Parasterryite Moelo Y, Guillot-Deudon C, Evain M, Orlandi P, Biagioni C Acta Crystallographica B68 (2012) 480-492 Comparative modular analysis of two complex sulfosalt structures: sterryite, Cu(Ag,Cu)3Pb19-(Sb,As)22(As-As)S56, and parasterryite, Ag4Pb20(Sb,As)24S58 Locality: Pollone mine, Tuscany, Italy _database_code_amcsd 0019483 8.3965 27.954 43.884 90 90.061 90 P2_1/c atom x y z occ Uiso U(1,1) U(2,2) U(3,3) U(1,2) U(1,3) U(2,3) Pb1 .36763 .36216 .18873 .0223 .0238 .0237 .0194 .0013 .0021 .0004 Pb2 .87463 .36391 .18918 .0242 .0275 .0248 .0203 -.0005 .0044 .0006 Pb3 .36370 .29977 .09552 .0239 .0245 .0213 .0261 -.0004 .0036 -.0048 Pb4 .86185 .29243 .10178 .0243 .0283 .0211 .0233 .0012 .0003 -.0024 Pb5 .35693 .45226 .10872 .0250 .0261 .0225 .0265 -.0014 .0037 .0030 Pb6 .85479 .45238 .10944 .0256 .0273 .0205 .0288 .0005 .0021 .0033 Ag7 .3362 .58389 .10610 .0555 .0449 .0421 .080 -.0317 .0088 -.0074 Pb8 .81865 .59875 .11581 .0323 .0338 .0228 .0403 -.0028 -.0014 .0096 As9 .6226 .49315 .18644 .0159 .0154 .0151 .0171 .0010 .0030 -.0006 Sb10 .1312 .49109 .19319 .0210 .0290 .0158 .0181 .0008 .0015 -.0019 Sb11 .3725 .90657 .23240 .12 .0173 .0123 .0238 .0157 .0011 .0012 -.0001 As11 .3725 .90657 .23240 .88 .0173 .0123 .0238 .0157 .0011 .0012 -.0001 Sb12 .8665 .91492 .23679 .87 .0203 .0254 .0153 .0203 -.0007 .0023 .0029 As12 .8665 .91492 .23679 .13 .0203 .0254 .0153 .0203 -.0007 .0023 .0029 Pb13 .61281 .78747 .22624 .0293 .0302 .0264 .0312 .0003 .0105 .0028 Pb14 .13196 .78428 .22712 .0250 .0256 .0266 .0230 -.0007 -.0027 .0000 Sb15 .5937 .22519 .16976 .91 .0191 .0247 .0146 .0182 -.0004 -.0003 .0007 As15 .5937 .22519 .16976 .09 .0191 .0247 .0146 .0182 -.0004 -.0003 .0007 As16 .1231 .23186 .17065 .0163 .0172 .0144 .0175 -.0006 .0017 .0007 Sb17 .6199 .16758 .09448 .43 .0210 .0180 .0239 .0212 .0001 .0039 .0037 As17 .6199 .16758 .09448 .57 .0210 .0180 .0239 .0212 .0001 .0039 .0037 Sb18 .1139 .15868 .08751 .0215 .0161 .0161 .0323 -.0010 .0008 .0002 Sb19 .6161 .07517 .00797 .8 .0168 .0166 .0176 .0160 -.0021 .0017 .0012 As19 .6161 .07517 .00797 .2 .0168 .0166 .0176 .0160 -.0021 .0017 .0012 Pb20 .1146 .08099 .01537 .46 .0319 .0249 .0453 .0256 .0033 .0036 .0110 Sb20 .1146 .08099 .01537 .54 .0319 .0249 .0453 .0256 .0033 .0036 .0110 Pb21 .38579 .00515 .06394 .0222 .0238 .0180 .0248 .0005 .0016 .0021 Sb22 .8772 .00802 .07129 .78 .0177 .0171 .0175 .0187 -.0012 .0037 .0018 As22 .8772 .00802 .07129 .22 .0177 .0171 .0175 .0187 -.0012 .0037 .0018 Sb23 .3700 .07949 .15271 .82 .0186 .0166 .0184 .0209 -.0014 .0030 -.0026 As23 .3700 .07949 .15271 .18 .0186 .0166 .0184 .0209 -.0014 .0030 -.0026 Pb24 .88296 .08179 .14700 .0230 .0249 .0183 .0258 .0014 .0023 .0005 Ag25 .3523 .16014 .23146 .0351 .0497 .0209 .0347 .0000 .0020 .0079 Sb26 .8696 .16689 .22674 .7 .0208 .0229 .0237 .0156 .0023 .0047 .0011 As26 .8696 .16689 .22674 .3 .0208 .0229 .0237 .0156 .0023 .0047 .0011 Pb27 .39721 .61845 .19934 .0276 .0262 .0308 .0258 .0014 .0009 .0021 Sb28 .8947 .61462 .20042 .6 .0210 .0188 .0270 .0174 -.0015 .0004 .0035 As28 .8947 .61462 .20042 .4 .0210 .0188 .0270 .0174 -.0015 .0004 .0035 Sb29 .6118 .03729 .22421 .0211 .0201 .0234 .0199 -.0023 .0001 -.0010 Pb30 .11604 .02959 .22269 .0251 .0268 .0238 .0247 -.0029 .0018 .0027 Pb31 .62627 .94878 .14183 .0233 .0212 .0215 .0271 .0024 .0002 -.0021 Pb32 .11873 .95038 .14272 .0227 .0210 .0191 .0279 -.0007 .0018 -.0030 Pb33a .62472 .86693 .06450 .0248 .0229 .0267 .0248 .0024 -.0004 -.0059 Pb34a .14489 .87105 .06308 .0233 .0231 .0241 .0227 -.0045 .0040 -.0021 Pb35 .35797 .21290 .01550 .0273 .0274 .0254 .0291 .0028 .0029 -.0013 Pb36 .86164 .21330 .01791 .0237 .0232 .0261 .0218 -.0039 .0022 .0002 As37 .5987 .38671 .03818 .95 .0162 .0145 .0182 .0159 -.0006 .0034 -.0020 Sb37 .5987 .38671 .03818 .05 .0162 .0145 .0182 .0159 -.0006 .0034 -.0020 Sb38 .1380 .39220 .03406 .9 .0207 .0253 .0193 .0175 -.0057 .0013 .0000 As38 .1380 .39220 .03406 .1 .0207 .0253 .0193 .0175 -.0057 .0013 .0000 Sb39 .6318 .52810 .03770 .57 .0220 .0179 .0229 .0251 -.0022 .0020 .0077 As39 .6318 .52810 .03770 .43 .0220 .0179 .0229 .0251 -.0022 .0020 .0077 Sb40 .0989 .52584 .04232 .87 .0201 .0200 .0201 .0202 -.0037 .0025 .0009 As40 .0989 .52584 .04232 .13 .0201 .0200 .0201 .0202 -.0037 .0025 .0009 Sb41 .5784 .66010 .04420 .0215 .0203 .0162 .0281 -.0026 -.0015 .0012 As42 .1522 .66143 .02030 .0173 .0144 .0173 .0203 .0000 .0025 -.0006 As43 .9503 .75165 .06151 .0176 .0201 .0134 .0194 -.0015 .0039 .0019 Pb44a .6387 .74091 .12709 .75 .0228 .0259 .0197 .0227 -.0043 .0044 .0000 Sb44b .650 .7466 .1205 .25 .034 .046 .040 .016 -.032 .030 -.012 Ag45 .2654 .70516 .09631 .0543 .0286 .074 .0603 .0093 -.0050 -.0083 Ag46 .0835 .71966 .15450 .0559 .081 .0287 .0576 -.0063 .0141 -.0071 Sb47 .3303 .83235 .14525 .35 .0260 .0223 .0246 .0310 .0085 .0100 .0095 As47 .3303 .83235 .14525 .65 .0260 .0223 .0246 .0310 .0085 .0100 .0095 As48 .8846 .84764 .16134 .0169 .0158 .0143 .0205 -.0007 .0020 -.0043 S1 .6128 .30470 .14902 .0185 .023 .009 .023 .001 .002 -.0015 S2 .1178 .3032 .14703 .0178 .023 .015 .016 -.003 .001 .0014 S3 .6084 .3777 .08942 .0156 .018 .017 .011 -.002 .003 -.0033 S4 .1212 .37573 .08806 .0159 .018 .016 .014 .002 .006 .0042 S5 .6167 .4229 .15998 .0174 .016 .016 .020 .001 .001 -.0014 S6 .1232 .42371 .15807 .0172 .022 .014 .015 -.006 .004 .0013 S7 .6268 .3412 .23469 .0174 .018 .020 .015 -.003 .003 -.0038 S8 .1314 .3382 .23789 .0177 .019 .018 .016 .000 .004 .0016 S9 .6118 .23581 .06312 .0172 .017 .014 .020 .000 .002 .000 S10 .1119 .2392 .06355 .0170 .013 .015 .023 -.001 .003 -.002 S11 .6102 .5196 .09193 .0164 .015 .018 .016 -.004 .002 .0049 S12 .1065 .5302 .09812 .0176 .014 .021 .017 .000 .002 .001 S13 .4124 .5310 .16301 .0203 .017 .025 .020 -.001 .001 .003 S14 .8350 .5246 .16117 .0184 .020 .013 .022 -.005 -.002 -.001 S15 .3397 .4508 .22736 .0179 .021 .017 .016 .001 .003 .003 S16 .9195 .4492 .22794 .0164 .015 .018 .016 .000 .002 -.004 S17 .5801 .8792 .20257 .0201 .020 .027 .014 .003 .005 .003 S18 .1613 .8827 .20223 .0179 .018 .019 .016 .000 .001 .003 S19 .3391 .2442 .20238 .0188 .015 .027 .015 .002 -.001 -.001 S20 .9211 .2497 .20391 .0198 .021 .021 .018 .000 .000 .004 S21 .4117 .1926 .12933 .0201 .020 .019 .021 -.003 .001 -.002 S22 .8298 .1955 .12646 .0204 .027 .013 .022 .000 .000 .000 S23 .3354 .1299 .05158 .0184 .013 .017 .025 -.004 .002 .001 S24 .8962 .1267 .05336 .0174 .014 .014 .023 -.005 -.002 .000 S25 .6067 .9543 .02238 .0210 .017 .016 .030 .000 -.005 .009 S26 .1601 .9522 .02319 .0204 .021 .020 .020 .001 .003 .002 S27 .6556 .0338 .10331 .0230 .022 .019 .028 .003 .006 .002 S28 .1024 .0356 .10293 .0207 .026 .016 .020 -.003 .003 .001 S29 .5970 .1057 .18492 .0204 .023 .015 .023 .002 -.001 .002 S30 .1581 .1115 .18398 .0217 .023 .019 .024 -.005 .002 .002 S31 .3492 .6990 .24609 .0242 .026 .019 .028 -.001 .001 .000 S32 .9218 .6860 .23571 .0208 .022 .020 .021 -.001 .002 -.004 S33 .6860 .6526 .17319 .029 .028 .023 .035 -.003 -.001 .009 S34 .0939 .6303 .16317 .030 .028 .028 .032 .006 .002 .008 S35 .5988 .5746 .24488 .0267 .018 .036 .026 -.002 .007 .002 S36 .1625 .5719 .24762 .0204 .021 .018 .022 .001 .005 .001 S37 .6358 .4985 .32563 .0190 .013 .016 .028 -.003 .001 .002 S38 .1140 .4981 .32276 .0199 .019 .015 .025 -.003 .004 .000 S39 .3796 .9258 .09634 .0171 .014 .019 .018 -.001 .005 -.0008 S40 .8829 .9279 .09136 .0200 .021 .017 .022 -.002 .004 .001 S41 .3884 .8440 .01412 .0190 .021 .021 .016 .003 .002 .001 S42 .8890 .84341 .01686 .0162 .019 .011 .018 -.006 .000 -.0024 S43 .3975 .3338 .02800 .0176 .015 .020 .017 -.003 .000 -.002 S44 .8137 .3337 .03128 .0202 .018 .024 .019 .005 .004 -.005 S45 .3230 .4604 .03968 .0202 .020 .020 .021 -.003 .002 -.002 S46 .9069 .4616 .03874 .0190 .019 .013 .025 .002 -.003 .000 S47 .4112 .5896 .03314 .0231 .024 .018 .028 .000 -.001 -.002 S48 .8246 .5900 .04252 .0216 .022 .017 .026 -.004 .005 .009 S49 .3297 .7174 .03390 .0188 .019 .019 .018 .000 .000 -.002 S50 .9310 .7104 .01616 .0180 .015 .019 .021 .003 .004 -.004 S51 .6874 .7623 .06275 .0198 .025 .015 .020 .006 .007 .000 S52 .3758 .7929 .09786 .0218 .022 .026 .017 .001 .001 -.006 S53 .6749 .8420 .13026 .0186 .023 .014 .018 .003 .005 .006 S54 1.0593 .8227 .12564 .0236 .019 .029 .022 .000 .007 .000 S55 .3550 .7631 .17457 .0255 .031 .020 .025 .005 .009 .003 S56 .8673 .7755 .18359 .0187 .016 .023 .017 -.002 .002 .002 S57 .5126 .6530 .10049 .0219 .025 .020 .020 -.002 .001 -.002 S58 .9728 .6938 .09658 .030 .029 .030 .030 -.010 -.006 .013