Kanonerovite Lightfoot P, Cheetham A K Acta Crystallographica C43 (1987) 4-7 Structure of manganese(II) trisodium tripolyphosphate dodecahydrate Locaality: synthetic _database_code_amcsd 0020872 CELL PARAMETERS: 14.7630 9.3250 15.1400 90.000 89.870 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 2084.242 Density (g/cm3): 1.890 MAX. ABS. INTENSITY / VOLUME**2: 2.919521717 RIR: 0.503 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.36 81.61 10.5818 1 0 1 2 8.37 64.85 10.5578 -1 0 1 2 11.14 30.13 7.9398 0 1 1 4 11.22 1.01 7.8839 1 1 0 4 11.99 81.88 7.3815 2 0 0 2 12.65 100.00 6.9961 1 1 1 4 12.67 43.54 6.9892 -1 1 1 4 15.07 46.35 5.8772 0 1 2 4 15.31 1.82 5.7877 2 1 0 4 16.22 13.67 5.4637 1 1 2 4 16.24 1.97 5.4571 -1 1 2 4 16.39 5.25 5.4093 2 1 1 4 16.41 11.64 5.4029 -2 1 1 4 18.57 10.36 4.7787 1 0 3 2 18.59 16.64 4.7720 -1 0 3 2 18.95 2.22 4.6831 3 0 1 2 18.98 3.65 4.6769 -3 0 1 2 19.03 12.16 4.6625 0 2 0 2 19.29 9.28 4.6018 2 1 2 4 19.32 9.21 4.5939 -2 1 2 4 19.93 3.33 4.4560 0 2 1 4 19.97 28.10 4.4460 1 2 0 4 20.01 9.69 4.4384 0 1 3 4 20.83 5.45 4.2651 -1 2 1 4 21.23 4.37 4.1850 3 1 1 4 21.25 8.46 4.1805 -3 1 1 4 22.39 42.50 3.9699 0 2 2 4 22.56 2.14 3.9420 2 2 0 4 23.19 2.78 3.8349 1 2 2 4 23.21 5.78 3.8326 -1 2 2 4 23.31 5.12 3.8159 2 2 1 4 23.33 1.16 3.8137 -2 2 1 4 23.37 1.87 3.8071 2 1 3 4 23.41 2.64 3.8004 -2 1 3 4 23.50 1.60 3.7850 0 0 4 2 23.56 17.03 3.7763 3 1 2 4 23.60 6.44 3.7698 -3 1 2 4 25.25 13.60 3.5273 3 0 3 2 25.31 31.03 3.5193 -3 0 3 2 25.40 7.13 3.5071 0 1 4 4 25.46 11.48 3.4981 2 2 2 4 26.02 20.52 3.4247 0 2 3 4 26.10 12.17 3.4138 1 1 4 4 26.13 5.32 3.4105 -1 1 4 4 26.33 11.85 3.3846 3 2 0 4 26.44 4.83 3.3711 2 0 4 2 26.49 1.28 3.3649 -2 0 4 2 26.62 11.64 3.3483 4 1 1 4 26.65 48.94 3.3453 -4 1 1 4 26.73 21.16 3.3349 -1 2 3 4 26.85 2.48 3.3204 4 0 2 2 26.99 18.50 3.3041 3 2 1 4 27.00 11.35 3.3020 -3 2 1 4 27.03 12.67 3.2991 3 1 3 4 27.08 1.14 3.2926 -3 1 3 4 28.15 21.02 3.1703 2 1 4 4 28.19 14.89 3.1652 -2 1 4 4 28.54 13.56 3.1280 4 1 2 4 28.58 13.45 3.1231 -4 1 2 4 29.33 3.73 3.0448 0 3 1 4 29.36 1.09 3.0416 1 3 0 4 30.42 3.63 2.9386 0 2 4 4 30.90 31.24 2.8938 4 2 0 4 31.02 7.12 2.8830 1 2 4 4 31.04 3.04 2.8811 -1 2 4 4 31.05 5.27 2.8800 0 1 5 4 31.10 14.49 2.8754 0 3 2 4 31.46 19.68 2.8433 4 2 1 4 31.48 4.67 2.8414 -4 2 1 4 31.49 7.15 2.8406 4 1 3 4 31.56 2.90 2.8350 -4 1 3 4 31.70 1.63 2.8228 1 3 2 4 31.71 1.86 2.8219 -1 3 2 4 31.79 2.89 2.8152 2 3 1 4 31.79 1.95 2.8149 5 1 0 4 32.34 3.99 2.7685 5 1 1 4 32.82 2.80 2.7286 -2 2 4 4 33.12 1.64 2.7047 4 2 2 4 33.16 10.91 2.7015 -4 2 2 4 33.37 10.78 2.6849 2 1 5 4 33.42 13.13 2.6810 -2 