H6 K3 Na3 O24 P6 Te Averbuch-Pouchot M, Durif A Acta Crystallographica C43 (1987) 1653-1655 Crystal structure of a new adduct between telluric acid and alkali cyclo-triphosphates: Te (O H)6 * Na3 P3 O9 * K3 P3 O9 _cod_database_code 1007168 _database_code_amcsd 0010049 CELL PARAMETERS: 18.4200 10.6440 12.3480 90.000 119.760 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2101.682 Density (g/cm3): 2.812 MAX. ABS. INTENSITY / VOLUME**2: 12.12280828 RIR: 1.404 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.07 4.41 7.9953 2 0 0 2 11.07 8.91 7.9940 -1 1 1 4 14.62 2.54 6.0599 1 1 1 4 14.63 1.25 6.0536 -2 0 2 2 16.54 60.12 5.3597 0 0 2 2 16.66 22.19 5.3220 0 2 0 2 16.67 44.08 5.3185 -3 1 1 4 18.62 1.00 4.7660 3 1 0 4 20.04 6.74 4.4303 2 2 0 4 20.06 3.35 4.4258 -4 0 2 2 22.24 8.72 3.9977 4 0 0 2 22.24 17.40 3.9970 -2 2 2 4 23.56 50.13 3.7769 3 1 1 4 23.56 49.87 3.7765 0 2 2 4 23.58 49.99 3.7736 -3 1 3 4 24.15 5.54 3.6855 2 0 2 2 24.16 10.99 3.6839 -1 1 3 4 25.72 2.45 3.4638 1 3 0 4 25.73 2.47 3.4624 -4 2 1 4 25.74 2.46 3.4608 -5 1 2 4 26.17 21.39 3.4048 -1 3 1 4 26.19 21.35 3.4032 -5 1 1 4 26.19 21.35 3.4029 -4 2 2 4 27.91 11.36 3.1969 1 3 1 4 27.91 11.38 3.1963 4 2 0 4 27.94 11.35 3.1936 -5 1 3 4 29.07 2.53 3.0720 -3 3 1 4 29.09 1.28 3.0700 -6 0 2 2 29.15 13.05 3.0631 -1 3 2 4 29.16 13.04 3.0629 5 1 0 4 29.17 12.91 3.0613 -4 2 3 4 29.41 2.38 3.0368 1 1 3 4 29.43 1.17 3.0351 -2 0 4 2 29.48 12.24 3.0299 2 2 2 4 29.51 6.14 3.0268 -4 0 4 2 30.12 4.57 2.9672 3 1 2 4 30.12 4.55 2.9666 0 2 3 4 30.14 4.56 2.9648 -3 1 4 4 32.24 10.35 2.7762 1 3 2 4 32.24 10.39 2.7762 4 2 1 4 32.28 10.35 2.7734 -5 1 4 4 33.44 5.02 2.6799 0 0 4 2 33.63 1.59 2.6647 -3 3 3 4 33.68 4.53 2.6610 0 4 0 2 33.70 8.92 2.6593 -6 2 2 4 34.05 1.07 2.6329 5 1 1 4 34.06 1.07 2.6325 -1 3 3 4 34.08 1.08 2.6311 -4 2 4 4 35.22 4.54 2.5483 -2 4 1 4 35.23 4.57 2.5474 -5 3 2 4 35.24 4.54 2.5467 -7 1 2 4 35.56 11.91 2.5248 2 4 0 4 35.57 11.91 2.5241 -5 3 1 4 35.59 11.99 2.5225 -7 1 3 4 37.57 2.06 2.3941 3 1 3 4 37.58 2.03 2.3935 0 2 4 4 37.60 2.07 2.3924 -3 1 5 4 38.07 9.21 2.3634 4 2 2 4 38.08 9.20 2.3633 1 3 3 4 38.11 9.21 2.3611 -5 1 5 4 40.26 2.67 2.2399 5 1 2 4 40.27 2.64 2.2393 -1 3 4 4 40.29 2.67 2.2382 -4 2 5 4 40.46 2.40 2.2293 2 0 4 2 40.48 4.80 2.2286 -1 1 5 4 40.73 3.06 2.2151 4 4 0 4 40.78 1.53 2.2129 -8 0 4 2 41.87 4.48 2.1574 2 4 2 4 41.88 4.47 2.1573 5 3 1 4 41.92 4.44 2.1550 -7 1 5 4 42.35 3.93 2.1342 6 2 1 4 42.35 3.93 2.1342 0 4 3 4 42.39 3.91 2.1324 -6 2 5 4 43.15 1.42 2.0966 -1 5 1 4 43.17 1.42 2.0954 -8 2 2 4 43.18 1.40 2.0953 -7 3 3 4 44.29 10.05 2.0452 1 5 1 4 44.30 9.98 2.0445 -7 3 1 4 44.33 10.01 2.0433 -8 2 4 4 44.87 3.58 2.0200 3 3 3 4 44.90 1.42 2.0189 -3 3 5 4 44.92 1.79 2.0179 -6 0 6 2 44.93 1.97 2.0174 4 2 3 4 44.94 1.98 2.0172 1 3 4 4 44.97 1.97 2.0156 -5 1 6 4 45.07 1.77 2.0113 -3 5 1 4 45.09 1.76 2.0108 -6 4 2 4 45.11 1.79 2.0098 -9 1 3 4 45.32 4.44 2.0012 7 1 1 4 45.32 