HfCl4(C4H8O)2 Duraj S A, Towns R L R, Baker R J, Schupp J Acta Crystallographica C46 (1990) 890-892 Structure of cis-tetrachlorobis(tetrahydrofuran)hafnium(IV) _database_code_amcsd 0010131 CELL PARAMETERS: 7.9140 12.8060 14.3570 90.000 90.000 90.000 SPACE GROUP: P2_12_12_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1455.034 Density (g/cm3): 2.047 MAX. ABS. INTENSITY / VOLUME**2: 23.62296137 RIR: 3.758 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.25 1.55 9.5567 0 1 1 4 12.33 11.71 7.1785 0 0 2 2 12.77 30.30 6.9308 1 0 1 4 13.15 50.74 6.7322 1 1 0 4 13.83 58.13 6.4030 0 2 0 2 14.14 100.00 6.2618 0 1 2 4 14.53 82.99 6.0953 1 1 1 4 15.15 2.11 5.8478 0 2 1 4 16.67 22.59 5.3170 1 0 2 4 18.06 4.27 4.9106 1 1 2 4 18.57 12.23 4.7783 0 2 2 4 18.87 33.45 4.7031 1 2 1 4 21.70 22.83 4.0951 1 0 3 4 21.73 11.69 4.0906 1 2 2 4 22.47 4.13 3.9570 2 0 0 2 22.80 2.59 3.9006 1 1 3 4 23.32 9.39 3.8148 2 0 1 4 23.68 1.67 3.7570 1 3 0 4 24.26 15.67 3.6690 0 3 2 4 24.35 5.86 3.6560 2 1 1 4 24.49 6.30 3.6346 1 3 1 4 25.71 11.68 3.4654 2 0 2 4 25.82 22.50 3.4499 1 2 3 4 26.48 2.14 3.3661 2 2 0 4 26.65 4.57 3.3451 2 1 2 4 26.78 6.07 3.3287 1 3 2 4 27.21 9.84 3.2772 2 2 1 4 27.28 1.09 3.2688 1 0 4 4 27.87 1.43 3.2015 0 4 0 2 28.51 7.76 3.1309 0 2 4 4 28.57 1.07 3.1248 0 4 1 4 30.12 13.87 2.9666 2 1 3 4 30.24 7.54 2.9551 1 3 3 4 30.71 8.01 2.9113 1 2 4 4 30.76 3.51 2.9064 1 4 1 4 31.45 2.14 2.8444 2 3 1 4 32.59 6.21 2.7472 0 3 4 4 32.65 2.60 2.7427 1 4 2 4 33.30 5.63 2.6904 2 3 2 4 33.94 4.62 2.6412 1 1 5 4 34.45 1.69 2.6030 2 1 4 4 34.56 2.23 2.5953 1 3 4 4 34.57 1.40 2.5946 3 0 1 4 34.72 6.23 2.5837 3 1 0 4 35.59 10.36 2.5222 1 4 3 4 36.20 10.52 2.4814 2 3 3 4 36.28 4.15 2.4761 3 0 2 4 36.60 2.91 2.4553 2 2 4 4 36.64 5.49 2.4523 2 4 1 4 36.98 2.79 2.4311 3 1 2 4 37.28 3.25 2.4123 0 5 2 4 37.40 1.26 2.4046 3 2 1 4 37.43 3.00 2.4024 1 5 1 4 37.65 6.08 2.3892 0 4 4 4 38.27 1.29 2.3516 2 4 2 4 38.75 5.31 2.3240 2 0 5 4 39.00 9.13 2.3094 3 2 2 4 39.04 3.82 2.3075 1 5 2 4 39.40 4.98 2.2872 1 4 4 4 39.50 10.39 2.2814 1 3 5 4 39.64 2.52 2.2736 3 1 3 4 39.99 2.09 2.2547 1 1 6 4 40.19 3.63 2.2441 3 3 0 4 40.23 2.54 2.2414 0 2 6 4 41.33 10.92 2.1846 2 2 5 4 42.35 1.10 2.1343 0 6 0 2 42.51 1.51 2.1264 2 5 1 4 42.53 2.73 2.1256 3 0 4 4 43.14 2.51 2.0969 3 1 4 4 43.40 2.89 2.0848 0 5 4 4 43.96 1.37 2.0597 2 5 2 4 44.27 1.32 2.0458 0 6 2 4 44.29 3.19 2.0453 2 4 4 4 44.83 1.17 2.0219 2 1 6 4 44.91 2.20 2.0182 1 3 6 4 44.93 3.20 2.0174 3 2 4 4 44.96 1.36 2.0161 1 5 4 4 45.70 1.19 1.9854 1 0 7 4 45.81 1.30 1.9807 1 6 2 4 46.29 3.57 1.9613 2 5 3 4 46.32 1.25 1.9600 4 0 1 4 46.36 5.34 1.9586 3 4 2 4 46.57 1.30 1.9503 2 2 6 4 47.43 3.48 1.9166 0 4 6 4 47.80 3.14 1.9028 3 3 4 4 47.97 2.47 1.8963 1 2 7 4 48.07 2.23 1.8927 1 6 3 4 48.14 1.79 1.8903 4 2 0 4 48.24 2.46 1.8866 4 1 2 4 48.40 4.60 1.8807 2 4 5 4 48.58 2.14 1.8741 4 2 1 4 48.90 2.58 1.8626 2 6 1 4 49.03 3.99 1.8579 1 5 5 4 49.61 2.05 1.8376 3 5 0 4 50.42 2.43 1.8101 4 1 3 4 50.63 3.64 1.8028 2 1 7 4 50.71 1.49 1.8002 1 3 7 4 51.25 1.00 1.7824 1 7 0 4 51.29 1.58 1.7812 4 3 1 4 51.41 2.01 1.7773 0 1 8 4 51.55 1.02 1.7728 0 7 2 4 51.61 1.38 1.7709 3 4 4 4 51.68 2.12 1.7688 1 7 1 4 52.10 2.83 1.7556 3 1 6 4 52.23 1.19 1.7515 2 2 7 4 52.55 1.56 1.7414 4 3 2 4 53.09 1.07 1.7250 2 4 6 4 54.37 1.16 1.6873 1 4 7 4 54.52 1.19 1.6830 4 4 0 4 54.60 1.14 1.6807 4 3 3 4 54.81 2.31 1.6749 2 3 7 4 54.93 1.58 1.6716 4 4 1 4 55.72 1.12 1.6496 2 7 1 4 56.20 1.81 1.6369 3 3 6 4 56.24 1.27 1.6357 3 5 4 4 56.48 1.01 1.6292 4 0 5 4 56.96 1.96 1.6166 3 6 2 4 58.45 1.03 1.5789 4 2 5 4 58.74 1.32 1.5720 2 6 5 4 59.07 1.04 1.5638 1 0 9 4 61.73 1.01 1.5027 5 0 3 4 62.59 1.08 1.4841 2 5 7 4 62.60 1.01 1.4838 3 0 8 4 62.96 1.36 1.4762 5 3 1 4 63.60 1.59 1.4630 5 2 3 4 64.05 1.12 1.4537 1 6 7 4 64.46 1.40 1.4455 3 2 8 4 68.03 1.57 1.3781 5 1 5 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.