Na.4(NH4)3.4Al3.8Si12.2O32*10H2O Gualtieri A F Acta Crystallographica B56 (2000) 584-593 Study of NH4+ in the zeolite phillipsite by combined synchrotron powder diffraction and IR spectroscopy Sample: 3 Locality: Monte Lungo, M. Berici, Vicenza, Italy _database_code_amcsd 0009924 CELL PARAMETERS: 9.9596 14.2015 8.7051 90.000 124.990 90.000 SPACE GROUP: P2_1/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 1008.713 Density (g/cm3): 2.036 MAX. ABS. INTENSITY / VOLUME**2: 4.564070184 RIR: 0.730 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.83 24.42 8.1723 -1 0 1 2 10.84 13.54 8.1594 1 0 0 2 12.41 77.53 7.1317 0 0 1 2 12.47 54.29 7.1007 0 2 0 2 12.50 12.29 7.0832 -1 1 1 4 12.51 10.50 7.0748 1 1 0 4 13.90 7.64 6.3732 0 1 1 4 16.54 17.36 5.3601 -1 2 1 4 16.55 24.64 5.3564 1 2 0 4 17.63 23.74 5.0319 0 2 1 4 17.81 41.82 4.9798 -2 0 1 2 20.72 3.51 4.2878 1 0 1 2 21.62 9.30 4.1097 -1 1 2 4 21.65 25.66 4.1048 1 1 1 4 21.70 10.86 4.0962 -1 3 1 4 21.70 4.12 4.0946 1 3 0 4 21.75 1.52 4.0862 -2 0 2 2 21.78 2.08 4.0797 2 0 0 2 21.80 9.71 4.0771 -2 2 1 4 22.54 10.92 3.9440 0 3 1 4 24.22 10.66 3.6740 -1 2 2 4 24.25 8.38 3.6705 1 2 1 4 25.08 1.07 3.5504 0 4 0 2 25.76 3.05 3.4585 0 1 2 4 27.39 1.99 3.2564 -1 4 1 4 27.40 14.00 3.2555 1 4 0 4 27.58 17.24 3.2346 -3 0 2 2 27.60 21.74 3.2322 -3 0 1 2 28.00 38.08 3.1866 0 2 2 4 28.06 1.40 3.1802 -1 3 2 4 28.07 95.64 3.1783 0 4 1 4 28.08 4.36 3.1780 1 3 1 4 28.30 12.21 3.1539 -3 1 2 4 28.32 38.61 3.1516 -3 1 1 4 28.89 1.71 3.0904 2 3 0 4 30.37 8.18 2.9436 -3 2 2 4 30.38 17.08 2.9418 -3 2 1 4 31.52 2.61 2.8384 2 1 1 4 32.64 10.15 2.7436 -1 0 3 2 32.67 10.28 2.7412 1 0 2 2 32.73 5.16 2.7361 -1 4 2 4 32.75 5.89 2.7346 1 4 1 4 32.93 4.83 2.7198 3 0 0 2 33.26 3.12 2.6938 -1 1 3 4 33.29 5.70 2.6915 1 1 2 4 33.36 8.10 2.6859 -2 2 3 4 33.40 5.15 2.6829 -1 5 1 4 33.40 7.89 2.6824 1 5 0 4 33.41 5.89 2.6823 2 2 1 4 33.46 1.12 2.6782 2 4 0 4 33.50 13.87 2.6753 -3 1 3 4 33.55 1.18 2.6713 3 1 0 4 33.56 7.07 2.6707 -3 3 2 4 35.06 7.76 2.5592 -1 2 3 4 35.09 2.76 2.5572 1 2 2 4 35.29 2.69 2.5434 -3 2 3 4 35.69 2.75 2.5159 0 4 2 4 36.07 1.14 2.4899 -4 0 2 2 37.62 6.78 2.3911 -3 4 2 4 37.63 2.83 2.3901 -3 4 1 4 38.16 1.81 2.3583 3 3 0 4 38.63 2.69 2.3310 2 5 0 4 38.81 1.72 2.3204 -4 1 3 4 40.14 2.85 2.2467 -2 4 3 4 40.14 1.41 2.2464 0 6 1 4 40.61 1.27 2.2217 0 5 2 4 41.80 2.59 2.1612 -3 4 3 4 41.84 1.46 2.1591 3 4 0 4 42.28 1.12 2.1377 -2 6 1 4 42.29 1.68 2.1372 3 1 1 4 42.35 2.25 2.1343 -3 5 2 4 42.94 1.47 2.1063 -4 3 3 4 44.07 1.82 2.0549 -2 2 4 4 44.12 1.01 2.0524 2 2 2 4 45.92 1.03 1.9762 1 1 3 4 46.10 2.40 1.9688 1 7 0 4 46.17 1.08 1.9660 -3 5 3 4 46.31 1.99 1.9606 4 2 0 4 46.48 1.66 1.9536 -5 1 2 4 46.54 1.10 1.9514 0 7 1 4 47.84 1.90 1.9012 -5 2 3 4 47.87 1.31 1.9004 -5 2 2 4 48.63 1.10 1.8723 -4 5 2 4 50.03 1.59 1.8231 -5 1 4 4 50.03 2.11 1.8230 0 5 3 4 50.96 2.59 1.7922 -1 6 3 4 50.98 1.29 1.7915 1 6 2 4 51.16 1.02 1.7855 3 6 0 4 51.24 3.68 1.7829 0 0 4 2 51.48 7.93 1.7752 0 8 0 2 51.61 3.63 1.7708 -4 4 4 4 51.68 5.36 1.7687 4 4 0 4 52.61 1.87 1.7396 1 4 3 4 53.09 1.33 1.7250 -3 1 5 4 53.19 2.32 1.7220 -3 5 4 4 53.23 2.10 1.7209 -4 0 5 2 53.31 1.99 1.7183 -3 7 1 4 53.33 2.55 1.7180 4 0 1 2 53.41 2.12 1.7155 -4 6 2 4 54.73 2.93 1.6773 0 6 3 4 54.90 1.46 1.6724 -4 2 5 4 55.35 3.43 1.6599 -6 0 3 2 56.32 1.04 1.6336 -1 5 4 4 56.97 1.80 1.6164 -6 2 3 4 57.76 1.20 1.5962 3 6 1 4 57.87 1.42 1.5933 0 4 4 4 58.00 1.06 1.5901 -2 6 4 4 59.39 1.34 1.5562 -3 8 2 4 60.05 1.04 1.5407 0 9 1 4 62.67 1.03 1.4824 -3 5 5 4 62.74 1.05 1.4809 1 9 1 4 63.17 1.29 1.4718 -6 4 4 4 66.91 1.32 1.3984 0 2 5 4 67.57 2.79 1.3863 -6 4 5 4 67.66 1.48 1.3848 -6 4 1 4 68.75 1.56 1.3654 -3 9 3 4 69.12 1.12 1.3590 -6 6 3 4 71.01 1.47 1.3274 -3 4 6 4 71.10 2.01 1.3259 3 4 3 4 71.25 1.45 1.3235 0 4 5 4 71.51 1.17 1.3194 0 10 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.