PbCo4(CO)16 Leigh J S, Whitmire K H Acta Crystallographica C46 (1990) 732-736 The structures of [Sn{Co(CO4)4}4] and [Pb{Co(CO)4}4] _database_code_amcsd 0010127 CELL PARAMETERS: 12.1840 12.2670 17.2200 90.000 90.000 90.000 SPACE GROUP: Pccn X-RAY WAVELENGTH: 1.541838 Cell Volume: 2573.720 Density (g/cm3): 2.299 MAX. ABS. INTENSITY / VOLUME**2: 36.78515219 RIR: 5.209 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.23 100.00 8.6446 1 1 0 4 10.27 11.32 8.6100 0 0 2 2 12.56 49.33 7.0473 0 1 2 4 12.59 20.09 7.0315 1 0 2 4 14.44 11.08 6.1335 0 2 0 2 14.52 13.77 6.1004 1 1 2 8 14.54 10.93 6.0920 2 0 0 2 17.75 3.34 4.9956 0 2 2 4 17.84 18.95 4.9731 2 0 2 4 19.20 17.09 4.6221 1 2 2 8 19.26 3.33 4.6087 2 1 2 8 22.94 1.57 3.8765 1 3 0 4 23.07 1.55 3.8555 3 1 0 4 24.09 10.19 3.6936 0 3 2 4 25.28 3.34 3.5237 0 2 4 4 25.31 7.53 3.5188 3 1 2 8 26.33 3.64 3.3850 1 2 4 8 26.37 15.37 3.3797 2 1 4 8 27.89 1.66 3.1994 1 1 5 8 28.26 3.84 3.1584 2 3 2 8 28.32 2.07 3.1513 3 2 2 8 29.12 1.11 3.0668 0 4 0 2 29.28 3.52 3.0502 2 2 4 8 29.32 4.36 3.0460 4 0 0 2 30.25 9.36 2.9542 3 0 4 4 30.50 1.39 2.9306 1 4 1 8 30.65 3.48 2.9166 3 2 3 8 30.66 1.50 2.9157 1 2 5 8 30.69 1.72 2.9136 4 1 1 8 31.04 15.21 2.8807 1 3 4 8 31.15 6.47 2.8716 4 0 2 4 31.83 10.63 2.8110 1 4 2 8 32.01 6.03 2.7960 4 1 2 8 32.69 1.36 2.7392 2 4 0 4 32.88 1.16 2.7238 1 1 6 8 33.62 5.53 2.6658 2 3 4 8 33.67 8.27 2.6616 3 2 4 8 34.36 4.70 2.6103 2 4 2 8 34.50 2.21 2.5995 0 2 6 4 34.55 2.99 2.5963 2 0 6 4 35.95 1.17 2.4978 0 4 4 4 36.73 2.64 2.4469 1 4 4 8 36.88 3.14 2.4370 4 1 4 8 37.39 2.75 2.4051 1 5 0 4 37.56 2.60 2.3946 3 3 4 8 37.62 6.13 2.3909 2 2 6 8 37.63 4.07 2.3901 5 1 0 4 38.14 2.04 2.3595 0 5 2 4 38.30 2.18 2.3500 4 3 2 8 38.39 2.44 2.3447 5 0 2 4 38.88 2.16 2.3164 1 5 2 8 39.05 4.92 2.3066 1 3 6 8 39.09 2.17 2.3044 4 2 4 8 39.13 5.67 2.3022 3 1 6 8 41.22 3.33 2.1901 5 2 2 8 42.49 3.46 2.1276 3 4 4 8 42.55 1.50 2.1245 4 3 4 8 43.07 1.25 2.1000 3 5 0 4 43.22 1.17 2.0933 5 3 0 4 44.30 1.48 2.0445 0 6 0 2 44.40 1.98 2.0402 3 5 2 8 44.56 7.11 2.0335 3 3 6 8 44.62 1.54 2.0307 6 0 0 2 45.06 2.53 2.0120 2 5 4 8 45.29 1.98 2.0023 2 1 8 8 45.79 2.82 1.9816 2 4 6 8 45.89 2.31 1.9773 4 2 6 8 46.24 1.52 1.9632 1 6 2 8 46.54 2.27 1.9513 6 1 2 8 46.87 1.44 1.9383 2 6 0 4 47.83 1.03 1.9019 3 0 8 4 48.12 1.69 1.8909 2 6 2 8 48.35 1.47 1.8825 5 3 4 8 48.37 1.79 1.8819 1 3 8 8 48.90 2.09 1.8627 5 4 2 8 50.22 1.22 1.8166 3 2 8 8 51.35 1.31 1.7795 6 3 2 8 52.59 1.46 1.7401 4 1 8 8 52.96 1.78 1.7289 5 5 0 4 53.04 1.36 1.7264 4 4 6 8 53.75 1.42 1.7053 0 1 10 4 54.12 1.02 1.6948 3 5 6 8 54.17 1.05 1.6931 6 4 0 4 54.24 1.26 1.6912 5 3 6 8 56.97 1.08 1.6163 3 4 8 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.