F12 H2 Np3 O Cousson A, Abazli H, Pages M, Gasperin M Acta Crystallographica C39 (1983) 425-427 Tetrafluorure de Neptunium Hydrate, Np3 F12 1. 1H H2 O _cod_database_code 1001844 _database_code_amcsd 0009974 CELL PARAMETERS: 8.4550 8.8580 8.3960 113.830 116.640 58.030 SPACE GROUP: P1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 465.156 Density (g/cm3): 6.817 MAX. ABS. INTENSITY / VOLUME**2: 77.20034189 RIR: 3.687 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.07 12.61 7.3308 0 1 0 1 12.09 12.16 7.3213 0 0 1 1 12.95 31.03 6.8374 1 0 0 1 12.95 30.97 6.8364 -1 -1 1 1 13.43 1.48 6.5938 1 1 0 1 15.11 3.61 5.8645 0 -1 1 1 18.92 11.99 4.6905 0 1 1 1 20.26 21.46 4.3839 -1 -2 1 1 20.27 21.38 4.3803 1 0 1 1 21.12 100.00 4.2071 -2 -1 1 1 21.21 51.67 4.1887 -1 1 0 1 21.23 52.03 4.1846 -1 -1 2 1 22.10 41.72 4.0218 1 2 0 1 22.12 42.28 4.0188 1 1 1 1 23.84 11.02 3.7328 -1 1 1 1 23.86 10.71 3.7301 -1 0 2 1 24.28 32.80 3.6654 0 2 0 1 24.31 32.02 3.6606 0 0 2 1 24.66 57.00 3.6105 0 -2 1 1 24.68 56.65 3.6071 0 -1 2 1 25.11 2.31 3.5458 1 -1 1 1 25.12 2.15 3.5454 -1 -2 2 1 25.20 26.96 3.5339 -2 0 1 1 25.21 27.56 3.5325 -2 -1 2 1 26.06 10.03 3.4187 2 0 0 1 26.07 10.01 3.4182 -2 -2 2 1 27.05 38.18 3.2969 2 2 0 1 29.48 18.60 3.0299 1 2 1 1 29.55 10.17 3.0225 0 2 1 1 29.57 10.03 3.0205 0 1 2 1 30.49 1.53 2.9323 0 -2 2 1 31.00 1.06 2.8848 1 0 2 1 31.11 2.50 2.8749 -2 -3 1 1 31.13 2.47 2.8729 2 1 1 1 31.48 35.92 2.8415 -1 1 2 1 32.05 36.83 2.7923 -2 -3 2 1 32.07 37.27 2.7911 2 0 1 1 32.25 7.85 2.7754 -1 2 0 1 32.29 7.66 2.7721 -1 -1 3 1 32.41 3.69 2.7627 -3 -2 1 1 32.83 6.30 2.7279 -3 -1 1 1 32.83 6.43 2.7277 -3 -2 2 1 33.27 8.46 2.6932 1 3 0 1 33.30 8.47 2.6905 1 1 2 1 33.30 2.64 2.6903 -2 1 0 1 33.33 2.68 2.6885 -2 -2 3 1 33.43 2.57 2.6801 -1 -3 2 1 33.46 2.46 2.6785 1 -1 2 1 33.64 9.78 2.6644 -2 1 1 1 33.66 9.67 2.6623 -2 -1 3 1 34.04 5.72 2.6337 1 -2 1 1 34.07 5.54 2.6317 -1 -2 3 1 34.26 2.93 2.6176 -3 -1 2 1 34.87 2.61 2.5731 2 3 0 1 34.88 2.53 2.5719 2 2 1 1 35.93 1.15 2.4995 -3 -3 2 1 35.94 1.27 2.4990 3 1 0 1 36.10 2.23 2.4879 0 -3 1 1 36.15 2.11 2.4849 0 -1 3 1 36.48 2.15 2.4627 -3 -3 1 1 36.49 2.34 2.4621 3 2 0 1 36.78 1.00 2.4436 0 3 0 1 37.62 2.94 2.3908 -3 0 1 1 37.64 2.95 2.3898 -3 -2 3 1 39.59 4.48 2.2765 0 -3 2 1 39.62 4.44 2.2750 0 -2 3 1 41.07 2.74 2.1979 3 3 0 1 42.24 5.16 2.1398 2 3 1 1 43.00 6.22 2.1035 -4 -2 2 1 43.20 4.78 2.0943 -2 2 0 1 43.24 4.84 2.0923 -2 -2 4 1 43.98 11.63 2.0587 -3 -4 1 1 44.00 10.50 2.0580 -1 -4 2 