O13 P4 Pb3 Averbuch-Pouchot M, Durif A Acta Crystallographica C43 (1987) 631-632 Structure of lead tetrapolyphosphate. _cod_database_code 1007160 _database_code_amcsd 0010036 CELL PARAMETERS: 7.8300 7.3470 10.2150 104.350 101.810 94.270 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 552.376 Density (g/cm3): 5.732 MAX. ABS. INTENSITY / VOLUME**2: 54.48367360 RIR: 3.095 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.65 47.33 7.5972 1 0 0 2 13.41 10.99 6.6024 0 -1 1 2 17.47 1.20 5.0761 0 1 1 2 17.49 31.10 5.0717 -1 -1 1 2 18.11 1.45 4.8997 1 -1 1 2 18.43 14.16 4.8144 0 0 2 2 18.80 47.64 4.7195 -1 1 1 2 19.32 1.58 4.5949 0 -1 2 2 19.42 19.90 4.5719 -1 0 2 2 23.09 13.02 3.8526 1 1 1 2 23.42 9.10 3.7986 2 0 0 2 23.94 5.69 3.7167 1 -1 2 2 24.06 55.29 3.6987 1 0 2 2 25.25 82.65 3.5277 0 2 0 2 26.08 69.73 3.4173 -2 1 1 2 26.32 3.71 3.3866 -2 0 2 2 26.41 2.27 3.3743 -1 2 0 2 26.66 42.13 3.3433 -2 -1 1 2 27.01 15.15 3.3012 0 -2 2 2 27.15 1.61 3.2841 2 0 1 2 27.25 8.13 3.2728 0 -1 3 2 27.49 60.82 3.2441 2 -1 1 2 27.56 6.22 3.2367 -1 0 3 2 27.74 100.00 3.2163 -1 -1 3 2 27.80 2.53 3.2096 0 0 3 2 29.29 48.96 3.0495 1 2 0 2 29.88 45.77 2.9899 1 -2 2 2 30.17 1.37 2.9620 1 1 2 2 31.59 3.51 2.8318 1 -1 3 2 32.27 4.51 2.7740 -2 2 0 2 32.35 21.16 2.7672 2 1 1 2 32.84 32.26 2.7275 -1 1 3 2 32.86 2.23 2.7254 -2 -1 3 2 33.22 1.93 2.6968 2 -2 1 2 33.25 17.02 2.6948 2 0 2 2 33.29 4.69 2.6914 -1 -2 3 2 33.65 33.02 2.6634 0 1 3 2 34.75 1.77 2.5813 -1 2 2 2 35.40 1.80 2.5359 -2 -2 2 2 35.45 2.54 2.5324 3 0 0 2 36.06 30.02 2.4907 -3 0 2 2 36.46 1.98 2.4645 -1 0 4 2 36.82 3.77 2.4414 0 -3 1 2 37.36 1.71 2.4072 0 0 4 2 37.60 1.08 2.3925 -3 -1 1 2 37.81 4.97 2.3793 1 -3 1 2 38.14 6.54 2.3598 -2 2 2 2 38.42 2.81 2.3430 1 1 3 2 38.52 17.02 2.3374 3 -1 1 2 38.57 1.21 2.3344 2 1 2 2 38.80 1.53 2.3208 3 0 1 2 39.22 2.91 2.2968 -2 -1 4 2 39.42 19.41 2.2860 -2 0 4 2 39.42 1.00 2.2859 -1 -2 4 2 39.43 2.54 2.2851 1 -3 2 2 39.81 15.01 2.2643 1 2 2 2 40.19 1.33 2.2440 1 -1 4 2 41.04 6.34 2.1994 -3 2 0 2 41.54 19.28 2.1738 -1 3 1 2 41.90 1.84 2.1559 1 0 4 2 41.93 4.68 2.1547 0 3 1 2 42.36 22.11 2.1339 -1 -3 3 2 42.41 17.65 2.1312 2 -3 1 2 42.46 1.02 2.1291 3 -2 1 2 42.62 11.26 2.1215 1 -2 4 2 42.90 2.70 2.1080 0 2 3 2 42.93 1.63 2.1068 -3 1 3 2 43.19 6.33 2.0945 -2 -2 4 2 43.19 2.48 2.0945 1 -3 3 2 43.24 20.06 2.0922 3 1 1 2 44.08 2.09 2.0543 3 0 2 2 44.32 11.60 2.0440 -3 -2 2 2 44.45 1.00 2.0381 -1 -1 5 2 44.62 9.35 2.0307 -2 3 1 2 44.74 11.74 2.0256 -3 2 2 2 45.35 11.34 1.9997 0 -1 5 2 45.61 9.31 1.9891 -3 0 4 2 45.71 1.95 1.9850 1 3 1 2 45.73 12.54 1.9842 -2 -3 1 2 45.92 1.55 1.9763 3 -2 2 2 46.11 1.13 1.9687 2 1 3 2 46.84 1.15 1.9395 3 2 0 2 46.86 1.71 1.9386 -2 -1 5 2 46.99 9.99 1.9337 -2 -3 3 2 47.18 8.39 1.9263 2 2 2 2 47.20 2.62 1.9258 0 0 5 2 47.21 8.60 1.9251 -4 0 2 2 47.29 3.84 1.9222 0 -2 5 2 47.31 3.30 1.9213 2 -1 4 2 47.89 11.65 1.8993 4 0 0 2 48.69 3.15 1.8700 1 -3 4 2 49.02 7.01 1.8583 2 -2 4 2 49.18 7.52 1.8527 3 -1 3 2 49.27 7.83 1.8493 2 0 4 2 49.42 6.90 1.8442 1 -1 5 2 49.80 2.40 1.8309 3 -3 1 2 49.83 2.41 1.8299 -1 2 4 2 49.88 8.60 1.8283 -3 -2 4 2 50.05 7.63 1.8225 0 -4 2 2 50.67 1.41 1.8017 -3 3 1 2 50.81 1.05 1.7969 1 -2 5 2 50.82 1.33 1.7965 3 0 3 2 50.95 6.73 1.7922 1 -4 2 2 51.10 1.70 1.7873 3 -2 3 2 51.32 7.80 1.7803 -2 2 4 2 51.55 12.90 1.7729 -4 2 0 2 51.58 2.58 1.7718 1 0 5 2 51.63 1.01 1.7704 -1 4 0 2 51.83 2.19 1.7639 0 4 0 2 51.94 3.46 1.7603 -4 1 3 2 52.52 3.58 1.7423 0 1 5 2 52.70 8.92 1.7370 0 -3 5 2 52.74 1.18 1.7356 -1 -3 5 2 52.82 1.14 1.7332 -1 3 3 2 53.86 1.48 1.7022 -1 -1 6 2 54.14 1.10 1.6941 2 -3 4 2 54.19 3.49 1.6925 -3 -3 1 2 54.21 12.15 1.6920 0 3 3 2 54.37 1.58 1.6875 -2 3 3 2 54.61 1.87 1.6806 2 1 4 2 54.93 8.47 1.6716 -4 -2 2 2 54.97 9.54 1.6703 1 4 0 2 55.33 1.24 1.6604 -1 -2 6 2 55.45 2.27 1.6571 -2 -1 6 2 55.68 1.74 1.6507 -3 2 4 2 55.69 1.20 1.6506 0 -4 4 2 55.74 5.84 1.6490 -1 0 6 2 56.15 1.02 1.6381 2 -1 5 2 56.33 6.29 1.6332 3 -3 3 2 56.41 3.48 1.6311 -3 1 5 2 56.90 3.17 1.6183 -2 0 6 2 57.01 5.84 1.6154 1 1 5 2 57.29 6.66 1.6082 -2 -2 6 2 57.55 4.43 1.6014 1 -4 4 2 58.12 1.07 1.5872 4 2 0 2 59.81 6.18 1.5463 -3 4 0 2 60.00 4.74 1.5418 -4 -1 5 2 60.47 3.30 1.5310 4 -1 3 2 60.77 1.92 1.5241 -1 1 6 2 60.92 2.26 1.5208 0 -4 5 2 60.94 4.88 1.5203 -2 4 2 2 60.98 3.00 1.5194 5 0 0 2 61.09 5.03 1.5169 3 3 1 2 62.09 1.15 1.4950 2 -4 4 2 62.23 1.76 1.4918 -2 -3 6 2 62.29 1.08 1.4906 4 0 3 2 62.65 7.72 1.4829 -5 1 3 2 62.74 4.32 1.4810 2 2 4 2 62.78 5.97 1.4802 -5 -1 3 2 63.10 3.99 1.4734 -4 1 5 2 63.99 3.56 1.4550 1 -5 1 2 64.34 1.04 1.4480 3 -4 