Sarrabusite Gemmi M, Campostrini I, Demartin F, Gorelik T E, Gamaccioli C M Acta Crystallographica B68 (2012) 15-23 Structure of the new mineral sarrabusite, Pb5CuCl4(SeO3)4, solved by manual electron-diffraction tomography Note: Automated data Locality: Baccu Locci mine, near Villaputzu, Sardinia, Italy _database_code_amcsd 0018633 CELL PARAMETERS: 24.9170 5.5060 14.2420 90.000 101.770 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1912.821 Density (g/cm3): 6.073 MAX. ABS. INTENSITY / VOLUME**2: 88.55004173 RIR: 4.748 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.25 1.17 12.1966 2 0 0 2 12.70 37.94 6.9713 0 0 2 2 13.28 7.78 6.6665 -2 0 2 2 14.53 12.62 6.0983 4 0 0 2 15.88 10.37 5.5817 2 0 2 2 19.78 6.81 4.4876 -3 1 1 4 21.22 3.46 4.1862 4 0 2 2 21.33 3.64 4.1651 1 1 2 4 21.86 1.34 4.0655 6 0 0 2 22.04 48.39 4.0327 -3 1 2 4 22.97 3.38 3.8725 -6 0 2 2 24.24 2.68 3.6724 -5 1 1 4 24.38 52.15 3.6515 5 1 0 4 24.52 13.73 3.6301 3 1 2 4 24.76 1.68 3.5952 -1 1 3 4 25.10 4.35 3.5481 -2 0 4 2 25.56 4.10 3.4856 0 0 4 2 25.76 2.32 3.4589 -5 1 2 4 25.76 5.89 3.4583 -3 1 3 4 26.15 5.62 3.4071 5 1 1 4 26.74 8.26 3.3333 -4 0 4 2 28.02 13.47 3.1842 2 0 4 2 29.29 10.39 3.0491 8 0 0 2 29.29 89.61 3.0489 5 1 2 4 29.48 33.78 3.0297 -8 0 2 2 29.93 31.03 2.9857 -1 1 4 4 30.18 15.95 2.9615 -6 0 4 2 30.36 1.70 2.9445 7 1 0 4 30.45 58.11 2.9358 -3 1 4 4 31.21 1.30 2.8657 1 1 4 4 32.07 2.21 2.7908 4 0 4 2 32.52 36.84 2.7530 0 2 0 2 32.70 7.03 2.7388 -5 1 4 4 33.17 5.45 2.7009 0 2 1 4 34.29 2.60 2.6152 2 2 1 4 34.42 7.05 2.6053 8 0 2 2 35.60 2.29 2.5216 -1 1 5 4 35.79 1.51 2.5092 4 2 0 4 36.39 2.34 2.4690 2 2 2 4 36.39 4.05 2.4689 -7 1 4 4 36.46 2.31 2.4645 -10 0 2 2 36.85 3.48 2.4393 10 0 0 2 36.85 8.60 2.4390 -9 1 2 4 36.97 2.06 2.4317 9 1 0 4 37.25 1.82 2.4140 6 0 4 2 37.91 1.79 2.3734 -2 0 6 2 38.54 1.43 2.3358 -4 0 6 2 38.75 1.27 2.3238 0 0 6 2 38.93 1.21 2.3136 7 1 3 4 39.16 1.29 2.3002 4 2 2 4 39.50 5.61 2.2812 2 2 3 4 39.53 1.98 2.2795 6 2 0 4 40.60 4.93 2.2222 -6 0 6 2 40.99 1.56 2.2016 2 0 6 2 41.52 4.40 2.1751 -2 2 4 4 41.55 2.19 2.1733 -3 1 6 4 41.65 9.06 2.1687 10 0 2 2 41.65 10.39 2.1685 -1 1 6 4 41.81 2.46 2.1604 0 2 4 4 42.11 2.94 2.1459 -6 2 3 4 42.35 1.05 2.1343 4 2 3 4 42.59 2.35 2.1226 -4 2 4 4 43.10 2.38 2.0986 1 1 6 4 43.22 1.24 2.0931 8 0 4 2 43.45 1.36 2.0828 -11 1 2 4 43.45 10.58 2.0826 2 2 4 4 43.52 7.75 2.0796 7 1 4 4 43.89 4.11 2.0626 -8 2 1 4 43.91 1.16 2.0621 -8 0 6 2 44.33 4.17 2.0434 8 2 0 4 