1 5 4 33.43 4.29 2.6801 2 3 2 4 33.45 4.13 2.6785 -2 3 2 4 33.87 8.56 2.6466 0 3 3 4 33.95 2.41 2.6402 5 1 2 4 33.96 1.68 2.6394 -4 0 4 2 34.12 3.54 2.6280 3 3 0 4 34.42 3.38 2.6056 1 3 3 4 34.43 1.95 2.6045 -1 3 3 4 34.64 3.08 2.5898 3 3 1 4 34.65 17.59 2.5887 -3 3 1 4 35.27 8.08 2.5450 4 1 4 4 35.34 6.28 2.5397 -4 1 4 4 35.55 3.34 2.5249 3 2 4 4 35.58 5.25 2.5233 0 0 6 2 35.80 2.01 2.5085 -4 2 3 4 35.87 3.20 2.5035 1 2 5 4 36.00 3.50 2.4945 5 2 0 4 36.10 5.21 2.4879 3 1 5 4 36.17 5.15 2.4836 3 3 2 4 36.17 12.37 2.4832 -3 1 5 4 36.20 1.53 2.4817 -3 3 2 4 36.49 7.47 2.4621 5 2 1 4 36.52 3.84 2.4605 6 0 0 2 37.41 2.69 2.4041 1 1 6 4 37.43 2.79 2.4027 2 2 5 4 37.43 1.24 2.4024 -1 1 6 4 37.47 4.89 2.3999 -2 2 5 4 37.65 17.88 2.3893 2 0 6 2 37.70 11.51 2.3860 -2 0 6 2 38.31 2.50 2.3492 4 3 1 4 38.33 1.58 2.3482 -4 3 1 4 38.62 5.07 2.3312 0 4 0 2 38.96 1.46 2.3115 -2 1 6 4 39.12 1.52 2.3027 1 4 0 4 39.15 3.31 2.3009 4 2 4 4 39.43 1.76 2.2852 2 3 4 4 39.47 1.70 2.2833 -2 3 4 4 39.65 1.27 2.2729 4 1 5 4 39.72 1.21 2.2692 4 3 2 4 39.74 1.21 2.2682 -6 1 2 4 39.74 2.82 2.2681 -4 1 5 4 39.87 2.50 2.2611 5 1 4 4 39.92 4.80 2.2584 3 2 5 4 39.96 2.43 2.2564 -5 1 4 4 40.30 3.83 2.2379 5 2 3 4 40.66 2.43 2.2192 0 2 6 4 40.96 4.15 2.2033 1 4 2 4 41.03 2.16 2.1997 2 4 1 4 41.04 7.89 2.1992 -2 4 1 4 41.12 2.84 2.1952 1 2 6 4 41.15 4.14 2.1939 -1 2 6 4 41.50 1.70 2.1761 6 2 0 4 41.82 1.57 2.1599 3 3 4 4 41.95 1.26 2.1538 6 1 3 4 41.98 5.83 2.1520 4 3 3 4 42.02 1.81 2.1501 -6 1 3 4 42.03 8.17 2.1496 -4 3 3 4 42.24 1.49 2.1393 -1 0 7 2 42.51 1.03 2.1264 2 2 6 4 42.56 4.73 2.1240 -2 2 6 4 42.65 7.33 2.1201 5 3 1 4 42.67 4.19 2.1192 -5 3 1 4 42.83 2.39 2.1116 -5 0 5 2 42.93 2.92 2.1068 3 4 0 4 43.18 7.09 2.0952 1 4 3 4 43.19 3.82 2.0947 -1 4 3 4 43.28 2.24 2.0903 -6 2 2 4 43.30 1.27 2.0895 7 0 1 2 43.33 2.45 2.0882 -7 0 1 2 43.36 1.04 2.0870 3 4 1 4 43.37 2.37 2.0864 1 1 7 4 43.37 1.50 2.0864 -3 4 1 4 43.93 2.34 2.0608 5 3 2 4 43.94 1.83 2.0608 -6 0 4 2 43.97 7.45 2.0591 -5 3 2 4 44.52 5.11 2.0349 2 4 3 4 44.63 1.98 2.0302 3 4 2 4 44.96 1.05 2.0162 6 1 4 4 45.00 1.07 2.0146 4 3 4 4 45.42 1.88 1.9968 -6 2 3 4 45.79 7.91 1.9817 3 0 7 2 45.87 2.53 1.9784 -3 0 7 2 46.15 1.17 1.9669 -1 4 4 4 46.27 1.46 1.9620 0 2 7 4 46.47 3.91 1.9542 -4 4 1 4 46.64 1.26 1.9475 7 0 3 2 46.69 3.46 1.9454 1 2 7 4 46.72 1.75 1.9443 -7 0 3 2 46.87 4.37 1.9384 3 1 7 4 46.95 2.73 1.9353 -3 1 7 4 47.26 4.48 1.9235 -5 2 5 4 47.31 1.50 1.9216 7 2 0 4 47.70 2.83 1.9068 7 2 1 4 47.71 2.15 1.9064 7 1 3 4 47.78 2.67 1.9035 4 2 6 4 47.78 1.30 1.9034 -7 1 3 4 47.87 1.66 1.9002 -4 2 6 4 48.07 1.16 1.8927 -2 3 6 4 48.08 2.13 