Na3AsO3S.12H2O Kempa P B, Wiebcke M, Felsche J Acta Crystallographica C46 (1990) 729-732 Structure of trisodium monothioarsenate dodecahydrate Sample: T = 213 K _database_code_amcsd 0010125 CELL PARAMETERS: 9.2200 12.8310 13.9060 90.000 90.000 90.000 SPACE GROUP: P2_12_12_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1645.105 Density (g/cm3): 1.679 MAX. ABS. INTENSITY / VOLUME**2: 7.472751980 RIR: 1.449 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.82 27.64 7.4874 1 1 0 4 12.73 12.23 6.9530 0 0 2 2 13.80 9.40 6.4155 0 2 0 2 14.49 2.54 6.1131 0 1 2 4 15.21 20.27 5.8254 0 2 1 4 15.96 4.06 5.5514 1 0 2 4 17.41 100.00 5.0950 1 1 2 4 18.82 11.81 4.7150 0 2 2 4 19.25 38.50 4.6100 2 0 0 2 21.16 5.65 4.1979 1 2 2 4 21.74 1.37 4.0880 0 3 1 4 22.56 27.82 3.9412 1 1 3 4 22.92 3.07 3.8799 1 3 0 4 23.15 10.24 3.8422 2 0 2 4 23.68 3.11 3.7572 0 2 3 4 23.77 1.84 3.7437 2 2 0 4 23.81 10.43 3.7371 1 3 1 4 24.18 1.06 3.6807 2 1 2 4 24.43 1.20 3.6430 0 3 2 4 24.63 21.69 3.6150 2 2 1 4 25.60 2.50 3.4794 1 2 3 4 25.62 6.77 3.4765 0 0 4 2 26.30 3.45 3.3881 1 3 2 4 27.05 3.60 3.2963 2 2 2 4 27.81 4.06 3.2078 0 4 0 2 28.30 12.41 3.1532 1 1 4 4 28.56 9.57 3.1257 0 4 1 4 29.20 1.41 3.0586 2 3 1 4 29.22 10.41 3.0566 0 2 4 4 29.77 2.56 3.0009 3 0 1 4 29.90 3.21 2.9888 3 1 0 4 30.19 2.30 2.9602 1 4 1 4 30.59 11.04 2.9221 3 1 1 4 30.70 18.87 2.9127 0 4 2 4 30.70 9.50 2.9124 2 2 3 4 30.82 2.82 2.9013 1 2 4 4 31.29 5.45 2.8582 2 3 2 4 31.84 1.75 2.8110 3 0 2 4 32.25 5.36 2.7757 2 0 4 4 32.30 8.65 2.7717 3 2 0 4 32.61 8.28 2.7459 3 1 2 4 33.02 9.22 2.7129 2 1 4 4 33.21 1.97 2.6977 0 3 4 4 33.66 5.20 2.6627 1 0 5 4 34.05 9.96 2.6330 2 4 0 4 34.40 5.20 2.6071 1 1 5 4 34.54 7.55 2.5971 2 3 3 4 34.64 2.42 2.5892 1 3 4 4 34.85 5.83 2.5747 3 2 2 4 35.03 1.09 2.5615 3 0 3 4 35.23 6.37 2.5475 2 2 4 4 35.39 6.22 2.5360 1 4 3 4 35.75 6.34 2.5119 3 1 3 4 35.98 1.30 2.4958 3 3 0 4 36.54 1.65 2.4593 1 2 5 4 36.58 7.06 2.4566 3 3 1 4 36.93 2.90 2.4341 1 5 1 4 37.78 2.25 2.3814 2 0 5 4 37.82 1.73 2.3789 3 2 3 4 38.32 1.61 2.3491 3 3 2 4 38.45 2.40 2.3414 2 1 5 4 38.65 8.63 2.3294 1 5 2 4 38.67 1.88 2.3283 2 3 4 4 38.86 4.01 2.3177 0 0 6 2 39.08 1.37 2.3050 4 0 0 2 39.35 7.64 2.2895 2 4 3 4 39.45 4.38 2.2840 1 4 4 4 39.88 1.55 2.2604 1 3 5 4 40.40 2.65 2.2325 2 