Np3F12H2O Cousson A, Gasperin M Acta Crystallographica C41 (1985) 804-805 Nouvelle description du tetrafluorure de neptunium hydrate, Np3F12H2O _cod_database_code 1001332 _database_code_amcsd 0010008 CELL PARAMETERS: 12.0230 11.7230 8.4350 90.000 128.770 90.000 SPACE GROUP: Cm X-RAY WAVELENGTH: 1.541838 Cell Volume: 926.926 Density (g/cm3): 6.842 MAX. ABS. INTENSITY / VOLUME**2: 88.21006135 RIR: 4.198 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.09 21.07 7.3212 1 1 0 2 12.97 52.63 6.8258 -1 1 1 2 13.46 1.37 6.5765 0 0 1 1 15.12 3.35 5.8615 0 2 0 2 18.93 10.33 4.6870 2 0 0 1 20.29 36.56 4.3757 0 2 1 2 21.16 89.02 4.1979 -2 0 2 1 21.23 91.47 4.1842 -2 2 1 2 22.15 75.33 4.0131 1 1 1 2 23.86 18.53 3.7300 -3 1 1 2 24.32 56.92 3.6606 2 2 0 2 24.68 100.00 3.6068 1 3 0 2 25.14 4.21 3.5427 -1 3 1 2 25.24 47.68 3.5291 -3 1 2 2 26.11 18.01 3.4129 -2 2 2 2 27.12 33.44 3.2882 0 0 2 1 29.53 15.69 3.0251 2 0 1 1 29.59 18.06 3.0192 3 1 0 2 30.50 1.32 2.9307 0 4 0 2 31.02 1.76 2.8831 1 3 1 2 31.19 4.22 2.8678 0 2 2 2 31.50 31.87 2.8404 -4 0 1 1 32.11 65.99 2.7872 -1 3 2 2 32.29 13.38 2.7726 -3 3 1 2 32.50 3.20 2.7553 -2 0 3 1 32.90 11.22 2.7221 -3 1 3 2 33.33 14.70 2.6882 2 2 1 2 33.35 4.55 2.6870 -3 3 2 2 33.47 4.63 2.6770 0 4 1 2 33.67 16.73 2.6617 -4 2 2 2 34.07 9.40 2.6312 -2 4 1 2 34.31 2.74 2.6136 -4 0 3 1 34.96 4.55 2.5669 1 1 2 2 36.02 1.98 2.4936 -2 2 3 2 36.15 3.76 2.4849 2 4 0 2 36.59 3.77 2.4559 -1 1 3 2 36.83 1.65 2.4404 3 3 0 2 37.42 1.01 2.4031 -2 4 2 2 37.68 4.86 2.3871 -4 2 3 2 39.61 1.60 2.2753 -3 3 3 2 39.62 7.76 2.2745 1 5 0 2 39.92 1.51 2.2582 -1 5 1 2 41.18 2.32 2.1922 0 0 3 1 41.72 1.62 2.1651 -5 1 1 2 42.32 4.43 2.1356 2 0 2 1 43.10 5.32 2.0990 -4 0 4 1 43.25 8.03 2.0921 -4 4 2 2 44.06 18.34 2.0553 1 5 1 2 44.11 20.33 2.0533 0 2 3 2 44.42 2.97 2.0397 -4 4 1 2 45.01 14.29 2.0141 -3 5 1 2 45.17 5.83 2.0075 -2 4 3 2 45.19 3.88 2.0065 2 2 2 2 45.53 39.36 1.9921 3 3 1 2 45.55 16.47 1.9916 -6 0 3 1 45.63 19.18 1.9883 -2 0 4 1 45.67 35.34 1.9867 -5 3 3 2 45.81 18.93 1.9806 -3 5 2 2 45.86 11.57 1.9787 -5 1 4 2 45.92 17.17 1.9761 -4 2 4 2 46.48 18.05 1.9538 0 6 0 2 47.37 27.49 1.9190 -5 3 1 2 48.55 10.22 1.8754 3 5 0 2 48.74 11.76 1.8684 4 0 1 1 48.83 5.92 1.8650 -6 2 2 2 48.85 7.15 1.8644 1 1 3 2 49.22 5.46 1.8513 5 1 0 2 49.24 1.91 1.8504 -6 0 4 1 49.42 14.54 1.8441 -3 3 4 2 50.80 4.80 1.7972 -3 5 3 2 50.92 4.48 1.7934 -6 0 1 1 51.16 1.72 1.7856 -5 3 4 2 51.60 12.56 1.7714 -2 6 2 2 51.81 1.04 1.7645 -6 2 4 2 52.10 4.19 1.7554 0 4 3 2 52.26 5.33 1.7503 1 5 2 2 53.06 3.54 1.7260 2 4 2 2 53.43 3.47 1.7149 -6 2 1 2 53.46 5.29 1.7139 -1 5 3 2 53.71 