H9 K3 O14 P2 Te Averbuch-Pouchot M, Durif A Acta Crystallographica C39 (1983) 27-28 Structure of a potassium diphosphate tellurate hydrate (K3HP2O7)(Te(OH)6)(H2O) _cod_database_code 1007096 _database_code_amcsd 0009969 CELL PARAMETERS: 15.9800 7.2260 6.2530 109.490 84.340 101.830 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 665.855 Density (g/cm3): 2.647 MAX. ABS. INTENSITY / VOLUME**2: 7.840330575 RIR: 0.964 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.32 44.20 7.8161 2 0 0 2 13.22 17.69 6.6963 0 1 0 2 13.40 1.74 6.6099 -1 1 0 2 15.04 35.12 5.8915 0 0 1 2 15.77 50.38 5.6201 -2 1 0 2 15.90 3.32 5.5736 1 0 1 2 16.54 80.71 5.3607 0 -1 1 2 17.02 2.10 5.2107 3 0 0 2 18.34 6.71 4.8374 2 -1 1 2 18.42 2.12 4.8165 -1 -1 1 2 18.56 76.67 4.7806 2 0 1 2 18.97 88.05 4.6788 2 1 0 2 19.16 28.16 4.6323 -2 0 1 2 21.70 23.03 4.0962 -2 -1 1 2 22.75 26.53 3.9080 4 0 0 2 23.09 97.32 3.8512 0 1 1 2 24.17 20.28 3.6821 -4 1 0 2 24.90 30.19 3.5759 -2 1 1 2 25.47 2.73 3.4973 1 -2 1 2 25.73 78.53 3.4626 4 -1 1 2 25.86 5.20 3.4446 -3 -1 1 2 26.04 52.65 3.4222 0 -2 1 2 26.18 56.53 3.4038 2 -2 1 2 26.62 44.17 3.3482 0 2 0 2 26.65 4.89 3.3449 2 1 1 2 27.62 1.68 3.2296 -3 1 1 2 27.80 100.00 3.2086 -4 0 1 2 27.81 3.45 3.2075 -1 -2 1 2 28.08 1.91 3.1774 3 -2 1 2 28.48 30.88 3.1342 4 1 0 2 28.80 2.14 3.0997 1 -1 2 2 28.92 37.37 3.0873 0 -1 2 2 29.22 1.54 3.0559 -5 1 0 2 29.82 23.45 2.9957 2 -1 2 2 30.17 1.51 2.9626 -1 -1 2 2 30.45 2.48 2.9358 5 -1 1 2 30.61 4.86 2.9210 -2 -2 1 2 30.70 2.69 2.9122 1 0 2 2 31.08 3.08 2.8777 -1 0 2 2 31.85 25.59 2.8101 -4 2 0 2 31.89 4.10 2.8065 3 -1 2 2 31.96 2.03 2.7999 5 0 1 2 32.12 10.81 2.7868 2 0 2 2 32.42 3.59 2.7614 -2 -1 2 2 32.84 9.64 2.7272 -2 0 2 2 32.89 1.40 2.7232 1 -2 2 2 33.37 2.26 2.6852 2 -2 2 2 34.03 16.92 2.6345 4 1 1 2 34.48 2.59 2.6011 3 0 2 2 34.83 3.71 2.5762 4 -1 2 2 34.95 6.33 2.5673 -1 -2 2 2 35.27 1.22 2.5448 -2 2 1 2 35.49 2.30 2.5291 -3 0 2 2 35.55 21.13 2.5252 6 -1 1 2 36.04 2.51 2.4920 1 2 1 2 37.17 3.94 2.4187 4 -2 2 2 37.28 21.01 2.4122 6 0 1 2 37.31 4.40 2.4100 -1 1 2 2 37.34 9.65 2.4082 -2 -2 2 2 37.45 2.25 2.4011 1 -3 1 2 37.57 1.21 2.3939 2 -3 1 2 37.63 15.38 2.3903 4 0 2 2 38.14 6.60 2.3596 2 2 1 2 38.23 4.33 2.3544 -6 0 1 2 38.25 8.26 2.3532 0 -3 1 2 38.37 2.57 2.3456 -4 -2 1 2 38.44 4.60 2.3416 -2 1 2 2 38.48 3.63 2.3394 4 2 0 2 38.88 6.03 2.3162 -4 0 2 2 39.28 5.64 2.2935 -4 -1 2 2 39.37 4.15 2.2886 -4 2 1 2 39.75 2.55 2.2677 -6 2 0 2 39.90 1.32 2.2594 -1 -3 1 2 39.92 15.06 2.2585 -2 3 0 2 40.12 1.06 2.2474 -6 1 1 2 40.41 24.96 2.2321 0 3 0 2 40.41 1.63 2.2319 -3 1 2 2 40.47 5.47 2.2287 -3 -2 2 2 41.11 2.05 2.1957 -6 -1 1 2 41.42 1.17 2.1799 5 0 2 2 41.43 5.08 2.1793 2 -3 2 2 42.20 1.48 2.1414 0 -3 2 2 42.30 2.93 2.1365 3 -3 2 2 42.34 12.16 2.1349 -2 -3 1 2 42.66 12.35 2.1192 6 -1 2 2 42.81 1.82 2.1123 -4 3 0 2 43.05 2.17 2.1009 5 2 0 2 43.07 3.32 2.1000 5 -3 1 2 43.13 26.66 2.0974 -4 1 2 2 43.97 2.90 2.0594 4 -3 2 2 43.98 2.82 2.0588 6 -2 2 2 44.16 1.07 2.0509 2 -1 3 2 44.19 4.33 2.0493 2 3 0 2 44.22 12.89 2.0481 -4 -2 2 2 44.44 1.21 2.0385 -7 2 0 2 44.51 2.96 2.0357 4 2 1 2 44.92 1.00 2.0180 1 -2 3 2 45.19 1.55 2.0065 -7 1 1 2 45.22 1.99 2.0052 2 -2 3 2 45.73 8.25 1.9841 6 0 2 2 45.93 11.68 1.9758 -8 1 0 2 46.23 4.40 1.9638 0 0 3 2 46.32 10.73 1.9600 -2 -1 3 2 46.34 1.81 1.9591 6 -3 1 2 46.47 1.03 1.9540 8 0 0 2 46.49 2.78 1.9534 -5 1 2 2 46.57 2.52 1.9501 8 -1 1 2 46.66 1.92 1.9468 -1 -2 3 2 47.20 3.11 1.9256 0 2 2 2 47.33 3.30 1.9206 -6 0 2 2 47.36 8.83 1.9196 2 0 3 2 47.68 5.61 1.9073 -2 2 2 2 48.01 5.73 1.8950 0 3 1 2 48.02 1.44 1.8946 6 2 0 2 48.11 1.60 1.8915 4 -2 3 2 48.14 6.56 1.8901 -2 0 3 2 48.31 1.56 1.8838 -6 -1 2 2 48.41 1.13 1.8802 5 1 2 2 48.48 1.39 1.8776 -5 -2 2 2 48.61 7.24 1.8731 8 0 1 2 48.63 1.29 1.8723 -2 -2 3 2 49.14 4.35 1.8539 -4 -3 1 2 49.40 9.40 1.8450 6 -3 2 2 49.51 1.73 1.8411 -8 2 0 2 49.63 2.62 1.8368 -8 0 1 2 49.71 2.21 1.8342 2 2 2 2 50.33 6.73 1.8129 2 -3 3 2 50.36 1.20 1.8118 1 -3 3 2 50.37 8.71 1.8116 -4 3 1 2 50.40 6.11 1.8107 -6 1 2 2 50.47 1.35 1.8083 7 0 2 2 50.57 2.45 1.8049 -8 1 1 2 50.60 5.88 1.8040 2 -4 1 2 50.68 4.20 1.8012 4 3 0 2 51.03 4.84 1.7896 8 1 0 2 51.38 1.83 1.7783 4 0 3 2 51.74 3.30 1.7667 0 -4 1 2 51.77 8.88 1.7659 -4 -1 3 2 52.31 3.50 1.7490 4 -4 1 2 52.32 4.16 1.7487 2 -4 2 2 52.57 7.31 1.7408 6 1 2 2 52.61 3.70 1.7396 -8 -1 1 2 52.68 1.56 1.7374 -4 -3 2 2 52.70 1.34 1.7369 9 0 0 2 52.88 4.53 1.7313 8 -2 2 2 53.06 7.30 1.7258 6 2 1 2 53.42 1.20 1.7152 -7 -1 2 2 53.56 5.90 1.7111 0 -4 2 2 53.69 11.69 1.7073 6 -2 3 2 53.87 3.57 1.7019 4 -4 2 2 53.94 2.98 1.6997 6 -1 3 2 54.24 2.53 1.6912 2 1 3 2 54.46 1.24 1.6849 5 -3 3 2 54.49 1.75 1.6839 8 -3 1 2 54.67 3.93 1.6787 -2 -3 3 2 54.84 4.60 1.6741 0 4 0 2 54.90 2.41 1.6724 4 2 2 2 55.28 4.47 1.6617 -8 2 1 2 55.58 5.88 1.6535 8 0 2 2 55.62 3.09 1.6525 -4 4 0 2 55.68 6.75 1.6508 -6 3 1 2 56.62 2.02 1.6255 -8 3 0 2 56.69 4.74 1.6237 6 -4 1 2 57.00 4.14 1.6155 4 3 1 2 57.03 1.24 1.6148 -6 2 2 2 57.11 1.81 1.6128 8 -3 2 2 57.44 7.07 1.6043 -8 0 2 2 57.46 4.01 1.6037 -2 -4 2 2 57.60 1.01 1.6002 -4 1 3 2 57.87 1.84 1.5935 6 0 3 2 57.98 1.62 1.5906 -6 -3 1 2 58.08 2.13 1.5882 -10 1 0 2 58.46 1.72 1.5787 2 4 0 2 58.48 1.61 1.5782 4 1 3 2 58.51 3.25 1.5775 10 -1 1 2 58.94 1.46 1.5671 8 2 0 2 59.10 2.16 1.5632 10 0 0 2 59.46 1.80 1.5545 -6 -1 3 2 59.66 6.47 1.5498 2 -2 4 2 59.90 3.63 1.5441 -6 0 3 2 59.92 1.17 1.5437 0 -2 4 2 59.95 1.06 1.5430 -6 4 0 2 59.98 1.29 1.5424 0 -4 3 2 60.08 2.58 1.5400 2 -1 4 2 60.67 1.23 1.5263 -4 -3 3 2 61.28 2.58 1.5127 -6 -3 2 2 61.56 2.71 1.5065 -2 4 1 2 61.74 3.54 1.5026 -4 3 2 2 61.88 1.50 1.4994 -4 -4 1 2 61.91 1.02 1.4988 -10 0 1 2 62.00 1.14 1.4968 0 2 3 2 62.16 3.07 1.4934 2 3 2 2 62.24 5.06 1.4916 8 -1 3 2 62.35 1.25 1.4893 0 4 1 2 62.50 4.34 1.4861 -6 -2 3 2 62.51 1.61 1.4858 -2 2 3 2 62.72 1.58 1.4813 -2 -2 4 2 62.90 3.24 1.4775 4 -1 4 2 63.27 2.71 1.4697 8 2 1 2 63.29 3.44 1.4694 -4 4 1 2 63.36 3.32 1.4679 10 -2 2 2 63.39 1.39 1.4674 8 -4 1 2 63.42 1.14 1.4667 10 -1 2 2 63.70 1.74 1.4609 -8 -2 2 2 63.74 3.45 1.4602 -2 -4 3 2 63.87 3.19 1.4575 6 -4 3 2 63.93 1.78 1.4561 2 0 4 2 64.38 3.32 1.4471 10 -3 1 2 64.44 2.05 1.4458 4 4 0 2 64.79 2.23 1.4389 -2 0 4 2 64.91 2.30 1.4365 6 3 1 2 64.92 1.21 1.4364 2 -5 1 2 65.03 1.21 1.4342 -10 -1 1 2 65.09 1.42 1.4331 -8 2 2 2 65.49 2.42 1.4252 -4 2 3 2 65.61 2.70 