 1.43 1.2256 3 1 24 4 78.27 2.07 1.2214 1 1 33 4 78.92 1.37 1.2131 1 4 22 4 79.07 2.24 1.2111 0 3 29 4 80.06 1.48 1.1986 2 4 18 4 80.35 1.21 1.1950 3 4 4 4 80.58 2.53 1.1921 1 2 32 4 80.66 2.43 1.1911 1 4 23 4 80.70 2.70 1.1907 3 4 5 4 80.72 2.48 1.1905 4 2 9 4 80.96 1.92 1.1875 3 2 23 4 81.12 1.18 1.1856 3 4 6 4 81.45 2.63 1.1816 4 2 10 4 81.49 3.39 1.1811 2 4 19 4 82.48 1.32 1.1694 1 4 24 4 82.78 2.22 1.1660 3 2 24 4 83.00 1.09 1.1635 2 4 20 4 83.09 2.30 1.1624 1 2 33 4 84.50 4.17 1.1466 2 3 27 4 85.07 1.09 1.1404 2 5 9 4 85.29 1.26 1.1379 4 1 18 4 85.62 3.68 1.1345 4 3 1 4 85.80 1.82 1.1325 2 5 10 4 86.65 1.01 1.1236 0 1 37 4 86.71 1.40 1.1229 4 1 19 4 88.79 3.19 1.1020 2 3 29 4 89.75 2.31 1.0926 0 6 0 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.