[Co(H2O)6]Cl2.2C6H12N4.4H2O Ganesh V, Seshasayee M, Aravamudan G, Heijdenrijk D, Schenk H Acta Crystallographica C46 (1990) 949-951 Structure of hexaaquacobalt(II) dichloride bis(hexamethylenetetramine)* tetrahydrate _database_code_amcsd 0010132 CELL PARAMETERS: 9.5080 9.4280 9.3090 78.860 105.080 120.130 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 694.910 Density (g/cm3): 1.305 MAX. ABS. INTENSITY / VOLUME**2: 3.467227434 RIR: 0.865 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.87 88.85 8.9631 0 0 1 2 11.17 1.31 7.9186 -1 1 0 2 12.83 36.88 6.8972 -1 1 1 2 14.15 3.30 6.2604 0 1 1 2 15.25 62.32 5.8095 0 -1 1 2 16.13 100.00 5.4948 1 0 1 2 16.77 3.06 5.2874 1 -1 1 2 18.83 28.62 4.7134 1 1 0 2 19.20 32.83 4.6230 -1 2 0 2 19.29 39.09 4.6010 -2 1 1 2 19.34 12.71 4.5892 -2 1 0 2 19.81 10.07 4.4816 0 0 2 2 19.81 19.15 4.4809 -1 2 1 2 20.05 48.54 4.4286 -1 1 2 2 20.68 24.44 4.2954 -1 -1 1 2 20.74 4.67 4.2831 -1 0 2 2 21.86 13.90 4.0656 0 2 0 2 22.04 8.10 4.0327 -2 2 1 2 22.36 12.16 3.9767 -2 0 1 2 22.46 7.41 3.9593 -2 2 0 2 23.34 16.21 3.8116 0 2 1 2 23.37 19.42 3.8061 0 -1 2 2 23.98 1.79 3.7108 2 -1 1 2 24.50 15.85 3.6326 1 0 2 2 24.71 3.64 3.6023 0 -2 1 2 25.83 7.55 3.4486 -2 2 2 2 26.48 1.63 3.3656 -1 -1 2 2 26.74 3.39 3.3344 -2 0 2 2 26.89 11.32 3.3152 2 -2 1 2 28.52 10.63 3.1302 0 2 2 2 28.77 11.76 3.1026 -3 2 1 2 28.92 3.31 3.0873 1 2 0 2 29.02 8.96 3.0771 2 1 0 2 29.05 4.73 3.0736 -1 1 3 2 29.34 1.01 3.0446 -1 3 0 2 29.47 10.79 3.0311 -1 3 1 2 29.59 7.27 3.0189 -3 1 0 2 29.82 1.10 2.9957 -1 0 3 2 29.84 3.73 2.9947 -3 2 0 2 29.91 2.17 2.9877 0 0 3 2 30.78 7.79 2.9047 0 -2 2 2 31.11 3.31 2.8750 0 1 3 2 31.13 7.00 2.8729 -3 2 2 2 31.33 8.74 2.8553 2 -1 2 2 31.83 1.32 2.8113 -2 3 2 2 31.85 1.67 2.8101 2 1 1 2 32.34 4.10 2.7680 -1 2 3 2 32.48 1.52 2.7569 -2 2 3 2 32.51 8.13 2.7543 1 -3 1 2 32.59 1.29 2.7474 2 0 2 2 32.70 4.41 2.7387 0 -1 3 2 32.87 1.56 2.7247 -3 0 1 2 33.31 1.60 2.6900 3 0 0 2 33.31 1.89 2.6895 -2 -1 2 2 33.55 2.79 2.6709 3 -1 1 2 33.83 1.03 2.6500 0 3 1 2 35.46 6.06 2.5311 -3 0 2 2 36.31 2.29 2.4744 -3 2 3 