Sarrabusite Gemmi M, Campostrini I, Demartin F, Gorelik T E, Gamaccioli C M Acta Crystallographica B68 (2012) 15-23 Structure of the new mineral sarrabusite, Pb5CuCl4(SeO3)4, solved by manual electron-diffraction tomography Note: Manual data, this is the prefered structure Locality: Baccu Locci mine, near Villaputzu, Sardinia, Italy _database_code_amcsd 0018632 CELL PARAMETERS: 24.9170 5.5060 14.2420 90.000 101.770 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1912.821 Density (g/cm3): 6.073 MAX. ABS. INTENSITY / VOLUME**2: 80.93844600 RIR: 4.340 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.25 1.23 12.1966 2 0 0 2 12.70 35.98 6.9713 0 0 2 2 13.28 5.36 6.6665 -2 0 2 2 14.53 10.19 6.0983 4 0 0 2 15.88 15.62 5.5817 2 0 2 2 19.78 8.01 4.4876 -3 1 1 4 20.42 1.05 4.3501 -1 1 2 4 21.22 4.34 4.1862 4 0 2 2 21.33 4.76 4.1651 1 1 2 4 22.04 56.94 4.0327 -3 1 2 4 22.97 2.09 3.8725 -6 0 2 2 24.24 3.51 3.6724 -5 1 1 4 24.38 60.35 3.6515 5 1 0 4 24.52 14.06 3.6301 3 1 2 4 24.76 1.81 3.5952 -1 1 3 4 25.10 5.32 3.5481 -2 0 4 2 25.56 4.64 3.4856 0 0 4 2 25.76 2.90 3.4589 -5 1 2 4 25.76 7.02 3.4583 -3 1 3 4 26.15 7.64 3.4071 5 1 1 4 26.74 13.87 3.3333 -4 0 4 2 28.02 16.10 3.1842 2 0 4 2 29.29 11.25 3.0491 8 0 0 2 29.29 88.75 3.0489 5 1 2 4 29.48 36.98 3.0297 -8 0 2 2 29.93 35.01 2.9857 -1 1 4 4 30.18 18.27 2.9615 -6 0 4 2 30.36 4.99 2.9445 7 1 0 4 30.45 58.46 2.9358 -3 1 4 4 32.07 3.63 2.7908 4 0 4 2 32.13 1.23 2.7856 7 1 1 4 32.52 41.96 2.7530 0 2 0 2 32.70 6.26 2.7388 -5 1 4 4 33.17 7.83 2.7009 0 2 1 4 33.44 1.01 2.6794 5 1 3 4 34.29 2.40 2.6152 2 2 1 4 34.42 9.21 2.6053 8 0 2 2 34.92 2.01 2.5693 -8 0 4 2 35.60 2.72 2.5216 -1 1 5 4 35.77 1.14 2.5100 -3 1 5 4 35.79 1.25 2.5092 4 2 0 4 36.39 2.76 2.4690 2 2 2 4 36.39 4.05 2.4689 -7 1 4 4 36.46 1.76 2.4645 -10 0 2 2 36.85 2.87 2.4393 10 0 0 2 36.85 11.43 2.4390 -9 1 2 4 36.97 3.37 2.4317 9 1 0 4 37.25 2.72 2.4140 6 0 4 2 37.91 1.08 2.3734 -2 0 6 2 38.54 2.31 2.3358 -4 0 6 2 38.93 1.83 2.3136 7 1 3 4 39.16 2.17 2.3002 4 2 2 4 39.50 6.71 2.2812 2 2 3 4 39.53 2.14 2.2795 6 2 0 4 40.60 5.79 2.2222 -6 0 6 2 40.99 1.42 2.2016 2 0 6 2 41.52 5.23 2.1751 -2 2 4 4 41.55 2.81 2.1733 -3 1 6 4 41.65 11.15 2.1687 10 0 2 2 41.65 10.82 2.1685 -1 1 6 4 41.81 2.68 2.1604 0 2 4 4 42.11 3.33 2.1459 -6 2 3 4 42.35 1.46 2.1343 4 2 3 4 42.59 3.60 2.1226 -4 2 4 4 43.10 2.39 2.0986 1 1 6 4 43.22 1.38 2.0931 8 0 4 2 43.45 1.71 2.0828 -11 1 2 4 43.45 11.64 2.0826 2 2 4 4 43.52 9.95 2.0796 7 1 4 4 43.77 1.09 2.0682 -12 0 2 2 43.89 4.38 2.0626 -8 2 1 4 43.91 1.08 2.0621 -8 0 6 2 44.33 4.38 2.0434 8 2 0 4 44.46 7.15 2.0376 4 0 6 2 44.47 20.16 2.0375 -8 2 2 4 44.96 5.22 2.0163 -6 2 4 4 45.81 3.05 1.9807 3 1 6 4 46.01 3.55 1.9725 -8 2 3 4 46.33 1.47 