44.46 6.41 2.0376 4 0 6 2 44.47 20.31 2.0375 -8 2 2 4 44.96 5.09 2.0163 -6 2 4 4 45.81 2.54 1.9807 3 1 6 4 46.01 2.81 1.9725 -8 2 3 4 46.33 1.02 1.9599 4 2 4 4 46.84 10.18 1.9394 -11 1 4 4 48.08 1.67 1.8923 2 2 5 4 48.08 3.12 1.8923 8 2 2 4 48.45 1.78 1.8788 11 1 2 4 48.46 1.06 1.8784 -8 2 4 4 48.61 2.53 1.8730 -6 2 5 4 49.02 8.97 1.8585 -9 1 6 4 49.61 5.68 1.8375 5 1 6 4 49.65 2.20 1.8362 -10 2 2 4 49.81 5.20 1.8308 10 0 4 2 50.27 2.74 1.8151 6 2 4 4 50.52 3.95 1.8066 -13 1 2 4 50.96 2.10 1.7919 4 2 5 4 51.15 2.89 1.7859 -3 3 1 4 51.40 1.25 1.7778 -14 0 2 2 51.45 14.22 1.7761 13 1 0 4 51.46 1.49 1.7757 0 2 6 4 51.46 1.46 1.7757 10 2 1 4 51.51 7.10 1.7741 -4 0 8 2 52.18 1.16 1.7531 -3 3 2 4 53.26 1.91 1.7200 -5 3 1 4 53.28 1.50 1.7194 2 2 6 4 53.33 1.97 1.7178 5 3 0 4 53.41 1.06 1.7156 3 3 2 4 53.50 1.40 1.7129 -12 0 6 2 53.63 1.58 1.7091 -11 1 6 4 53.81 1.46 1.7037 -14 0 4 2 53.81 3.40 1.7036 10 2 2 4 54.06 3.49 1.6964 -3 3 3 4 54.27 3.46 1.6902 5 3 1 4 54.35 1.32 1.6881 7 1 6 4 54.63 1.05 1.6800 -1 1 8 4 54.70 1.26 1.6780 2 0 8 2 55.58 1.04 1.6535 -12 2 2 4 56.05 1.18 1.6408 11 1 4 4 56.05 6.26 1.6408 5 3 2 4 56.16 2.51 1.6378 4 2 6 4 56.22 3.26 1.6363 1 1 8 4 56.43 1.26 1.6307 -1 3 4 4 56.53 1.15 1.6280 -4 2 7 4 56.74 4.37 1.6224 -3 3 4 4 57.92 1.71 1.5921 4 0 8 2 58.85 1.51 1.5692 3 1 8 4 59.32 5.87 1.5580 -9 1 8 4 59.35 1.11 1.5571 -16 0 2 2 59.46 2.52 1.5545 -14 0 6 2 59.88 1.21 1.5447 9 1 6 4 60.04 1.64 1.5409 -1 3 5 4 60.57 1.31 1.5286 -7 3 4 4 60.76 3.83 1.5245 10 2 4 4 60.89 1.45 1.5215 -9 3 2 4 61.18 2.09 1.5149 -16 0 4 2 62.26 5.65 1.4913 -4 2 8 4 62.34 1.27 1.4895 7 3 3 4 63.18 2.65 1.4717 13 1 4 4 64.02 2.20 1.4544 -12 2 6 4 64.30 1.66 1.4487 -14 2 4 4 65.39 1.31 1.4272 1 3 6 4 67.07 1.28 1.3954 8 0 8 2 67.51 1.57 1.3875 -17 1 4 4 68.12 1.66 1.3765 0 4 0 2 68.50 1.35 1.3698 0 4 1 4 69.34 1.77 1.3552 18 0 0 2 69.43 2.21 1.3536 -14 2 6 4 69.44 1.18 1.3536 -7 1 10 4 69.99 1.08 1.3442 -9 3 6 4 70.54 2.87 1.3350 1 1 10 4 70.86 2.06 1.3299 15 1 4 4 71.02 1.27 1.3272 -16 2 4 4 71.22 1.24 1.3240 -13 3 1 4 71.97 2.46 1.3121 13 3 0 4 72.24 2.42 1.3078 9 1 8 4 72.48 1.09 1.3041 2 4 3 4 74.01 1.01 1.2809 -9 3 7 4 74.22 1.36 1.2778 -12 0 10 2 75.51 1.50 1.2591 -19 1 4 4 75.52 1.08 1.2590 -8 4 1 4 76.54 1.06 1.2447 8 2 8 4 78.70 1.59 1.2158 18 2 0 4 79.28 2.05 1.2084 -17 1 8 4 83.38 1.02 1.1591 -21 1 2 4 83.39 1.03 1.1590 -12 2 10 4 84.14 1.04 1.1506 -7 1 12 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.