2 36.68 2.86 2.4500 3 0 1 2 36.81 2.48 2.4417 -3 1 3 2 37.29 1.65 2.4115 -2 3 3 2 37.35 3.32 2.4073 2 1 2 2 37.47 3.36 2.4003 0 3 2 2 37.97 2.09 2.3695 3 -3 1 2 38.19 2.24 2.3567 2 2 0 2 38.78 2.22 2.3222 -1 3 3 2 38.96 1.50 2.3115 -2 4 0 2 39.46 1.05 2.2833 -4 1 1 2 39.48 7.60 2.2827 -2 -1 3 2 39.86 1.04 2.2618 -3 -1 1 2 40.25 4.58 2.2408 0 0 4 2 40.48 5.07 2.2281 3 -2 2 2 40.58 2.32 2.2229 -3 0 3 2 40.62 1.26 2.2212 -4 1 0 2 40.97 2.14 2.2030 0 1 4 2 41.09 4.78 2.1967 -3 4 2 2 41.11 2.52 2.1957 -4 3 0 2 41.21 1.70 2.1907 -1 -3 1 2 41.72 4.69 2.1650 -1 -2 3 2 42.07 2.87 2.1477 -2 -2 2 2 42.20 3.91 2.1415 -2 0 4 2 42.40 1.50 2.1317 2 -2 3 2 42.45 1.16 2.1293 1 2 3 2 42.59 3.13 2.1228 -1 4 2 2 42.72 1.02 2.1164 3 1 1 2 42.92 3.35 2.1072 1 -4 1 2 43.17 4.81 2.0954 4 -2 1 2 43.36 4.03 2.0868 0 3 3 2 43.44 2.11 2.0833 -3 2 4 2 44.07 3.12 2.0547 -4 0 1 2 44.10 3.42 2.0536 -4 3 3 2 44.14 2.04 2.0517 3 -3 2 2 44.20 2.38 2.0493 -4 4 1 2 44.23 1.92 2.0478 4 -1 1 2 44.57 3.74 2.0328 0 4 0 2 44.60 1.51 2.0316 -2 3 4 2 44.63 2.20 2.0303 -2 4 3 2 44.71 2.09 2.0271 2 1 3 2 44.83 1.97 2.0219 1 -1 4 2 44.89 1.73 2.0191 -3 4 3 2 44.98 1.44 2.0153 0 4 1 2 45.02 1.72 2.0138 -1 -3 2 2 45.84 1.04 1.9796 -4 4 0 2 46.40 3.14 1.9571 -1 3 4 2 47.46 1.32 1.9156 -2 -2 3 2 47.65 1.16 1.9087 3 1 2 2 47.66 1.62 1.9080 2 -4 2 2 47.76 1.67 1.9042 3 -1 3 2 47.79 1.09 1.9031 0 -2 4 2 48.49 1.86 1.8774 3 -2 3 2 48.74 1.12 1.8682 -3 -2 1 2 49.10 1.08 1.8554 4 -2 2 2 49.81 2.73 1.8308 -3 5 0 2 49.95 1.56 1.8259 -1 0 5 2 50.06 1.30 1.8220 -2 2 5 2 50.85 1.61 1.7956 -5 1 1 2 50.91 1.54 1.7936 -2 4 4 2 51.19 1.89 1.7844 -4 5 1 2 51.70 1.15 1.7682 -4 5 2 2 52.71 1.52 1.7365 -3 5 3 2 53.02 1.05 1.7271 -5 4 0 2 53.47 1.20 1.7137 -3 -1 4 2 53.77 2.19 1.7047 -3 3 5 2 54.04 1.22 1.6970 5 -3 1 2 55.10 1.52 1.6667 0 -3 4 2 56.77 1.42 1.6216 0 5 1 2 58.46 1.60 1.5788 3 0 4 2 58.78 1.63 1.5708 2 2 4 2 61.73 1.21 1.5026 -6 2 3 2 62.14 1.02 1.4939 0 0 6 2 64.30 1.10 1.4486 1 -3 5 2 71.97 1.19 1.3120 -3 2 7 2 72.25 1.02 1.3076 2 5 0 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.