H30 N6 O24 P6 Te Boudjada N, Boudjada A, Guitel J Acta Crystallographica C39 (1983) 656-658 Structure du Trimetaphosphate-Tellurate d'Ammonium, 2(N H4)3 P3 O9 * Te (O H)6 _cod_database_code 1008202 _database_code_amcsd 0016138 CELL PARAMETERS: 11.1600 11.1600 17.8600 90.000 90.000 120.000 SPACE GROUP: R-3 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1926.373 Density (g/cm3): 2.099 MAX. ABS. INTENSITY / VOLUME**2: 15.58347336 RIR: 2.418 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.41 25.52 8.5001 1 0 1 6 13.50 1.59 6.5589 0 1 2 6 14.88 92.69 5.9533 0 0 3 2 15.88 59.55 5.5800 1 1 0 6 19.03 4.27 4.6647 0 2 1 6 20.90 2.11 4.2500 2 0 2 6 21.83 58.41 4.0712 2 -1 3 6 21.83 41.59 4.0712 1 1 3 6 24.88 3.14 3.5789 2 1 1 6 24.88 42.25 3.5789 3 -1 1 6 26.36 2.93 3.3810 -1 3 2 6 26.36 56.34 3.3810 1 2 2 6 26.60 1.35 3.3505 0 1 5 6 27.19 3.24 3.2794 0 2 4 6 30.02 6.59 2.9767 0 0 6 2 31.14 2.37 2.8725 2 0 5 6 31.65 29.40 2.8273 3 -1 4 6 32.08 2.59 2.7900 2 2 0 6 33.81 4.83 2.6509 -1 4 1 6 34.14 1.85 2.6263 1 1 6 6 34.14 10.53 2.6263 2 -1 6 6 34.95 3.60 2.5674 3 1 2 6 34.95 9.00 2.5674 4 -1 2 6 35.14 7.80 2.5539 -1 3 5 6 36.42 1.35 2.4669 1 0 7 6 37.56 8.13 2.3944 4 0 1 6 38.60 1.32 2.3323 0 4 2 6 39.96 1.25 2.2563 0 2 7 6 41.02 11.01 2.2004 5 -2 1 6 41.29 1.04 2.1863 0 3 6 6 41.29 2.96 2.1863 3 0 6 6 41.99 3.22 2.1519 -2 5 2 6 42.15 6.63 2.1440 3 1 5 6 42.15 5.97 2.1440 4 -1 5 6 42.54 4.00 2.1250 4 0 4 6 42.88 8.22 2.1090 4 1 0 6 43.25 3.72 2.0917 2 1 7 6 45.31 3.26 2.0013 0 4 5 6 45.63 1.12 1.9880 4 1 3 6 45.68 11.47 1.9859 5 -2 4 6 47.74 1.92 1.9049 1 2 8 6 48.31 2.80 1.8838 -2 5 5 6 48.70 3.28 1.8697 1 1 9 6 48.70 3.04 1.8697 2 -1 9 6 49.31 1.39 1.8481 1 3 7 6 49.31 3.66 1.8481 -1 4 7 6 50.21 2.09 1.8170 2 4 1 6 51.04 5.20 1.7894 6 -2 2 6 52.13 4.91 1.7544 4 0 7 6 53.41 2.57 1.7155 3 1 8 6 53.93 1.27 1.7000 5 0 5 6 54.26 2.56 1.6905 -2 6 4 6 54.86 8.71 1.6736 5 -2 7 6 56.09 2.44 1.6397 0 4 8 6 56.60 1.17 1.6262 6 -2 5 6 56.91 2.66 1.6179 6 -1 4 6 57.19 2.55 1.6108 6 0 0 6 57.43 2.18 1.6045 3 -1 10 6 58.30 1.03 1.5826 4 3 1 6 58.69 1.09 1.5732 -2 5 8 6 58.69 1.31 1.5732 2 3 8 6 59.45 1.29 1.5549 0 6 3 6 59.45 3.64 1.5549 6 0 3 6 59.75 4.85 1.5476 5 2 0 6 61.95 4.50 1.4978 -2 7 3 6 61.95 3.11 1.4978 5 2 3 6 62.39 1.67 1.4883 0 0 12 2 62.49 1.69 1.4863 -1 4 10 6 62.61 1.21 1.4837 1 2 11 6 63.31 1.14 1.4689 1 6 1 6 64.83 1.41 1.4381 1 1 12 6 64.93 1.52 1.4362 4 0 10 6 65.94 1.33 1.4167 6 0 6 6 67.32 2.86 1.3909 5 -2 10 6 68.11 2.11 1.3766 3 5 1 6 68.31 1.36 1.3731 -2 7 6 6 68.80 1.48 1.3645 8 -3 2 6 69.72 1.01 1.3487 7 -3 7 6 69.79 1.42 1.3476 0 4 11 6 72.10 3.40 1.3100 2 3 11 6 73.54 1.30 1.2878 8 -3 5 6 74.06 3.92 1.2801 7 1 0 6 76.05 1.70 1.2515 -1 8 3 6 76.05 1.34 1.2515 7 1 3 6 76.11 1.45 1.2506 0 6 9 6 78.18 1.15 1.2226 -1 4 13 6 78.35 1.15 1.2204 -2 7 9 6 78.35 1.50 1.2204 5 2 9 6 78.82 1.34 1.2143 3 5 7 6 79.60 1.44 1.2044 1 2 14 6 80.41 1.37 1.1943 4 0 13 6 81.92 1.23 1.1760 -1 8 6 6 81.92 1.22 1.1760 7 1 6 6 82.07 1.08 1.1743 8 -3 8 6 82.91 1.03 1.1645 1 1 15 6 89.78 1.02 1.0923 3 5 10 6 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.