2 5 4 40.75 3.54 2.2140 1 1 6 4 40.76 1.03 2.2136 2 5 1 4 41.07 1.38 2.1975 3 3 3 4 41.26 1.13 2.1879 4 0 2 4 41.39 5.66 2.1814 1 5 3 4 41.67 1.03 2.1672 3 2 4 4 42.16 4.16 2.1433 4 2 1 4 42.62 2.59 2.1213 1 2 6 4 42.78 4.44 2.1137 0 6 1 4 43.50 1.47 2.0806 2 3 5 4 43.71 2.08 2.0707 2 0 6 4 44.21 2.67 2.0488 1 4 5 4 44.50 2.44 2.0360 3 1 5 4 44.70 1.69 2.0274 3 3 4 4 44.99 1.02 2.0147 1 5 4 4 45.31 1.57 2.0016 3 4 3 4 45.59 4.03 1.9897 1 3 6 4 46.08 2.57 1.9698 3 5 0 4 46.57 4.88 1.9503 3 5 1 4 47.31 13.41 1.9213 2 6 1 4 47.55 1.61 1.9121 2 4 5 4 47.87 1.08 1.9001 1 6 3 4 47.88 2.18 1.8999 4 1 4 4 47.94 1.29 1.8977 0 2 7 4 48.00 1.61 1.8952 3 5 2 4 48.46 1.05 1.8786 0 4 6 4 48.64 1.62 1.8719 4 4 0 4 48.73 1.41 1.8686 2 6 2 4 49.32 2.11 1.8477 1 5 5 4 49.53 4.24 1.8404 4 2 4 4 49.79 2.58 1.8315 3 1 6 4 50.33 5.43 1.8129 3 5 3 4 50.49 1.10 1.8075 4 4 2 4 51.24 3.12 1.7830 1 7 1 4 51.39 2.84 1.7780 3 2 6 4 51.69 3.15 1.7683 1 3 7 4 51.78 7.74 1.7654 5 1 2 4 52.12 2.73 1.7548 2 2 7 4 52.20 1.39 1.7524 4 3 4 4 52.42 1.40 1.7456 2 5 5 4 52.58 1.59 1.7406 1 7 2 4 52.66 1.06 1.7383 0 0 8 2 52.74 2.71 1.7357 4 4 3 4 53.17 2.05 1.7225 0 1 8 4 53.58 2.94 1.7105 4 2 5 4 53.87 1.10 1.7020 3 6 2 4 53.99 5.36 1.6983 5 1 3 4 54.17 1.19 1.6932 1 1 8 4 54.60 1.67 1.6809 5 3 1 4 54.70 1.41 1.6781 2 3 7 4 55.30 2.63 1.6613 1 4 7 4 56.11 1.30 1.6392 4 3 5 4 57.08 2.27 1.6136 2 1 8 4 57.21 1.40 1.6103 0 3 8 4 57.32 1.96 1.6075 3 5 5 4 57.73 3.52 1.5969 1 7 4 4 57.96 1.72 1.5911 2 6 5 4 59.05 2.61 1.5643 3 7 1 4 59.11 1.07 1.5628 0 8 2 4 59.32 4.45 1.5578 4 6 1 4 60.22 1.33 1.5367 6 0 0 2 60.94 1.98 1.5203 2 3 8 4 61.14 1.07 1.5157 0 8 3 4 61.41 1.82 1.5098 1 7 5 4 61.83 1.09 1.5005 6 0 2 4 62.29 1.15 1.4906 3 7 3 4 62.37 1.92 1.4889 5 5 1 4 62.55 2.06 1.4851 4 6 3 4 62.78 1.33 1.4801 3 4 7 4 62.78 1.41 1.4801 2 8 2 4 63.14 1.42 1.4726 3 2 8 4 64.08 1.27 1.4532 0 3 9 4 65.04 1.82 1.4341 3 7 4 4 65.50 1.18 1.4250 5 5 3 4 66.40 1.77 1.4078 5 2 6 4 67.48 1.91 1.3879 2 6 7 4 67.59 1.15 1.3860 2 3 9 4 68.12 1.40 1.3764 1 4 9 4 68.32 1.44 1.3729 6 2 4 4 69.97 1.55 1.3445 1 2 10 4 73.16 1.03 1.2935 4 8 2 4 73.56 1.33 1.2876 7 1 2 4 74.89 1.13 1.2680 3 4 9 4 76.67 1.21 1.2429 3 2 10 4 77.57 1.74 1.2307 4 6 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.