1 44.01 11.82 2.0576 3 2 1 1 44.04 10.37 2.0561 1 -1 3 1 44.36 1.79 2.0419 -1 3 0 1 44.42 1.84 2.0393 -1 -1 4 1 44.96 8.40 2.0161 1 -3 1 1 45.01 8.28 2.0140 -1 -2 4 1 45.08 3.35 2.0110 -3 -4 3 1 45.09 2.26 2.0109 2 4 0 1 45.09 3.48 2.0105 3 0 1 1 45.12 2.08 2.0094 2 2 2 1 45.45 21.95 1.9955 1 4 0 1 45.49 21.35 1.9938 -4 -3 1 1 45.51 21.87 1.9933 1 1 3 1 45.51 18.32 1.9929 -3 0 3 1 45.61 19.80 1.9891 -3 1 1 1 45.64 20.17 1.9877 -3 -2 4 1 45.77 10.46 1.9826 2 -2 1 1 45.78 6.82 1.9821 -4 -1 2 1 45.78 6.95 1.9818 -4 -2 3 1 45.79 10.33 1.9814 -2 -3 4 1 45.83 9.62 1.9801 -4 -1 1 1 45.83 9.61 1.9799 -4 -3 3 1 46.45 20.03 1.9548 0 -3 3 1 47.32 15.40 1.9209 -1 3 1 1 47.38 15.25 1.9188 -1 0 4 1 48.48 6.00 1.8777 0 -4 1 1 48.55 5.99 1.8753 0 -1 4 1 48.67 13.08 1.8707 1 3 2 1 48.72 4.22 1.8690 3 4 0 1 48.74 4.14 1.8685 3 3 1 1 48.79 3.32 1.8664 -2 2 2 1 48.83 3.31 1.8650 -2 0 4 1 49.17 3.09 1.8530 0 3 2 1 49.18 2.44 1.8527 -4 -1 3 1 49.19 3.13 1.8523 0 2 3 1 49.31 8.23 1.8481 -4 -4 3 1 49.32 8.26 1.8479 4 1 0 1 50.73 2.61 1.7995 3 -1 1 1 50.74 2.60 1.7993 -3 -4 4 1 50.89 5.29 1.7942 -1 2 3 1 51.55 6.85 1.7729 2 -2 2 1 51.56 6.85 1.7727 -2 -4 4 1 51.97 2.52 1.7594 -3 -5 2 1 52.02 2.44 1.7580 3 1 2 1 52.16 2.85 1.7535 -2 -5 2 1 52.22 2.97 1.7517 2 0 3 1 52.94 2.08 1.7294 -2 -5 1 1 53.01 2.06 1.7275 2 1 3 1 53.36 3.25 1.7171 -3 -5 3 1 53.38 1.80 1.7163 -1 3 2 1 53.39 3.16 1.7161 3 0 2 1 53.42 1.92 1.7151 -1 1 4 1 53.62 2.11 1.7093 4 0 0 1 53.62 2.08 1.7091 -4 -4 4 1 53.78 4.32 1.7044 -3 -5 1 1 53.83 4.32 1.7031 3 2 2 1 53.93 1.63 1.7002 -3 1 3 1 53.95 1.71 1.6997 -3 0 4 1 54.44 1.12 1.6854 -5 -3 2 1 54.56 3.85 1.6821 -2 -5 3 1 54.60 3.88 1.6809 2 -1 3 1 55.41 3.50 1.6583 -4 -5 2 1 55.44 3.50 1.6575 4 2 1 1 55.54 1.59 1.6545 -4 0 3 1 55.56 1.60 1.6542 -4 -1 4 1 55.70 1.02 1.6502 -1 -5 1 1 55.78 1.05 1.6481 1 0 4 1 55.95 2.16 1.6436 -1 -5 2 1 55.95 1.05 1.6434 1 -3 3 1 55.96 1.19 1.6433 -1 -4 4 1 56.01 2.16 1.6417 1 -1 4 1 56.14 1.84 1.6383 -2 2 3 1 56.16 1.79 1.6377 -2 1 4 1 56.25 5.97 1.6354 3 4 1 1 56.27 1.24 1.6350 -2 3 1 1 56.33 1.31 1.6332 -2 -1 5 1 56.50 4.60 1.6288 -5 -2 3 1 56.81 1.02 1.6206 2 5 0 1 56.84 1.12 1.6199 -5 -4 3 1 56.84 1.17 1.6198 -5 -2 1 1 57.16 5.17 1.6115 1 -4 1 1 57.24 5.02 1.6096 -1 -2 5 1 58.67 2.49 1.5735 -3 2 2 1 58.72 2.51 1.5723 -3 -1 5 1 59.09 1.75 1.5635 -4 -5 4 1 59.09 1.81 1.5633 4 0 1 1 59.80 1.37 1.5466 -5 -4 1 1 59.87 1.00 1.5450 -2 -5 4 1 60.64 3.67 1.5270 -4 1 0 1 60.67 3.60 1.5264 -4 -4 5 1 61.34 2.47 