Mo O7 P2 Rb Riou D, Leclaire A, Grandin A, Raveau B Acta Crystallographica C45 (1989) 989-991 Structure of a diphosphate of trivalent molybdenum Rb Mo P2 O7 _cod_database_code 1001391 _database_code_amcsd 0010078 CELL PARAMETERS: 7.5237 10.3537 8.3998 90.000 105.832 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 629.507 Density (g/cm3): 3.749 MAX. ABS. INTENSITY / VOLUME**2: 21.99420493 RIR: 1.910 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.23 11.38 7.2383 1 0 0 2 13.90 14.62 6.3704 0 1 1 4 14.93 23.99 5.9323 1 1 0 4 16.44 30.74 5.3917 -1 1 1 4 20.37 5.74 4.3591 0 2 1 4 20.46 4.53 4.3414 1 1 1 4 22.00 39.52 4.0406 0 0 2 2 22.08 7.11 4.0265 -1 0 2 2 22.20 3.27 4.0037 -1 2 1 4 23.64 12.15 3.7641 0 1 2 4 23.71 24.75 3.7527 -1 1 2 4 24.60 28.27 3.6191 2 0 0 2 25.35 32.28 3.5128 1 2 1 4 26.08 4.47 3.4164 2 1 0 4 28.01 12.78 3.1852 0 2 2 4 28.08 18.73 3.1783 -1 2 2 4 28.11 21.45 3.1739 0 3 1 4 28.66 69.80 3.1152 1 3 0 4 29.40 73.69 3.0384 1 1 2 4 29.58 32.91 3.0204 -2 1 2 4 29.67 100.00 3.0108 -2 2 1 4 30.93 1.87 2.8910 2 1 1 4 33.23 4.20 2.6958 -2 2 2 4 33.31 25.25 2.6895 -1 1 3 4 34.22 1.92 2.6204 -1 3 2 4 34.46 1.19 2.6026 2 2 1 4 34.66 14.24 2.5884 0 4 0 2 35.57 2.38 2.5241 -2 3 1 4 35.96 4.17 2.4976 2 3 0 4 36.89 10.89 2.4366 -3 1 1 4 37.27 6.67 2.4128 3 0 0 2 37.55 6.35 2.3951 -1 4 1 4 37.86 1.39 2.3765 -3 0 2 2 38.30 1.29 2.3498 3 1 0 4 38.51 5.53 2.3379 1 3 2 4 39.59 2.75 2.2764 1 4 1 4 39.72 9.26 2.2691 1 1 3 4 39.73 5.49 2.2688 2 3 1 4 39.86 1.67 2.2616 -2 2 3 4 39.96 1.12 2.2563 -3 2 1 4 41.28 5.55 2.1869 3 2 0 4 41.43 2.08 2.1796 0 4 2 4 41.60 7.43 2.1707 2 2 2 4 41.67 17.43 2.1674 -1 3 3 4 42.84 7.91 2.1110 3 1 1 4 42.96 9.96 2.1054 2 4 0 4 43.08 8.37 2.0999 -1 0 4 2 43.89 6.30 2.0630 -3 1 3 4 44.00 1.72 2.0580 -1 1 4 4 44.86 13.13 2.0203 0 0 4 2 45.20 3.78 2.0059 0 5 1 4 45.30 1.73 2.0018 -2 4 2 4 45.56 1.52 1.9909 1 5 0 4 45.57 1.49 1.9905 3 2 1 4 45.76 2.65 1.9829 0 1 4 4 45.89 5.90 1.9774 3 3 0 4 46.13 15.94 1.9677 -1 5 1 4 46.25 2.73 1.9628 2 4 1 4 46.39 6.49 1.9573 -3 3 2 4 47.12 1.12 1.9286 1 3 3 4 48.10 1.71 1.8917 2 1 3 4 48.52 3.39 1.8763 -2 2 4 4 48.79 6.25 1.8664 0 4 3 4 49.24 6.75 1.8505 -4 0 2 2 49.80 3.59 1.8309 3 1 2 4 49.87 6.01 1.8287 3 3 1 4 50.07 4.25 1.8217 -4 1 2 4 50.08 3.51 1.8215 1 0 4 2 50.38 1.63 1.8112 -3 0 4 2 50.61 2.62 1.8035 2 2 3 4 50.61 6.55 1.8035 -2 4 3 4 50.69 1.02 1.8008 -3 4 1 4 50.80 1.77 1.7973 2 5 0 4 50.80 3.96 1.7972 -3 3 3 4 50.90 2.01 1.7939 1 1 4 4 50.90 1.43 1.7939 -1 3 4 4 51.20 4.38 1.7841 -3 1 4 4 51.77 16.86 1.7658 -4 2 1 4 51.80 1.66 1.7649 3 4 0 4 52.07 5.06 1.7564 2 4 2 4 52.26 1.07 1.7506 -3 4 2 4 52.48 2.39 1.7435 0 3 4 4 52.63 2.71 1.7390 -2 3 4 4 52.76 1.43 1.7350 1 5 2 4 52.93 4.93 1.7300 1 4 3 4 53.07 1.19 1.7256 0 6 0 2 53.48 3.25 1.7135 -4 1 3 4 53.61 1.20 1.7096 -3 2 4 4 53.72 1.58 1.7062 2 5 1 4 54.61 2.58 1.6805 2 3 3 4 55.18 2.23 1.6646 -1 6 1 4 55.28 1.11 1.6618 -1 5 3 4 55.48 3.14 1.6561 -1 1 5 4 56.17 3.17 1.6375 3 3 2 4 56.33 2.79 1.6332 -3 4 3 4 57.18 4.99 1.6109 1 3 4 4 57.46 2.42 1.6037 -3 3 4 4 57.51 1.19 1.6026 4 3 0 4 57.75 14.18 1.5965 -3 5 1 4 57.77 1.10 1.5960 -1 2 5 4 57.90 1.31 1.5926 0 4 4 4 57.99 1.48 1.5905 4 2 1 4 58.04 5.13 1.5892 2 0 4 2 58.04 1.18 1.5891 -2 4 4 4 58.13 5.99 1.5870 0 6 2 4 58.16 2.58 1.5861 -1 6 2 4 58.59 2.13 1.5755 3 1 3 4 58.62 7.35 1.5749 -2 2 5 4 59.07 1.49 1.5640 -2 6 1 4 59.57 1.64 1.5519 -4 3 3 4 59.90 2.04 1.5442 2 4 3 4 59.96 7.91 1.5428 0 2 5 4 61.21 1.61 1.5143 -2 6 2 4 61.39 1.56 1.5102 -4 2 4 4 61.61 1.31 1.5054 -4 4 2 4 61.98 1.31 1.4971 2 6 1 4 62.33 2.92 1.4897 4 1 2 4 62.44 4.84 1.4874 -3 2 5 4 64.09 1.56 1.4530 0 6 3 4 64.28 9.40 1.4492 1 7 0 4 64.35 1.07 1.4477 5 0 0 2 64.43 1.31 1.4461 0 5 4 4 64.61 1.76 1.4426 -4 4 3 4 64.80 3.02 1.4387 -5 2 1 4 65.06 1.93 1.4337 5 1 0 4 65.62 4.33 1.4228 -2 6 3 4 66.61 4.36 1.4041 4 4 1 4 66.86 4.93 1.3993 2 6 2 4 67.02 1.08 1.3963 -3 6 2 4 67.23 1.31 1.3926 -2 0 6 2 68.22 2.61 1.3748 -5 3 2 4 68.47 1.11 1.3704 1 3 5 4 68.53 2.03 1.3692 2 7 0 4 69.37 4.31 1.3547 -5 1 4 4 69.40 3.81 1.3543 2 4 4 4 69.63 2.32 1.3503 5 1 1 4 71.96 1.11 1.3121 0 6 4 4 72.09 1.77 1.3102 -2 6 4 4 72.51 7.14 1.3036 -1 5 5 4 72.79 4.84 1.2992 4 2 3 4 73.27 2.06 1.2920 -2 5 5 4 74.23 2.91 1.2776 3 3 4 4 74.97 1.04 1.2669 5 3 1 4 75.05 1.97 1.2656 -5 4 3 4 75.23 1.94 1.2631 3 5 3 4 75.65 3.01 1.2571 -4 0 6 2 75.91 2.06 1.2535 -6 0 2 2 76.09 2.78 1.2509 -3 3 6 4 76.23 1.07 1.2490 5 1 2 4 77.43 1.50 1.2325 0 8 2 4 77.84 2.93 1.2271 -5 2 5 4 78.00 1.78 1.2250 -6 1 3 4 78.88 1.88 1.2135 -5 5 1 4 79.07 1.88 1.2111 1 5 5 4 79.90 1.03 1.2005 4 6 1 4 80.48 1.39 1.1934 0 7 4 4 80.59 1.28 1.1920 -2 7 4 4 81.26 1.24 1.1839 -1 1 7 4 82.73 1.08 1.1666 0 8 3 4 82.73 1.93 1.1665 -4 5 5 4 83.15 1.34 1.1617 -6 3 3 4 84.35 2.83 1.1482 1 7 4 4 84.62 1.20 1.1452 4 7 0 4 85.42 1.24 1.1366 -3 8 2 4 85.87 1.10 1.1318 -1 9 1 4 85.96 1.02 1.1308 -4 4 6 4 89.40 1.08 1.0960 -5 3 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.