Massicot Hill R J Acta Crystallographica C41 (1985) 1281-1284 Refinement of the structure of orthorhombic PbO (massicot) by Rietveld analysis of neutron powder diffraction data Locality: synthetic: Merck "pro analyse" (batch number 0093820) _database_code_amcsd 0010011 CELL PARAMETERS: 5.8931 5.4904 4.7528 90.000 90.000 90.000 SPACE GROUP: Pbcm X-RAY WAVELENGTH: 1.541838 Cell Volume: 153.779 Density (g/cm3): 9.639 MAX. ABS. INTENSITY / VOLUME**2: 679.2876635 RIR: 22.946 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 15.03 4.99 5.8931 1 0 0 2 22.13 1.36 4.0171 1 1 0 4 29.11 100.00 3.0680 1 1 1 8 30.33 24.52 2.9465 2 0 0 2 32.62 22.09 2.7452 0 2 0 2 37.86 16.21 2.3764 0 0 2 2 39.55 1.72 2.2785 2 1 1 8 45.14 15.26 2.0086 2 2 0 4 46.21 1.44 1.9644 3 0 0 2 49.26 11.99 1.8498 2 0 2 4 50.82 11.80 1.7967 0 2 2 4 53.14 18.09 1.7236 3 1 1 8 56.06 15.78 1.6404 1 3 1 8 57.71 1.15 1.5975 3 2 0 4 60.34 11.97 1.5340 2 2 2 8 61.22 1.11 1.5141 3 0 2 4 63.08 10.11 1.4738 1 1 3 8 63.10 1.85 1.4733 4 0 0 2 68.34 1.80 1.3726 0 4 0 2 68.88 1.88 1.3632 4 1 1 8 71.11 1.13 1.3258 3 2 2 8 72.86 2.45 1.2981 4 2 0 4 73.47 5.46 1.2889 3 3 1 8 76.00 2.03 1.2522 4 0 2 4 76.57 2.51 1.2442 2 4 0 4 79.69 4.72 1.2032 3 1 3 8 80.87 2.13 1.1886 0 4 2 4 80.90 1.38 1.1882 0 0 4 2 82.11 4.55 1.1738 1 3 3 8 85.17 3.08 1.1392 4 2 2 8 87.00 2.88 1.1199 5 1 1 8 88.76 3.32 1.1023 2 4 2 8 88.79 1.85 1.1020 2 0 4 4 89.98 1.92 1.0904 0 2 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.