3 2 64.39 1.53 1.4469 1 4 2 2 65.09 2.27 1.4330 -3 4 2 2 65.44 5.33 1.4262 -4 3 3 2 65.98 1.94 1.4159 2 -2 6 2 66.31 1.12 1.4096 -1 -5 3 2 66.51 1.41 1.4058 2 -5 1 2 66.53 1.96 1.4054 -3 -4 4 2 67.08 6.34 1.3953 4 1 3 2 67.53 3.13 1.3870 -4 4 0 2 68.15 1.55 1.3760 5 1 1 2 68.37 2.23 1.3721 -3 -1 7 2 68.54 5.33 1.3692 -1 2 6 2 68.88 2.73 1.3631 2 -5 3 2 68.93 3.04 1.3624 5 -2 2 2 68.95 4.26 1.3620 -1 5 1 2 69.12 3.43 1.3590 -4 -3 5 2 69.14 1.69 1.3586 2 -3 6 2 69.21 1.01 1.3575 0 -3 7 2 69.24 1.26 1.3570 -5 3 1 2 69.70 1.36 1.3491 1 -2 7 2 69.72 1.35 1.3488 1 -1 7 2 69.74 1.19 1.3484 -5 -1 5 2 69.88 1.09 1.3461 -3 0 7 2 69.90 2.90 1.3457 -2 -4 6 2 69.94 1.01 1.3451 0 5 1 2 70.53 3.74 1.3352 -2 -5 3 2 70.61 2.63 1.3339 2 4 2 2 70.67 4.00 1.3330 5 2 0 2 71.44 2.06 1.3205 0 -5 5 2 71.69 1.08 1.3165 4 3 1 2 71.85 1.45 1.3139 -2 -5 1 2 72.18 1.76 1.3087 -1 -5 5 2 72.36 3.16 1.3059 -3 3 5 2 72.62 1.37 1.3018 1 0 7 2 72.98 1.85 1.2963 -6 1 1 2 73.36 2.32 1.2906 -2 4 4 2 73.80 3.77 1.2840 -4 -4 2 2 74.07 1.19 1.2800 -3 -3 7 2 74.23 1.64 1.2775 -3 1 7 2 74.29 1.72 1.2767 3 -2 6 2 74.31 1.97 1.2764 -5 3 3 2 74.44 1.42 1.2745 3 -1 6 2 74.69 2.48 1.2709 3 -5 3 2 74.77 1.02 1.2696 -1 -2 8 2 75.10 2.17 1.2650 2 -4 6 2 75.66 1.06 1.2569 -6 -1 3 2 75.67 1.21 1.2568 1 3 5 2 76.04 1.62 1.2516 -6 -1 1 2 76.42 1.51 1.2464 0 -2 8 2 76.64 1.66 1.2433 0 -1 8 2 76.96 1.07 1.2389 3 -3 6 2 77.21 1.16 1.2356 6 -1 1 2 77.41 2.40 1.2329 3 0 6 2 77.64 1.09 1.2297 -4 3 5 2 77.71 1.58 1.2288 -1 -3 8 2 78.29 1.12 1.2212 1 1 7 2 78.33 3.38 1.2207 0 -6 2 2 78.66 1.11 1.2164 4 -3 5 2 78.99 1.56 1.2121 -5 -3 5 2 79.24 1.60 1.2090 -3 -5 1 2 79.66 1.21 1.2036 0 0 8 2 80.25 1.62 1.1962 5 -4 2 2 80.48 1.16 1.1934 -4 -3 7 2 81.20 1.44 1.1846 -6 3 1 2 81.59 1.91 1.1799 0 5 3 2 83.13 1.86 1.1619 6 -3 1 2 83.27 1.32 1.1604 6 0 2 2 83.38 1.25 1.1591 -1 -4 8 2 83.65 1.06 1.1560 2 -5 6 2 84.34 1.79 1.1483 -5 2 6 2 84.55 1.68 1.1460 4 3 3 2 84.83 1.18 1.1430 -4 0 8 2 85.14 1.67 1.1396 1 6 0 2 85.40 1.10 1.1368 0 1 8 2 85.77 1.68 1.1329 1 5 3 2 86.14 1.75 1.1289 -6 0 6 2 86.54 2.78 1.1248 -3 6 0 2 87.28 1.19 1.1170 3 5 1 2 87.54 1.79 1.1144 -6 -3 3 2 88.63 2.06 1.1035 -4 5 3 2 89.16 1.73 1.0983 -6 -2 6 2 89.31 1.63 1.0969 -5 5 1 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.