1.4230 2 4 1 2 65.83 2.13 1.4187 -10 2 1 2 65.86 1.51 1.4181 4 -5 1 2 66.41 1.79 1.4078 10 1 1 2 66.42 2.99 1.4075 0 -5 1 2 66.73 2.56 1.4017 -2 -3 4 2 66.78 1.43 1.4008 0 -5 2 2 66.83 1.08 1.4000 10 0 2 2 68.08 2.06 1.3772 6 -1 4 2 68.45 1.49 1.3706 -8 -3 1 2 68.85 1.98 1.3636 -4 0 4 2 68.93 1.28 1.3623 -2 5 0 2 68.97 1.44 1.3616 2 -4 4 2 69.25 1.40 1.3567 6 -5 2 2 69.50 2.30 1.3524 8 3 0 2 69.63 1.05 1.3502 0 1 4 2 69.68 1.97 1.3494 2 -5 3 2 69.95 2.29 1.3449 -4 5 0 2 70.72 1.73 1.3321 -2 1 4 2 70.79 2.36 1.3310 -6 2 3 2 70.91 2.49 1.3290 2 1 4 2 71.07 1.43 1.3264 10 -2 3 2 71.15 2.04 1.3251 -12 1 0 2 71.32 1.71 1.3224 -10 -2 1 2 72.01 2.30 1.3114 -8 1 3 2 72.05 1.50 1.3108 12 -2 1 2 72.30 1.04 1.3069 10 -1 3 2 72.50 1.67 1.3038 6 4 0 2 72.57 2.67 1.3027 12 0 0 2 72.89 2.57 1.2978 -2 4 2 2 73.44 3.28 1.2894 6 -5 3 2 73.54 3.67 1.2879 6 -4 4 2 73.58 2.73 1.2873 -6 -1 4 2 73.78 1.24 1.2843 -8 4 1 2 73.79 1.78 1.2841 -2 3 3 2 74.45 3.93 1.2744 6 3 2 2 74.58 1.06 1.2724 -4 4 2 2 74.66 1.09 1.2712 8 3 1 2 74.96 1.89 1.2670 6 2 3 2 74.97 2.88 1.2668 -12 1 1 2 75.16 2.59 1.2641 -10 4 0 2 75.81 1.48 1.2549 12 -1 2 2 76.15 3.43 1.2500 2 3 3 2 76.66 1.15 1.2431 10 0 3 2 76.92 1.33 1.2395 -4 -5 2 2 77.62 2.01 1.2300 0 -1 5 2 77.78 1.91 1.2279 2 -1 5 2 77.82 2.13 1.2274 -12 3 0 2 77.88 2.27 1.2267 -6 -4 3 2 78.10 1.11 1.2237 2 -5 4 2 78.11 2.06 1.2235 10 -4 3 2 78.55 1.73 1.2178 -6 4 2 2 78.58 1.96 1.2175 -12 -1 1 2 78.68 1.41 1.2161 4 -5 4 2 78.89 1.79 1.2134 -8 5 0 2 79.21 1.77 1.2093 -2 -2 5 2 79.87 1.39 1.2009 -6 -3 4 2 80.70 2.42 1.1907 2 2 4 2 81.32 1.01 1.1832 -6 5 1 2 81.60 1.20 1.1798 4 4 2 2 82.19 1.12 1.1728 -8 -4 2 2 82.35 1.74 1.1709 10 -5 2 2 82.51 1.37 1.1691 10 -5 1 2 82.54 2.41 1.1688 2 -4 5 2 82.54 1.21 1.1687 -10 3 2 2 82.73 1.16 1.1666 10 2 2 2 83.03 1.08 1.1631 6 -3 5 2 83.19 1.20 1.1613 10 -3 4 2 83.72 1.14 1.1552 -2 -5 4 2 84.63 1.53 1.1451 12 2 0 2 85.03 1.01 1.1407 0 -6 3 2 85.24 1.69 1.1385 4 0 5 2 85.33 1.08 1.1375 7 -2 5 2 86.21 1.06 1.1281 10 3 1 2 87.23 1.01 1.1176 4 5 1 2 87.38 1.17 1.1161 0 6 0 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.