Antimonpearceite Evain M, Bindi L, Menchetti S Acta Crystallographica B62 (2006) 768-774 Structure and phase transition of the Se-rich variety of antimonpearceite, [(Ag,Cu)6(Sb,As)2(S,Se)7]-[Ag9Cu(S,Se)2Se2] Note: T = 120 K Locality: De Lamar mine, Idaho, USA _database_code_amcsd 0020664 CELL PARAMETERS: 13.1426 7.5879 23.7290 90.000 90.000 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2366.368 Density (g/cm3): 6.700 MAX. ABS. INTENSITY / VOLUME**2: 73.08017047 RIR: 3.551 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.45 29.95 11.8645 0 0 2 2 13.47 3.24 6.5713 1 1 0 4 13.47 2.33 6.5713 2 0 0 2 14.93 14.19 5.9323 0 0 4 2 15.41 2.18 5.7485 1 1 2 4 20.27 1.02 4.3809 3 0 0 2 21.12 3.22 4.2067 -2 1 3 4 21.62 1.65 4.1097 -3 0 2 2 22.09 2.27 4.0236 0 1 5 4 22.48 1.36 3.9548 0 0 6 2 23.45 1.14 3.7939 3 1 0 4 23.49 1.08 3.7871 -1 0 6 2 24.64 1.96 3.6137 -3 1 2 4 24.64 2.00 3.6137 3 1 2 4 24.71 3.32 3.6028 -1 2 1 4 26.05 1.26 3.4208 -3 1 3 4 26.30 3.19 3.3885 1 1 6 4 26.30 2.36 3.3885 -2 0 6 2 27.14 3.85 3.2857 2 2 0 4 27.14 2.18 3.2857 4 0 0 2 27.91 5.18 3.1962 0 2 4 4 27.91 4.43 3.1962 -3 1 4 4 27.91 3.45 3.1962 3 1 4 4 28.18 3.51 3.1665 -2 2 2 4 28.18 14.76 3.1665 2 2 2 4 28.18 10.23 3.1665 -4 0 2 2 28.18 2.29 3.1665 4 0 2 2 29.44 1.71 3.0343 2 2 3 4 29.87 5.22 2.9911 4 1 1 4 30.13 48.52 2.9661 0 0 8 2 30.45 2.75 2.9356 3 0 6 2 30.93 1.19 2.8908 -1 2 5 4 31.12 57.70 2.8742 2 2 4 4 31.12 14.85 2.8742 -2 2 4 4 31.12 6.96 2.8742 4 0 4 2 31.12 20.48 2.8742 -4 0 4 2 31.42 2.91 2.8472 -3 2 1 4 31.42 2.37 2.8472 3 2 1 4 31.76 1.87 2.8174 -4 1 3 4 31.76 3.99 2.8174 4 1 3 4 32.11 6.19 2.7877 -3 2 2 4 32.11 2.41 2.7877 3 2 2 4 32.71 2.31 2.7378 -3 1 6 4 32.71 1.87 2.7378 3 1 6 4 33.14 1.49 2.7035 2 0 8 2 33.16 1.39 2.7014 -2 2 5 4 33.23 2.43 2.6962 -3 2 3 4 33.23 8.96 2.6962 3 2 3 4 33.43 1.84 2.6803 -1 2 6 4 34.74 7.93 2.5820 -3 2 4 4 34.74 4.91 2.5820 3 2 4 4 35.27 2.23 2.5449 4 1 5 4 35.52 4.33 2.5273 2 2 6 4 35.52 6.30 2.5273 -2 2 6 4 35.52 2.39 2.5273 -4 0 6 2 35.52 5.00 2.5273 4 0 6 2 35.70 1.75 2.5151 0 3 1 4 36.19 2.14 2.4823 1 2 7 4 36.32 2.71 2.4737 0 3 2 4 36.37 2.66 2.4702 -1 3 1 4 36.37 1.58 2.4702 5 1 1 4 36.59 1.37 2.4561 3 0 8 2 36.61 3.08 2.4546 3 2 5 4 36.61 10.40 2.4546 -3 2 5 4 36.98 1.72 2.4310 1 3 2 4 36.98 1.79 2.4310 -1 3 2 4 36.98 1.63 2.4310 -4 2 2 4 36.98 5.95 2.4310 4 2 2 4 36.98 2.78 2.4310 -5 1 2 4 37.33 6.74 2.4091 0 3 3 4 37.97 1.99 2.3696 -1 3 3 4 37.97 2.63 2.3696 5 1 3 4 38.53 3.39 2.3368 0 2 8 4 38.53 8.56 2.3367 -3 