1.9599 4 2 4 4 46.84 9.66 1.9394 -11 1 4 4 48.08 1.74 1.8923 2 2 5 4 48.08 4.27 1.8923 8 2 2 4 48.45 1.23 1.8788 11 1 2 4 48.46 1.59 1.8784 -8 2 4 4 48.61 3.16 1.8730 -6 2 5 4 49.02 8.96 1.8585 -9 1 6 4 49.18 1.25 1.8526 12 0 2 2 49.61 6.40 1.8375 5 1 6 4 49.65 1.93 1.8362 -10 2 2 4 49.81 4.01 1.8308 10 0 4 2 50.27 3.30 1.8151 6 2 4 4 50.52 5.45 1.8066 -13 1 2 4 50.96 2.75 1.7919 4 2 5 4 51.15 3.58 1.7859 -3 3 1 4 51.40 1.67 1.7778 -14 0 2 2 51.45 15.14 1.7761 13 1 0 4 51.46 1.05 1.7757 0 2 6 4 51.46 1.90 1.7757 10 2 1 4 51.51 8.09 1.7741 -4 0 8 2 52.18 1.11 1.7531 -3 3 2 4 52.95 1.11 1.7292 -6 2 6 4 53.26 2.66 1.7200 -5 3 1 4 53.28 1.11 1.7194 2 2 6 4 53.33 2.06 1.7178 5 3 0 4 53.41 1.12 1.7156 3 3 2 4 53.50 2.03 1.7129 -12 0 6 2 53.53 1.09 1.7118 -1 3 3 4 53.63 2.16 1.7091 -11 1 6 4 53.81 4.64 1.7036 10 2 2 4 54.06 1.59 1.6965 -5 3 2 4 54.06 4.29 1.6964 -3 3 3 4 54.27 4.57 1.6902 5 3 1 4 54.35 1.16 1.6881 7 1 6 4 54.63 1.21 1.6800 -1 1 8 4 54.70 1.24 1.6780 2 0 8 2 55.58 1.02 1.6535 -12 2 2 4 55.69 1.09 1.6504 -8 2 6 4 56.05 1.61 1.6408 11 1 4 4 56.05 6.01 1.6408 5 3 2 4 56.16 2.59 1.6378 4 2 6 4 56.22 5.75 1.6363 1 1 8 4 56.43 1.35 1.6307 -1 3 4 4 56.53 1.52 1.6280 -4 2 7 4 56.74 4.17 1.6224 -3 3 4 4 56.93 1.02 1.6174 10 2 3 4 57.92 1.89 1.5921 4 0 8 2 58.85 1.40 1.5692 3 1 8 4 59.32 6.98 1.5580 -9 1 8 4 59.46 2.62 1.5545 -14 0 6 2 59.88 2.45 1.5447 9 1 6 4 60.04 2.19 1.5409 -1 3 5 4 60.57 1.30 1.5286 -7 3 4 4 60.76 3.03 1.5245 10 2 4 4 60.89 1.91 1.5215 -9 3 2 4 61.18 3.16 1.5149 -16 0 4 2 61.86 1.13 1.4999 4 2 7 4 62.26 6.61 1.4913 -4 2 8 4 62.34 1.37 1.4895 7 3 3 4 62.75 1.17 1.4807 -12 0 8 2 63.18 2.60 1.4717 13 1 4 4 64.02 3.19 1.4544 -12 2 6 4 64.30 1.29 1.4487 -14 2 4 4 65.39 1.54 1.4272 1 3 6 4 66.12 1.18 1.4132 11 1 6 4 66.58 1.00 1.4045 -11 3 3 4 67.07 1.37 1.3954 8 0 8 2 67.45 1.42 1.3885 17 1 0 4 67.51 1.71 1.3875 -17 1 4 4 68.12 1.85 1.3765 0 4 0 2 68.50 1.57 1.3698 0 4 1 4 69.34 2.10 1.3552 18 0 0 2 69.43 2.39 1.3536 -14 2 6 4 69.44 2.26 1.3536 -7 1 10 4 69.99 1.09 1.3442 -9 3 6 4 70.47 1.16 1.3362 5 3 6 4 70.54 3.56 1.3350 1 1 10 4 70.86 2.55 1.3299 15 1 4 4 71.02 2.11 1.3272 -16 2 4 4 71.22 1.59 1.3240 -13 3 1 4 71.97 2.56 1.3121 13 3 0 4 72.24 2.45 1.3078 9 1 8 4 72.48 1.33 1.3041 2 4 3 4 74.01 1.33 1.2809 -9 3 7 4 74.22 1.85 1.2778 -12 0 10 2 74.59 1.13 1.2723 -4 4 4 4 75.51 1.45 1.2591 -19 1 4 4 75.52 1.33 1.2590 -8 4 1 4 76.54 1.12 1.2447 8 2 8 4 78.61 1.05 1.2171 8 4 2 4 78.70 1.90 1.2158 18 2 0 4 79.01 1.02 1.2119 -6 4 5 4 79.28 3.11 1.2084 -17 1 8 4 81.62 1.05 1.1796 -2 0 12 2 83.38 1.49 1.1591 -21 1 2 4 83.39 1.35 1.1590 -12 2 10 4 84.14 1.37 1.1506 -7 1 12 4 89.17 1.01 1.0982 -17 1 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.