N(C2H5)4I.2GeI4 Muller V U, Krug V Acta Crystallographica C46 (1990) 523-525 Tetraethylammoniumiodid-germaniumtetraiodid(1/2), eine strukture mit einem von acht iodatomen koordinierten iodidion _database_code_amcsd 0010115 CELL PARAMETERS: 17.9530 9.9900 17.5090 90.000 108.870 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2971.474 Density (g/cm3): 3.123 MAX. ABS. INTENSITY / VOLUME**2: 17.55415103 RIR: 1.830 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.41 31.88 8.4941 2 0 0 2 10.68 39.98 8.2840 0 0 2 2 10.77 100.00 8.2117 -1 1 1 4 12.28 36.30 7.2095 -2 0 2 2 12.34 67.49 7.1747 1 1 1 4 13.56 12.41 6.5287 -1 1 2 4 17.20 42.29 5.1554 2 0 2 2 17.28 74.85 5.1330 -3 1 1 4 17.60 64.18 5.0394 -1 1 3 4 17.76 39.63 4.9950 0 2 0 2 18.18 1.63 4.8802 -3 1 2 4 20.18 1.57 4.4011 -4 0 2 2 20.20 18.30 4.3962 3 1 1 4 20.44 2.05 4.3443 -2 2 1 4 20.48 8.79 4.3369 1 1 3 4 20.51 13.48 4.3311 -3 1 3 4 20.59 17.41 4.3128 -2 0 4 2 20.63 25.67 4.3057 2 2 0 4 20.77 8.65 4.2776 0 2 2 4 20.92 3.08 4.2470 4 0 0 2 22.17 10.08 4.0103 2 2 1 4 22.24 12.24 3.9974 -1 1 4 4 23.86 1.61 3.7290 -3 1 4 4 24.03 1.92 3.7027 -2 2 3 4 24.70 17.72 3.6047 -4 0 4 2 24.82 31.73 3.5874 2 2 2 4 25.34 5.89 3.5144 1 1 4 4 26.48 1.94 3.3665 -5 1 2 4 26.50 56.07 3.3634 4 0 2 2 26.56 27.83 3.3558 -5 1 1 4 26.74 4.27 3.3339 -4 2 1 4 26.83 12.67 3.3235 2 0 4 2 27.00 83.38 3.3022 -4 2 2 4 27.21 68.97 3.2779 -1 1 5 4 27.29 12.21 3.2678 1 3 0 4 27.32 32.45 3.2644 -2 2 4 4 27.44 6.87 3.2500 3 1 3 4 27.49 26.33 3.2451 -5 1 3 4 27.49 44.97 3.2446 -1 3 1 4 27.98 22.06 3.1884 0 2 4 4 28.16 2.81 3.1688 1 3 1 4 28.29 3.20 3.1541 2 2 3 4 28.33 5.92 3.1508 -4 2 3 4 28.74 2.95 3.1065 -1 3 2 4 29.87 13.75 2.9910 5 1 1 4 30.45 2.26 2.9355 1 1 5 4 30.58 1.67 2.9230 -4 2 4 4 30.64 6.16 2.9182 -2 0 6 2 30.73 5.42 2.9097 -3 3 1 4 30.92 2.26 2.8923 -1 3 3 4 31.25 10.02 2.8626 -2 2 5 4 31.26 2.87 2.8612 -3 3 2 4 31.60 16.20 2.8314 6 0 0 2 31.90 1.60 2.8053 3 1 4 4 32.00 1.72 2.7965 -6 0 4 2 32.08 2.42 2.7899 4 2 2 4 32.36 1.63 2.7670 2 2 4 4 32.40 2.99 2.7630 -3 1 6 4 32.42 14.27 2.7613 0 0 6 2 32.46 1.87 2.7583 -4 0 6 2 32.70 1.24 2.7387 1 3 3 4 32.72 22.98 2.7372 -3 3 3 4 33.61 1.19 2.6666 -4 2 5 4 34.71 5.61 2.5843 3 3 2 4 34.80 20.75 2.5777 4 0 4 2 34.96 39.37 2.5665 -6 2 2 4 34.99 6.51 2.5643 -3 3 4 4 35.30 3.42 2.5427 -6 2 1 4 35.48 3.30 2.5299 -6 2 3 4 35.63 34.13 2.5197 -2 2 6 4 35.96 16.32 2.4975 0 4 0 2 36.37 1.19 2.4700 5 1 3 4 36.38 10.63 2.4696 0 4 1 4 36.42 2.89 2.4668 -7 1 3 4 36.48 1.16 2.4632 6 2 0 4 36.77 7.14 2.4444 -7 1 1 4 37.21 1.21 2.4166 0 2 6 4 37.23 1.10 2.4151 -3 1 7 4 37.36 3.95 2.4071 2 0 6 2 37.42 10.39 2.4032 -6 0 6 2 37.43 2.78 2.4026 -1 3 5 4 37.61 19.62 2.3916 3 3 3 4 37.96 3.77 2.3704 -3 3 5 4 38.13 1.92 2.3599 -2 4 2 4 39.48 2.34 2.2825 5 3 1 4 39.60 1.05 2.2756 