1 8 4 38.53 10.42 2.3367 3 1 8 4 38.70 4.35 2.3266 0 3 4 4 38.79 2.46 2.3217 -3 2 6 4 38.79 6.00 2.3217 3 2 6 4 39.85 2.26 2.2619 -2 3 3 4 40.02 10.30 2.2529 -4 1 7 4 40.41 1.35 2.2321 0 3 5 4 40.41 1.23 2.2318 -1 1 10 4 40.99 14.27 2.2017 -2 2 8 4 40.99 9.16 2.2017 4 0 8 2 41.01 1.09 2.2006 -1 3 5 4 41.01 1.37 2.2006 5 1 5 4 41.01 1.05 2.2006 -5 1 5 4 41.21 4.87 2.1904 3 3 0 4 41.21 5.63 2.1904 6 0 0 2 41.23 2.42 2.1895 3 2 7 4 41.94 1.43 2.1540 -3 3 2 4 41.94 8.99 2.1540 3 3 2 4 41.94 2.19 2.1540 -6 0 2 2 41.94 1.13 2.1540 6 0 2 2 42.31 2.56 2.1363 -1 2 9 4 42.42 2.82 2.1308 0 3 6 4 43.00 1.15 2.1033 -4 2 6 4 43.00 2.66 2.1033 5 1 6 4 43.42 1.25 2.0843 -5 2 3 4 43.91 1.39 2.0618 3 2 8 4 44.07 1.18 2.0548 -3 3 4 4 44.07 1.38 2.0548 3 3 4 4 44.07 2.50 2.0548 6 0 4 2 44.55 10.27 2.0337 -6 1 3 4 44.70 2.27 2.0272 0 3 7 4 45.06 8.44 2.0118 0 2 10 4 45.06 7.87 2.0118 -3 1 10 4 45.06 7.26 2.0118 3 1 10 4 45.26 1.48 2.0035 -5 1 7 4 45.41 1.66 1.9971 -4 3 1 4 45.86 3.73 1.9787 -2 1 11 4 45.89 1.05 1.9774 0 0 12 2 47.25 3.92 1.9238 6 1 5 4 47.25 4.90 1.9237 2 2 10 4 47.25 2.11 1.9237 -4 0 10 2 47.45 3.11 1.9162 -3 3 6 4 47.45 1.22 1.9162 6 0 6 2 47.76 1.68 1.9043 -4 2 8 4 47.96 7.54 1.8970 0 4 0 2 47.96 20.74 1.8970 6 2 0 4 48.05 1.36 1.8935 1 1 12 4 48.61 2.26 1.8732 6 2 2 4 49.92 1.18 1.8268 1 4 3 4 51.08 1.30 1.7880 -6 1 7 4 52.53 1.25 1.7422 2 4 4 4 53.13 1.04 1.7240 3 2 11 4 53.40 1.07 1.7157 4 2 10 4 53.58 2.85 1.7104 0 4 6 4 53.58 2.20 1.7104 -6 2 6 4 53.58 1.52 1.7104 6 2 6 4 53.93 1.59 1.7001 3 4 3 4 54.13 5.76 1.6942 2 2 12 4 54.13 2.06 1.6942 -4 0 12 2 56.03 1.47 1.6413 0 3 11 4 56.03 1.19 1.6412 2 0 14 2 56.55 1.12 1.6273 8 0 2 2 57.68 1.56 1.5981 -6 2 8 4 57.68 1.66 1.5981 6 2 8 4 58.28 5.08 1.5832 -4 4 4 4 58.28 1.75 1.5832 8 0 4 2 59.32 1.15 1.5578 0 3 12 4 60.08 1.15 1.5399 -3 2 13 4 61.56 2.19 1.5064 -6 1 11 4 61.57 1.02 1.5063 2 2 14 4 61.57 1.26 1.5063 -2 2 14 4 61.57 1.09 1.5063 4 0 14 2 62.64 2.39 1.4831 0 0 16 2 62.70 1.53 1.4817 0 4 10 4 62.70 2.56 1.4817 6 2 10 4 63.79 1.20 1.4592 3 2 14 4 64.46 1.02 1.4455 0 5 5 4 64.88 2.21 1.4371 4 4 8 4 66.78 1.51 1.4008 -4 1 15 4 69.54 1.90 1.3517 -2 2 16 4 69.54 1.16 1.3517 4 0 16 2 69.61 1.11 1.3507 8 0 10 2 70.21 1.39 1.3405 -3 3 14 4 75.12 1.30 1.2646 9 3 0 4 75.19 1.45 1.2636 -4 4 12 4 77.83 1.67 1.2273 6 4 10 4 77.83 1.57 1.2273 -6 4 10 4 78.73 1.43 1.2155 2 6 4 4 78.73 1.10 1.2155 8 4 4 4 81.05 1.44 1.1865 0 0 20 2 89.48 1.21 1.0952 6 6 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.