Pt(NH3)4(TcO4)2 Rochon F D, Kong P C, Melanson R Acta Crystallographica C46 (1990) 8-10 Tetraammineplatinum(II) bis[pertechnetate(VII)] _database_code_amcsd 0010085 CELL PARAMETERS: 5.1780 7.7250 7.9350 69.330 79.740 77.410 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 288.044 Density (g/cm3): 3.315 MAX. ABS. INTENSITY / VOLUME**2: 35.90628280 RIR: 3.527 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.99 8.86 7.3785 0 0 1 2 12.42 10.26 7.1244 0 1 0 2 14.18 7.20 6.2471 0 1 1 2 19.83 54.45 4.4779 1 1 1 2 19.84 55.49 4.4753 1 1 0 2 19.96 100.00 4.4492 0 -1 1 2 20.26 60.46 4.3839 1 0 1 2 22.49 50.75 3.9531 -1 0 1 2 23.24 69.34 3.8269 0 1 2 2 23.33 46.14 3.8135 -1 1 0 2 23.92 63.33 3.7195 0 2 1 2 25.29 35.96 3.5210 -1 1 1 2 28.17 17.73 3.1683 1 2 0 2 28.39 16.30 3.1441 1 0 2 2 29.81 19.27 2.9968 1 2 2 2 31.25 2.77 2.8622 0 -2 1 2 31.64 18.48 2.8276 -1 0 2 2 33.13 1.48 2.7043 -1 2 1 2 33.19 16.24 2.6989 -1 2 0 2 34.47 5.37 2.6022 0 1 3 2 34.61 6.31 2.5919 -1 -2 1 2 35.36 17.85 2.5386 1 -1 2 2 35.73 1.02 2.5130 0 3 1 2 35.76 21.44 2.5112 2 0 0 2 35.86 4.60 2.5043 2 1 0 2 35.92 8.07 2.5003 1 1 3 2 35.95 4.91 2.4980 -1 -1 2 2 36.36 19.83 2.4711 1 3 1 2 36.50 2.16 2.4619 2 0 1 2 36.53 21.77 2.4595 0 0 3 2 37.33 5.55 2.4090 1 2 3 2 37.40 6.37 2.4047 -1 2 2 2 37.58 2.19 2.3934 1 -2 1 2 37.69 3.94 2.3867 1 3 2 2 37.75 2.06 2.3829 0 3 2 2 37.89 16.71 2.3748 0 3 0 2 38.32 17.13 2.3490 2 2 1 2 38.63 8.49 2.3306 2 1 2 2 40.31 1.04 2.2376 2 2 0 2 40.55 10.77 2.2246 0 -2 2 2 40.57 11.15 2.2238 -2 -1 1 2 41.18 1.01 2.1920 2 0 2 2 41.86 4.56 2.1583 -1 1 3 2 41.89 2.96 2.1567 -2 1 1 2 41.99 13.67 2.1518 2 -1 1 2 43.46 8.64 2.0824 0 3 3 2 43.62 4.39 2.0752 -1 3 1 2 44.95 5.10 2.0168 -1 2 3 2 45.38 4.09 1.9984 -1 -3 1 2 45.49 1.24 1.9939 2 1 3 2 45.68 4.65 1.9862 1 -1 3 2 45.82 1.26 1.9805 -2 -2 1 2 45.91 3.01 1.9766 -1 3 2 2 47.19 8.65 1.9259 -2 1 2 2 47.24 4.89 1.9241 1 1 4 2 47.28 4.46 1.9227 -1 -1 3 2 47.52 9.71 1.9135 0 2 4 2 48.09 7.33 1.8919 2 3 0 2 48.13 5.07 1.8905 1 4 1 2 48.19 6.95 1.8882 -2 2 1 2 48.88 6.50 1.8634 2 0 3 2 48.98 8.17 1.8598 0 4 2 2 49.50 5.01 1.8414 1 -3 1 2 49.67 6.89 1.8355 2 3 3 2 50.78 4.63 1.7980 1 3 4 2 50.80 4.94 1.7972 1 0 4 2 51.29 5.03 1.7811 1 4 3 2 51.47 3.52 1.7755 1 4 0 2 53.11 3.62 1.7246 3 1 1 2 53.15 5.00 1.7231 -1 1 4 2 53.95 3.59 1.6996 2 2 4 2 54.01 3.92 1.6979 -2 -2 2 2 54.12 2.10 1.6945 3 1 0 2 54.14 5.89 1.6941 2 4 2 2 54.17 2.85 1.6932 -1 -3 2 2 54.87 1.97 1.6731 3 0 1 2 54.89 2.64 1.6726 -1 0 4 2 54.90 3.44 1.6724 -1 -2 3 2 55.05 3.83 1.6682 1 -2 3 2 55.08 5.83 1.6672 -2 0 3 2 55.38 6.41 1.6589 0 -1 4 2 55.68 2.69 1.6509 3 2 2 2 55.69 2.81 1.6505 -1 4 1 2 56.29 5.18 1.6343 2 -2 2 2 56.68 3.57 1.6241 3 2 0 2 56.86 1.57 