0 4 3 4 39.78 4.34 2.2662 -5 1 7 4 40.29 2.52 2.2387 7 1 1 4 40.36 3.20 2.2345 -2 2 7 4 41.02 2.17 2.2005 -8 0 4 2 41.09 1.40 2.1967 3 3 4 4 41.40 1.35 2.1809 -2 0 8 2 41.58 1.85 2.1721 -4 4 2 4 41.76 3.47 2.1631 3 1 6 4 41.82 3.07 2.1599 5 3 2 4 42.47 1.28 2.1283 2 4 3 4 43.22 2.30 2.0931 -1 1 8 4 44.24 1.89 2.0473 1 3 6 4 44.28 3.19 2.0455 -5 3 6 4 44.77 3.46 2.0242 5 3 3 4 44.81 1.24 2.0224 -7 3 3 4 44.88 6.86 2.0196 5 1 5 4 44.93 1.97 2.0174 -7 1 7 4 45.02 2.75 2.0138 -8 2 4 4 45.05 1.38 2.0125 3 3 5 4 45.11 10.61 2.0100 -7 3 1 4 45.11 5.31 2.0097 -6 0 8 2 45.22 5.40 2.0051 4 4 2 4 45.72 1.25 1.9846 -7 3 4 4 45.72 1.07 1.9843 1 5 0 4 45.83 10.51 1.9798 -4 2 8 4 45.92 4.28 1.9762 -1 3 7 4 46.29 3.28 1.9615 1 5 1 4 46.29 2.30 1.9613 7 3 0 4 46.39 1.08 1.9574 -8 2 5 4 46.43 2.76 1.9558 -9 1 3 4 46.47 10.59 1.9542 8 2 0 4 46.66 1.66 1.9465 -1 5 2 4 47.04 9.26 1.9318 3 1 7 4 47.29 1.31 1.9223 -7 3 5 4 47.42 2.52 1.9172 -6 4 2 4 47.52 4.89 1.9134 1 5 2 4 47.53 1.02 1.9131 0 2 8 4 47.57 1.41 1.9116 -9 1 1 4 47.62 2.40 1.9096 -3 1 9 4 47.68 7.12 1.9073 -5 3 7 4 47.79 3.98 1.9030 4 4 3 4 47.94 6.02 1.8975 -2 4 6 4 47.99 6.78 1.8957 6 2 4 4 48.01 3.26 1.8951 -3 5 1 4 48.38 1.82 1.8815 -3 5 2 4 48.39 4.58 1.8808 -8 2 6 4 48.50 1.88 1.8769 8 2 1 4 48.54 1.10 1.8756 -7 1 8 4 48.61 1.26 1.8730 6 4 0 4 48.87 1.28 1.8638 -1 1 9 4 48.90 1.98 1.8626 1 3 7 4 48.91 3.71 1.8624 -5 1 9 4 49.22 1.74 1.8514 -4 4 6 4 49.26 1.61 1.8499 3 5 1 4 49.47 1.72 1.8424 -7 3 6 4 49.90 1.98 1.8277 -3 3 8 4 50.23 7.28 1.8165 -1 5 4 4 50.65 1.92 1.8024 -8 0 8 2 50.91 2.02 1.7937 4 4 4 4 51.09 7.86 1.7878 -10 0 4 2 51.12 5.45 1.7869 8 2 2 4 51.28 3.21 1.7817 9 1 1 4 52.04 7.93 1.7572 2 2 8 4 52.09 1.48 1.7557 -9 1 7 4 52.22 5.16 1.7518 -7 3 7 4 52.39 1.37 1.7466 -4 0 10 2 52.46 5.57 1.7442 -5 5 2 4 52.51 1.02 1.7428 1 1 9 4 52.51 1.57 1.7427 -5 5 1 4 52.76 2.36 1.7350 -2 0 10 2 52.82 1.82 1.7332 2 4 6 4 52.88 4.57 1.7315 -1 5 5 4 53.04 1.47 1.7266 -5 5 3 4 53.18 2.82 1.7223 5 5 0 4 53.31 3.71 1.7185 6 0 6 2 53.56 4.79 1.7110 -9 3 3 4 53.97 1.45 1.6991 -9 3 4 4 54.09 2.89 1.6954 -8 2 8 4 54.11 2.91 1.6948 3 3 7 4 54.38 1.07 1.6871 7 1 5 4 54.50 1.11 1.6836 4 4 5 4 54.64 3.06 1.6798 -3 3 9 4 54.70 1.27 1.6779 -10 2 2 4 55.16 1.36 1.6650 0 6 0 2 55.47 2.13 1.6567 0 6 1 4 55.69 1.28 1.6506 -6 4 7 4 56.04 1.78 1.6411 -1 5 6 4 57.28 1.47 1.6083 10 2 0 4 60.85 1.49 1.5224 7 3 5 4 61.19 1.01 1.5147 -10 2 8 4 61.62 1.26 1.5052 5 5 4 4 63.30 1.18 1.4693 8 0 6 2 64.05 1.52 1.4537 -10 4 4 4 64.30 1.39 1.4486 4 6 3 4 64.79 1.03 1.4389 -10 4 5 4 64.96 1.23 1.4356 9 1 5 4 65.04 1.51 1.4340 -3 3 11 4 65.15 1.07 1.4318 -11 3 1 4 65.65 1.06 1.4221 1 7 0 4 65.83 2.73 1.4187 -11 1 9 4 66.69 1.26 1.4024 3 5 7 4 80.86 1.24 1.1888 12 2 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.