Onoratoite Menchetti S, Sabelli C, Trosti-Ferroni R Acta Crystallographica C40 (1984) 1506-1510 The structures of onoratoite, Sb8O11Cl2 and Sb8O11Cl2*6H2O Locality: synthetic Note: anisoB's from ICSD, corrected _database_code_amcsd 0009996 CELL PARAMETERS: 19.0470 4.0530 10.3180 90.000 110.250 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 747.292 Density (g/cm3): 5.393 MAX. ABS. INTENSITY / VOLUME**2: 80.95383573 RIR: 4.888 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.14 13.68 9.6803 0 0 1 2 9.90 2.61 8.9349 2 0 0 2 10.91 4.14 8.1126 -2 0 1 2 15.65 1.13 5.6613 2 0 1 2 17.56 6.74 5.0504 -2 0 2 2 18.33 4.54 4.8401 0 0 2 2 18.78 7.75 4.7261 -4 0 1 2 19.87 10.18 4.4674 4 0 0 2 21.91 6.95 4.0563 -4 0 2 2 22.49 3.01 3.9526 1 1 0 4 23.65 15.18 3.7615 -1 1 1 4 23.75 10.87 3.7471 2 0 2 2 24.67 1.46 3.6088 4 0 1 2 24.98 12.22 3.5650 1 1 1 4 25.91 6.66 3.4389 -2 0 3 2 26.40 4.92 3.3762 -3 1 1 4 27.65 8.46 3.2268 0 0 3 2 27.95 4.00 3.1923 -4 0 3 2 28.03 100.00 3.1832 -1 1 2 4 28.13 18.23 3.1718 -6 0 1 2 29.27 25.51 3.0514 -6 0 2 2 29.31 8.78 3.0466 -3 1 2 4 29.87 1.90 2.9916 3 1 1 4 30.27 1.54 2.9527 1 1 2 4 31.61 33.99 2.8306 4 0 2 2 32.25 5.02 2.7753 -5 1 1 4 32.60 5.79 2.7464 2 0 3 2 33.13 9.20 2.7042 -6 0 3 2 33.43 50.01 2.6806 5 1 0 4 34.43 6.93 2.6045 6 0 1 2 34.51 3.55 2.5990 -1 1 3 4 34.89 8.13 2.5712 -2 0 4 2 35.43 4.05 2.5338 3 1 2 4 35.55 7.32 2.5252 -4 0 4 2 37.05 2.72 2.4265 5 1 1 4 37.65 5.57 2.3892 -5 1 3 4 40.02 4.24 2.2531 -7 1 1 4 41.92 1.70 2.1552 2 0 4 2 42.51 1.06 2.1266 3 1 3 4 43.03 14.84 2.1020 -7 1 3 4 44.31 5.00 2.0442 -2 0 5 2 44.72 21.87 2.0265 0 2 0 2 45.42 10.05 1.9970 1 1 4 4 46.24 3.78 1.9632 -6 0 5 2 47.51 2.24 1.9138 -7 1 4 4 48.50 2.49 1.8771 -10 0 1 2 48.62 1.53 1.8726 -9 1 2 4 48.90 1.09 1.8625 -4 2 1 4 48.98 4.55 1.8597 -10 0 3 2 49.38 1.39 1.8455 4 2 0 4 49.53 4.24 1.8404 5 1 3 4 49.58 1.90 1.8386 -3 1 5 4 50.18 1.21 1.8181 -9 1 3 4 50.48 2.56 1.8080 -5 1 5 4 50.59 1.83 1.8044 8 0 2 2 50.59 1.86 1.8044 -8 0 5 2 50.65 7.40 1.8024 3 1 4 4 50.91 2.70 1.7938 -1 1 5 4 51.10 1.02 1.7873 7 1 2 4 51.11 3.39 1.7870 10 0 0 2 51.23 1.13 1.7831 9 1 0 4 51.25 2.08 1.7825 2 2 2 4 52.41 1.74 1.7459 -2 2 3 4 53.39 2.47 1.7161 0 2 3 4 53.51 5.97 1.7123 -7 1 5 4 53.56 1.11 1.7109 -4 2 3 4 53.67 4.72 1.7077 -6 2 1 4 54.34 2.81 1.6884 1 1 5 4 54.35 6.93 1.6881 -6 2 2 4 55.21 2.27 1.6638 9 1 1 4 55.42 1.19 1.6578 10 0 1 2 55.79 10.03 1.6478 4 2 2 4 56.43 1.71 1.6306 2 2 3 4 56.71 1.50 1.6232 6 0 4 2 56.77 2.81 1.6217 -6 2 3 4 57.09 3.41 1.6134 0 0 6 2 57.63 2.51 1.5994 6 2 1 4 57.76 1.15 1.5962 8 0 3 2 57.91 2.87 1.5923 7 1 3 4 57.92 1.76 1.5922 -11 1 2 4 57.94 2.90 1.5916 -2 2 4 4 58.39 2.66 1.5805 -4 2 4 4 58.60 2.03 1.5754 -12 0 3 2 58.62 4.81 1.5747 -5 1 6 4 58.66 2.76 1.5737 -11 1 3 4 58.88 4.23 1.5685 -11 1 1 4 59.44 1.30 1.5549 -12 0 1 2 59.62 1.98 1.5507 3 1 5 4 60.67 3.40 1.5263 9 1 2 4 61.08 1.55 1.5171 -11 1 4 4 64.78 2.45 1.4392 -2 2 5 4 65.06 3.64 1.4337 -11 1 5 4 65.65 2.57 1.4221 11 1 1 4 65.85 1.56 1.4183 7 1 4 4 66.01 1.49 1.4153 -8 0 7 2 66.03 1.00 1.4148 6 0 5 2 66.29 2.08 1.4100 -6 2 5 4 68.09 1.33 1.3771 -10 2 1 4 68.13 3.79 1.3763 -3 1 7 4 68.19 1.04 1.3752 -13 1 2 4 68.48 2.49 1.3702 -10 2 3 4 69.10 1.46 1.3594 -7 1 7 4 69.79 1.10 1.3476 8 2 2 4 69.79 1.05 1.3476 -8 2 5 4 70.22 2.00 1.3403 10 2 0 4 72.31 4.03 1.3067 -1 3 2 4 74.96 1.05 1.2669 6 2 4 4 75.18 3.05 1.2637 5 3 0 4 75.29 2.36 1.2622 0 2 6 4 76.39 1.76 1.2467 5 1 6 4 76.61 1.44 1.2438 -12 2 3 4 80.98 1.03 1.1873 -9 1 8 4 81.25 1.29 1.1840 -7 3 3 4 81.36 1.54 1.1826 -1 1 8 4 82.93 1.09 1.1642 1 3 4 4 83.27 1.25 1.1603 -8 2 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.