4.42 2.0009 -2 4 4 4 45.34 4.42 2.0000 -5 3 5 4 45.38 1.96 1.9985 -4 4 4 4 47.32 2.27 1.9211 1 5 2 4 47.33 2.25 1.9207 7 3 0 4 47.37 2.25 1.9192 -8 2 5 4 47.40 1.55 1.9181 5 1 3 4 47.41 1.56 1.9176 -1 3 5 4 47.43 1.56 1.9168 -4 2 6 4 48.33 1.82 1.8833 3 5 1 4 48.33 1.82 1.8831 6 4 0 4 48.38 1.81 1.8813 -9 1 5 4 48.60 5.29 1.8734 4 4 2 4 48.65 1.32 1.8715 -1 5 3 4 48.66 2.63 1.8712 -8 0 6 2 48.66 1.32 1.8712 8 2 0 4 48.69 1.32 1.8701 -7 3 5 4 49.48 1.16 1.8419 -2 2 6 4 49.79 2.43 1.8313 -5 5 1 4 49.83 1.21 1.8298 -10 0 4 2 50.83 3.44 1.7964 -5 5 3 4 50.84 1.72 1.7959 -10 0 2 2 51.73 3.13 1.7670 1 5 3 4 51.74 3.11 1.7669 7 3 1 4 51.79 3.10 1.7653 -8 2 6 4 52.55 1.22 1.7413 4 2 4 4 52.56 1.21 1.7411 1 3 5 4 52.60 1.22 1.7399 -5 1 7 4 52.86 3.60 1.7319 2 6 0 4 52.89 3.56 1.7312 -8 4 2 4 52.91 3.56 1.7304 -10 2 4 4 53.63 1.67 1.7089 5 3 3 4 53.63 1.66 1.7089 2 4 4 4 53.69 1.64 1.7072 -7 1 7 4 54.14 1.96 1.6940 3 1 5 4 54.15 1.97 1.6937 0 2 6 4 54.17 1.96 1.6931 -3 1 7 4 54.78 5.23 1.6758 5 5 1 4 54.84 2.60 1.6739 -10 0 6 2 54.99 1.98 1.6698 6 2 3 4 55.00 1.98 1.6695 0 4 5 4 55.04 1.98 1.6683 -6 2 7 4 55.24 1.19 1.6628 5 1 4 4 55.26 1.20 1.6623 -1 3 6 4 55.28 1.21 1.6617 -4 2 7 4 56.59 1.57 1.6263 -4 4 6 4 57.26 1.14 1.6089 3 5 3 4 57.26 1.14 1.6089 6 4 2 4 57.33 1.12 1.6071 -9 1 7 4 58.24 1.63 1.5842 2 0 6 2 58.25 3.25 1.5839 -1 1 7 4 58.39 2.59 1.5803 7 1 3 4 58.42 2.60 1.5798 -2 4 6 4 58.44 2.58 1.5793 -5 3 7 4 60.25 7.30 1.5360 -6 6 2 4 60.29 3.64 1.5350 -12 0 4 2 60.44 1.23 1.5316 -2 6 4 4 60.45 1.23 1.5314 10 2 0 4 60.48 1.22 1.5307 -8 4 6 4 61.02 1.26 1.5184 2 2 6 4 61.18 2.55 1.5150 4 4 4 4 61.25 1.27 1.5134 -8 0 8 2 61.46 2.48 1.5087 -1 7 1 4 61.50 2.48 1.5078 -11 3 3 4 61.50 2.47 1.5077 -10 4 4 4 62.62 1.24 1.4836 6 2 4 4 62.63 1.23 1.4833 0 4 6 4 62.67 1.23 1.4824 -6 2 8 4 62.94 3.89 1.4768 6 6 0 4 62.96 2.91 1.4764 -6 6 4 4 62.97 1.45 1.4761 -12 0 2 2 62.97 1.85 1.4760 -3 7 1 4 63.00 1.83 1.4754 -9 5 3 4 63.01 1.94 1.4753 -12 0 6 2 63.03 1.83 1.4749 -12 2 4 4 63.89 2.19 1.4571 7 3 3 4 63.89 2.19 1.4569 1 5 5 4 63.96 2.17 1.4557 -8 2 8 4 64.78 1.00 1.4392 1 7 2 4 64.80 1.00 1.4387 -10 4 1 4 66.28 1.09 1.4101 8 2 3 4 66.30 1.09 1.4098 -1 5 6 4 66.34 1.10 1.4090 -7 3 8 4 69.17 1.47 1.3581 -5 5 7 4 69.75 1.08 1.3482 4 2 6 4 69.77 1.09 1.3480 1 3 7 4 69.81 1.08 1.3473 -5 1 9 4 70.25 2.55 1.3399 0 0 8 2 70.67 1.80 1.3329 6 6 2 4 70.71 1.64 1.3323 -6 6 6 4 72.78 1.40 1.2995 -2 8 2 4 72.82 1.39 1.2988 -13 3 3 4 72.83 1.39 1.2987 -11 5 5 4 74.80 2.03 1.2693 7 1 5 4 74.83 2.04 1.2688 -2 4 8 4 74.86 2.03 1.2685 -5 3 9 4 78.32 1.08 1.2208 -6 8 2 4 78.34 1.08 1.2206 -9 7 3 4 79.00 1.85 1.2120 5 5 5 4 80.02 1.21 1.1991 5 7 3 4 80.02 1.21 1.1991 8 6 2 4 80.13 1.21 1.1977 -13 1 9 4 80.74 1.81 1.1902 -6 8 4 4 80.76 1.82 1.1899 -9 7 5 4 83.87 1.12 1.1536 11 1 3 4 83.90 1.12 1.1532 -4 6 8 4 83.93 1.12 1.1529 -7 5 9 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.