Ru(HSO3)2(NH3)4 Condren S M, Cordes A W, Durham B Acta Crystallographica C46 (1990) 889-890 Structure of cis-tetraamminebis(hydrogensulfito)ruthenium(II) _database_code_amcsd 0010130 CELL PARAMETERS: 6.2019 7.0213 11.7610 90.000 115.300 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 463.014 Density (g/cm3): 2.376 MAX. ABS. INTENSITY / VOLUME**2: 15.53607186 RIR: 2.129 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 15.12 66.31 5.8591 0 1 1 4 15.81 100.00 5.6070 1 0 0 2 16.68 98.46 5.3165 0 0 2 2 17.40 29.21 5.0955 -1 0 2 2 19.16 42.65 4.6324 -1 1 1 4 20.27 21.75 4.3814 1 1 0 4 20.96 13.75 4.2385 0 1 2 4 21.55 20.60 4.1239 -1 1 2 4 24.42 19.69 3.6448 1 1 1 4 25.37 1.12 3.5106 0 2 0 2 26.55 20.32 3.3579 -1 1 3 4 27.62 29.16 3.2298 1 0 2 2 28.20 10.00 3.1640 0 1 3 4 29.28 10.99 3.0506 -1 2 1 4 30.03 4.53 2.9755 1 2 0 4 30.51 1.12 2.9296 0 2 2 4 30.93 50.13 2.8909 -1 2 2 4 31.70 1.10 2.8222 -2 1 2 4 31.98 4.66 2.7985 -2 1 1 4 33.67 29.83 2.6621 -2 1 3 4 34.69 5.32 2.5859 -1 2 3 4 37.56 1.99 2.3949 -2 1 4 4 37.60 27.37 2.3925 1 1 3 4 38.73 10.14 2.3247 2 1 1 4 38.88 17.59 2.3162 -2 2 2 4 39.42 9.43 2.2857 0 3 1 4 40.03 12.93 2.2523 -1 2 4 4 40.50 3.46 2.2275 -1 1 5 4 41.21 11.09 2.1907 2 2 0 4 41.26 13.07 2.1880 -1 3 1 4 41.82 1.60 2.1598 1 3 0 4 42.19 1.40 2.1421 0 3 2 4 42.39 5.61 2.1322 2 0 2 2 42.66 8.43 2.1192 0 2 4 4 42.93 10.43 2.1069 -2 1 5 4 43.46 5.38 2.0821 1 0 4 2 43.91 13.13 2.0620 -2 2 4 4 43.95 1.00 2.0601 -3 0 2 2 44.14 1.45 2.0517 1 3 1 4 44.52 7.91 2.0353 0 1 5 4 45.44 8.45 1.9962 -1 3 3 4 46.02 3.53 1.9721 -3 1 3 4 46.50 3.73 1.9530 0 3 3 4 46.69 1.66 1.9455 -1 0 6 2 47.45 1.90 1.9160 -3 1 1 4 48.72 2.23 1.8690 3 0 0 2 49.05 3.06 1.8571 -2 3 1 4 50.05 2.74 1.8224 2 2 2 4 50.25 2.71 1.8155 -2 3 3 4 50.82 1.58 1.7967 2 3 0 4 51.07 7.81 1.7885 -3 1 5 4 51.11 5.70 1.7870 2 1 3 4 51.43 5.88 1.7768 -3 2 2 4 52.06 2.14 1.7566 0 3 4 4 52.10 3.28 1.7553 0 4 0 2 53.16 4.96 1.7229 -3 2 4 4 53.17 1.43 1.7226 1 3 3 4 53.84 3.86 1.7028 1 1 5 4 53.88 5.77 1.7017 -1 2 6 4 53.99 1.47 1.6985 -3 0 6 2 54.04 3.92 1.6968 2 3 1 4 54.67 3.67 1.6789 -2 2 6 4 54.80 3.19 1.6752 1 4 0 4 54.97 2.33 1.6704 3 1 1 4 55.10 3.22 1.6668 0 4 2 4 55.36 1.91 1.6596 -1 4 2 4 55.42 1.72 1.6579 -1 3 5 4 55.68 2.35 1.6509 -3 1 6 4 55.72 7.15 1.6498 3 2 0 4 56.77 1.15 1.6218 -2 1 7 4 57.03 3.92 1.6149 2 0 4 2 57.17 1.80 1.6114 -1 1 7 4 57.36 1.15 1.6063 -2 3 5 4 58.33 6.35 1.5820 0 2 6 4 58.56 1.84 1.5762 2 3 2 4 58.66 3.30 1.5739 0 3 5 4 59.90 1.05 1.5441 -3 3 3 4 59.98 6.74 1.5423 1 4 2 4 60.03 1.36 1.5411 -4 0 4 2 60.56 1.48 1.5289 -3 2 6 4 60.70 1.22 1.5257 -4 0 2 2 60.72 1.00 1.5253 -2 4 2 4 61.10 2.14 1.5168 -3 3 1 4 61.26 1.11 1.5131 -4 1 3 4 61.42 1.96 1.5095 -3 1 7 4 62.57 1.58 1.4846 0 1 7 4 63.32 1.42 1.4687 -4 1 5 4 63.35 1.76 1.4682 -2 0 8 2 63.51 1.32 1.4648 0 4 4 4 64.18 1.35 1.4511 -3 3 5 4 64.22 1.46 1.4503 2 3 3 4 64.46 1.72 1.4455 -2 4 4 4 64.62 1.34 1.4423 -4 1 1 4 64.81 2.61 1.4385 -4 0 6 2 65.23 2.19 1.4303 3 2 2 4 66.60 1.47 1.4042 1 3 5 4 66.68 1.69 1.4027 -3 0 8 2 66.86 3.14 1.3992 -4 2 2 4 67.25 2.74 1.3922 0 5 1 4 67.35 1.56 1.3903 1 2 6 4 67.60 2.12 1.3858 3 3 1 4 68.53 1.33 1.3692 -1 5 1 4 69.34 2.62 1.3552 2 4 2 4 69.38 1.16 1.3545 -2 2 8 4 69.55 1.49 1.3516 -1 3 7 4 70.12 4.20 1.3420 1 4 4 4 70.55 1.15 1.3349 -4 1 7 4 70.78 2.59 1.3312 -1 2 8 4 72.62 2.28 1.3018 4 2 0 4 73.27 1.00 1.2920 -4 3 3 4 74.48 1.46 1.2739 -4 0 8 2 74.59 1.72 1.2724 2 0 6 2 75.31 1.02 1.2620 -2 5 3 4 76.37 1.10 1.2471 -4 3 1 4 76.66 1.45 1.2430 0 2 8 4 76.86 1.21 1.2404 -5 0 4 2 78.33 1.48 1.2206 -3 4 6 4 78.95 1.11 1.2126 -5 1 3 4 80.88 1.62 1.1885 2 4 4 4 81.95 1.05 1.1757 -4 3 7 4 83.09 1.04 1.1624 4 2 2 4 84.40 1.45 1.1477 -3 5 1 4 86.76 1.30 1.1225 1 2 8 4 87.72 1.45 1.1126 -4 4 6 4 89.42 1.13 1.0958 -3 4 8 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.