3.77 1.7065 -4 4 4 2 53.92 7.56 1.7003 1 3 3 2 53.97 3.04 1.6991 -7 1 3 2 54.59 1.02 1.6812 -4 0 5 1 54.64 6.76 1.6797 0 6 2 2 55.56 6.24 1.6540 -1 3 4 2 55.60 2.93 1.6529 -7 1 4 2 55.80 1.94 1.6475 3 5 1 2 55.88 1.03 1.6454 -2 4 4 2 55.99 1.89 1.6424 -1 7 1 2 56.03 3.91 1.6413 2 6 1 2 56.18 3.02 1.6374 -7 1 2 2 56.33 2.34 1.6334 -6 4 2 2 56.38 5.19 1.6319 2 0 3 1 56.61 3.99 1.6259 -6 0 5 1 56.93 1.60 1.6173 3 3 2 2 56.99 2.11 1.6160 -4 2 5 2 57.23 8.64 1.6098 -4 6 1 2 57.39 1.09 1.6055 -5 5 1 2 57.85 1.58 1.5938 -2 6 3 2 58.29 1.51 1.5830 0 2 4 2 58.73 4.57 1.5721 -7 3 3 2 59.03 1.81 1.5649 -4 6 3 2 59.20 2.93 1.5608 -3 5 4 2 59.27 1.45 1.5591 1 7 1 2 59.93 1.72 1.5434 -1 7 2 2 59.96 1.01 1.5428 -5 3 5 2 59.98 1.13 1.5423 -2 0 5 1 60.70 1.02 1.5258 -3 7 2 2 60.74 6.38 1.5249 -5 5 4 2 61.42 4.25 1.5096 6 2 0 2 61.60 2.84 1.5055 -3 3 5 2 61.96 2.86 1.4977 -7 1 1 2 62.24 2.84 1.4915 -2 2 5 2 62.97 1.57 1.4761 3 7 0 2 63.23 4.34 1.4707 1 5 3 2 63.52 3.89 1.4646 4 2 2 2 63.54 4.39 1.4642 5 5 0 2 63.83 1.48 1.4583 -4 4 5 2 64.17 2.40 1.4514 5 3 1 2 64.36 1.68 1.4475 -8 2 4 2 64.41 4.08 1.4464 -8 2 3 2 64.89 1.62 1.4371 -3 7 3 2 65.23 2.41 1.4303 0 8 1 2 65.33 8.36 1.4284 -7 3 5 2 65.60 4.18 1.4232 -2 8 1 2 65.60 1.14 1.4231 -8 0 5 1 65.70 3.60 1.4212 -1 1 5 2 65.75 3.45 1.4202 -8 0 2 1 66.90 3.50 1.3986 2 8 0 2 67.11 6.78 1.3947 -6 6 3 2 67.16 3.49 1.3939 -5 1 6 2 67.17 8.00 1.3936 -2 6 4 2 67.62 3.02 1.3854 -7 5 3 2 67.73 2.00 1.3835 -2 8 2 2 67.76 3.24 1.3829 -8 2 5 2 68.00 1.24 1.3787 6 4 0 2 68.05 2.07 1.3777 -4 0 6 1 68.14 1.81 1.3761 1 3 4 2 69.00 3.13 1.3611 -6 2 6 2 69.34 1.05 1.3553 -5 7 3 2 69.57 2.54 1.3513 -7 5 2 2 69.63 5.44 1.3503 4 6 1 2 69.98 1.19 1.3443 -1 3 5 2 70.18 1.09 1.3411 -4 2 6 2 70.38 4.80 1.3377 3 3 3 2 71.39 1.13 1.3212 -6 6 1 2 71.54 3.06 1.3188 2 8 1 2 71.74 2.31 1.3156 -4 8 2 2 71.76 1.33 1.3153 0 0 5 1 72.18 1.38 1.3088 6 2 1 2 72.44 1.59 1.3047 5 1 2 2 73.39 1.54 1.2902 1 9 0 2 73.49 1.08 1.2886 -7 3 6 2 73.84 1.58 1.2834 0 2 5 2 74.19 1.66 1.2782 -4 8 3 2 74.78 2.16 1.2695 -7 5 1 2 74.97 2.28 1.2668 7 3 0 2 75.25 1.35 1.2628 -6 4 6 2 75.78 2.27 1.2553 -3 3 6 2 75.98 2.64 1.2525 2 6 3 2 76.17 1.90 1.2498 -6 6 5 2 77.04 2.54 1.2378 -1 9 2 2 78.23 3.50 1.2219 -1 5 5 2 78.33 1.05 1.2207 6 4 1 2 78.51 3.64 1.2183 0 8 3 2 79.59 3.23 1.2044 -5 5 6 2 79.82 2.89 1.2015 -4 8 4 2 82.28 1.87 1.1717 8 0 0 1 83.49 1.86 1.1578 6 0 2 1 84.21 3.47 1.1497 1 3 5 2 84.60 2.52 1.1455 5 5 2 2 85.54 2.86 1.1353 3 9 1 2 85.63 1.38 1.1343 -5 -9 3 2 86.42 1.75 1.1259 -4 6 6 2 88.41 1.15 1.1057 -3 9 4 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.