1.6192 1 -3 2 2 57.02 5.15 1.6151 0 -4 1 2 57.40 2.91 1.6053 1 4 4 2 57.75 3.58 1.5964 -2 3 0 2 57.76 2.24 1.5961 -1 4 0 2 57.81 2.81 1.5949 -3 0 1 2 57.91 2.16 1.5923 3 0 2 2 58.72 2.54 1.5724 1 2 5 2 58.74 2.46 1.5718 -3 1 0 2 59.34 2.78 1.5574 3 3 2 2 59.35 2.87 1.5571 3 3 1 2 59.45 2.30 1.5548 -1 3 4 2 59.63 1.86 1.5506 3 2 3 2 59.69 3.88 1.5492 0 1 5 2 60.12 2.40 1.5391 1 5 2 2 60.14 2.32 1.5386 3 1 3 2 60.45 1.32 1.5314 -1 4 3 2 60.62 2.53 1.5275 -3 1 1 2 60.84 2.18 1.5227 1 3 5 2 61.53 2.40 1.5070 -3 -2 1 2 61.96 1.48 1.4977 1 5 3 2 62.18 4.89 1.4929 0 5 1 2 62.64 3.95 1.4831 0 -3 3 2 63.52 1.59 1.4647 -3 0 2 2 63.60 2.59 1.4630 3 -1 2 2 63.73 1.54 1.4603 1 0 5 2 64.46 2.06 1.4455 -2 -4 1 2 64.68 2.17 1.4410 -2 3 3 2 64.75 1.64 1.4396 -3 -1 2 2 64.95 1.76 1.4358 1 5 0 2 65.48 2.05 1.4255 -3 2 0 2 65.54 2.85 1.4243 2 -1 4 2 65.81 2.08 1.4190 2 1 5 2 66.15 2.50 1.4126 2 5 1 2 66.21 1.80 1.4115 -1 2 5 2 66.23 1.31 1.4111 -1 -4 2 2 66.57 1.20 1.4047 1 -2 4 2 66.78 1.83 1.4007 3 4 1 2 66.90 1.09 1.3986 -1 4 4 2 67.33 1.11 1.3908 -1 -2 4 2 67.34 2.90 1.3905 -2 2 4 2 67.36 1.60 1.3902 3 -2 1 2 67.59 1.05 1.3860 3 1 4 2 67.63 1.38 1.3852 3 4 3 2 67.71 1.55 1.3839 3 3 4 2 67.95 3.36 1.3795 0 4 5 2 68.83 2.39 1.3640 0 5 4 2 69.03 1.42 1.3605 -1 5 2 2 69.52 2.04 1.3521 -2 4 2 2 69.67 2.59 1.3497 2 4 5 2 69.81 2.35 1.3472 -2 -1 4 2 70.00 1.65 1.3440 3 -1 3 2 70.00 1.40 1.3440 1 -4 2 2 70.04 1.70 1.3434 2 5 4 2 70.40 1.11 1.3375 3 4 0 2 70.49 1.36 1.3360 1 -1 5 2 71.31 1.02 1.3226 -1 -5 1 2 71.61 1.48 1.3178 -1 5 3 2 71.85 1.17 1.3139 -1 5 0 2 72.05 1.56 1.3108 3 4 4 2 72.37 1.06 1.3057 -3 1 3 2 72.81 2.02 1.2990 -2 -3 3 2 73.38 1.47 1.2903 1 1 6 2 73.42 1.17 1.2896 -1 -1 5 2 73.56 1.34 1.2875 1 5 5 2 73.66 1.12 1.2861 1 6 2 2 73.67 1.12 1.2859 -3 -1 3 2 73.71 1.62 1.2853 2 -4 1 2 73.85 1.61 1.2832 4 2 1 2 74.36 1.63 1.2756 0 3 6 2 74.54 1.50 1.2730 4 1 2 2 75.61 1.17 1.2577 3 3 5 2 75.72 1.18 1.2561 2 -3 3 2 75.76 1.16 1.2556 4 0 0 2 75.91 1.05 1.2534 -3 2 3 2 76.43 1.10 1.2462 1 4 6 2 76.50 1.41 1.2453 2 3 6 2 76.84 1.13 1.2405 -1 -4 3 2 76.89 1.44 1.2398 0 6 3 2 77.10 1.28 1.2370 -3 3 2 2 77.13 1.55 1.2367 -2 1 5 2 77.27 1.05 1.2348 -1 -3 4 2 77.64 1.38 1.2298 0 0 6 2 77.73 1.66 1.2286 0 -2 5 2 78.33 1.37 1.2207 -4 -1 1 2 78.45 1.01 1.2190 -3 -2 3 2 78.83 1.00 1.2142 3 -2 3 2 78.96 1.59 1.2125 4 3 3 2 79.67 1.45 1.2034 0 -5 2 2 80.23 1.34 1.1965 4 -1 1 2 80.24 1.38 1.1964 4 3 0 2 80.97 1.34 1.1874 0 6 0 2 81.25 1.35 1.1840 -2 5 1 2 82.05 1.31 1.1745 4 4 2 2 82.25 1.24 1.1721 4 0 3 2 82.84 1.31 1.1653 4 2 4 2 83.64 1.17 1.1562 2 0 6 2 85.74 1.21 1.1331 -2 -5 2 2 87.58 1.08 1.1140 -4 2 1 2 89.78 1.06 1.0923 -2 5 4 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.