1.8925 0 0 8 2 48.28 1.99 1.8849 -6 2 4 4 48.39 1.01 1.8809 5 1 6 4 48.50 2.55 1.8769 -5 1 6 4 48.62 3.24 1.8727 6 1 5 4 48.66 1.32 1.8713 4 3 5 4 48.69 3.39 1.8703 6 3 2 4 48.73 1.22 1.8687 -6 1 5 4 48.73 1.67 1.8687 -6 3 2 4 48.84 1.05 1.8647 5 3 4 4 48.92 3.74 1.8620 -5 3 4 4 49.39 13.98 1.8454 8 0 0 2 49.52 1.75 1.8407 1 1 8 4 49.55 2.12 1.8397 -1 1 8 4 49.64 1.11 1.8367 4 4 3 4 49.64 1.94 1.8366 -1 5 1 4 49.75 2.06 1.8326 -1 4 5 4 49.84 1.10 1.8297 5 4 0 4 50.01 2.10 1.8238 3 2 7 4 50.24 3.66 1.8162 -5 4 1 4 50.39 3.31 1.8109 0 5 2 4 50.55 1.63 1.8057 -7 1 4 4 50.62 3.00 1.8031 6 3 3 4 50.78 2.90 1.7979 8 1 1 4 50.81 1.24 1.7970 7 2 3 4 51.86 1.45 1.7630 1 3 7 4 52.69 1.33 1.7371 -1 5 3 4 52.80 1.48 1.7339 4 2 7 4 52.83 1.49 1.7329 6 1 6 4 52.84 3.53 1.7327 3 5 1 4 52.85 1.89 1.7323 -3 5 1 4 52.95 1.25 1.7291 -4 3 6 4 53.34 1.47 1.7176 -6 3 4 4 53.53 1.04 1.7120 -7 2 4 4 53.75 3.07 1.7053 -2 2 8 4 53.76 1.28 1.7052 8 1 3 4 53.94 2.87 1.6999 -7 3 2 4 53.94 1.42 1.6997 3 5 2 4 54.20 1.78 1.6923 6 4 0 4 54.56 2.57 1.6821 6 4 1 4 54.58 3.11 1.6815 -6 4 1 4 54.89 1.03 1.6727 -8 2 2 4 54.95 2.28 1.6710 -1 0 9 2 55.55 1.16 1.6544 -4 5 1 4 55.61 1.31 1.6528 4 4 5 4 55.72 5.59 1.6496 6 2 6 4 55.79 1.71 1.6479 -3 5 3 4 55.84 2.89 1.6463 -6 2 6 4 55.87 1.03 1.6456 1 1 9 4 56.24 1.17 1.6357 5 2 7 4 56.36 1.59 1.6326 -5 2 7 4 56.41 1.01 1.6311 -5 3 6 4 56.97 1.27 1.6164 -3 4 6 4 58.09 1.91 1.5880 0 5 5 4 58.18 1.53 1.5856 0 4 7 4 58.89 1.30 1.5681 -5 5 1 4 59.62 1.18 1.5507 2 4 7 4 59.76 3.65 1.5474 9 2 0 4 60.23 1.41 1.5366 3 3 8 4 60.30 1.04 1.5348 -3 3 8 4 60.34 1.37 1.5339 6 3 6 4 60.50 2.64 1.5303 7 2 6 4 60.63 1.27 1.5272 -7 2 6 4 61.20 2.70 1.5145 1 6 2 4 61.21 1.48 1.5143 -1 6 2 4 61.22 2.55 1.5140 0 0 10 2 61.25 2.05 1.5133 2 6 1 4 61.26 1.57 1.5131 -2 6 1 4 61.32 1.00 1.5118 3 5 5 4 61.37 1.73 1.5107 -3 5 5 4 61.40 1.22 1.5099 3 4 7 4 61.47 1.12 1.5084 -3 4 7 4 61.52 1.66 1.5073 3 2 9 4 62.17 1.64 1.4932 -7 4 3 4 62.66 1.39 1.4826 6 1 8 4 62.81 1.08 1.4795 -6 1 8 4 63.29 1.04 1.4693 0 4 8 4 63.63 1.17 1.4623 1 4 8 4 63.66 1.29 1.4618 -1 4 8 4 63.84 2.44 1.4581 -6 5 2 4 63.94 1.57 1.4559 -4 4 7 4 64.84 1.18 1.4380 7 2 7 4 64.99 1.44 1.4350 -7 2 7 4 65.27 1.02 1.4294 6 2 8 4 65.45 1.41 1.4261 4 6 1 4 66.44 1.25 1.4072 -3 4 8 4 69.08 1.62 1.3596 -10 1 4 4 69.83 1.06 1.3470 7 5 3 4 70.74 1.34 1.3318 -6 4 7 4 71.26 1.25 1.3233 0 6 6 4 71.47 1.16 1.3200 0 2 11 4 71.58 1.06 1.3182 1 6 6 4 72.38 1.63 1.3055 -9 0 7 2 74.37 2.13 1.2755 10 0 6 2 74.82 1.15 1.2690 6 3 9 4 75.30 2.37 1.2621 0 6 7 4 83.12 1.30 1.1620 1 8 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.