1.5112 0 4 2 1 61.39 2.48 1.5102 0 2 4 1 61.43 1.72 1.5092 -5 -5 3 1 61.45 1.68 1.5089 5 2 0 1 61.92 1.73 1.4987 -1 3 3 1 61.94 1.73 1.4982 -1 2 4 1 62.05 1.62 1.4956 -5 -5 2 1 62.07 1.66 1.4953 5 3 0 1 63.08 2.44 1.4738 -3 -6 2 1 63.14 2.44 1.4724 3 1 3 1 63.39 2.23 1.4672 2 5 1 1 63.44 2.18 1.4664 2 3 3 1 63.45 2.51 1.4662 0 5 0 1 63.54 2.46 1.4643 0 0 5 1 64.06 1.27 1.4536 1 5 1 1 64.12 1.30 1.4523 1 2 4 1 64.30 1.00 1.4487 -4 1 3 1 64.37 2.35 1.4474 -3 2 3 1 64.40 2.32 1.4466 -3 0 5 1 65.17 1.32 1.4314 -1 -5 4 1 65.20 1.30 1.4309 1 -3 4 1 65.22 4.76 1.4305 -5 0 2 1 65.25 4.72 1.4299 -5 -3 5 1 65.50 1.96 1.4251 -5 -5 1 1 65.51 1.96 1.4249 5 4 0 1 65.52 1.28 1.4247 -5 -1 4 1 65.54 2.39 1.4243 1 -4 3 1 65.57 2.39 1.4236 -1 -4 5 1 65.72 4.03 1.4207 -2 2 4 1 66.83 1.99 1.3999 0 -5 3 1 66.89 1.97 1.3988 0 -3 5 1 66.97 1.98 1.3973 -6 -4 3 1 66.97 1.94 1.3973 -6 -3 2 1 67.03 3.74 1.3962 -3 3 0 1 67.03 4.57 1.3962 -4 -6 4 1 67.06 4.51 1.3956 4 0 2 1 67.10 3.80 1.3949 -3 -3 6 1 67.55 1.65 1.3868 -3 3 1 1 67.62 1.67 1.3854 -3 -2 6 1 67.67 1.82 1.3846 -5 0 3 1 67.67 1.07 1.3845 2 -3 3 1 67.68 1.13 1.3844 -2 -5 5 1 67.69 1.86 1.3842 -5 -2 5 1 67.85 2.25 1.3813 -6 -4 2 1 68.83 1.82 1.3640 -6 -2 2 1 68.84 1.83 1.3639 -6 -4 4 1 69.49 1.48 1.3527 -2 4 1 1 69.50 2.96 1.3524 -1 -6 1 1 69.58 1.47 1.3511 -2 -1 6 1 69.61 2.97 1.3507 1 0 5 1 70.21 2.74 1.3406 3 6 0 1 70.27 2.73 1.3396 3 3 3 1 71.45 1.63 1.3204 -1 -6 3 1 71.53 1.72 1.3191 1 -2 5 1 71.55 1.53 1.3188 5 5 0 1 71.67 1.31 1.3168 2 -4 2 1 71.73 1.26 1.3158 -2 -4 6 1 72.75 1.39 1.2999 -5 0 4 1 72.77 1.36 1.2996 -5 -1 5 1 74.69 1.21 1.2709 -1 5 1 1 74.79 1.15 1.2694 -1 0 6 1 74.87 1.32 1.2683 0 5 2 1 74.94 1.33 1.2672 0 2 5 1 75.54 1.29 1.2586 -6 -6 3 1 75.56 1.27 1.2583 6 3 0 1 75.89 1.48 1.2537 3 1 4 1 76.04 1.15 1.2516 -5 1 0 1 76.07 1.12 1.2511 -5 -5 6 1 76.96 1.50 1.2389 -2 -6 5 1 76.99 1.47 1.2386 2 -3 4 1 78.06 1.92 1.2242 5 2 2 1 78.44 2.10 1.2192 3 -1 4 1 79.41 1.81 1.2068 -6 -6 5 1 79.41 1.83 1.2068 6 1 0 1 79.72 1.63 1.2029 4 -2 2 1 79.73 1.62 1.2027 -4 -6 6 1 79.97 2.50 1.1997 -4 1 5 1 81.23 2.43 1.1843 -2 4 3 1 81.30 2.39 1.1834 -2 1 6 1 82.18 1.02 1.1729 0 -5 5 1 82.21 2.11 1.1726 0 4 4 1 83.35 2.03 1.1594 2 5 3 1 83.77 1.12 1.1547 -6 -1 5 1 84.00 1.92 1.1521 5 4 2 1 84.19 1.30 1.1500 -2 5 1 1 84.52 1.46 1.1463 2 2 5 1 84.85 1.49 1.1427 -5 2 2 1 85.52 1.56 1.1355 1 -2 6 1 85.53 1.56 1.1354 3 -4 2 1 88.79 1.41 1.1019 -2 3 5 1 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.