Na2Th(SO4)3(H2O)3.3H2O Habash J, Smith A J Acta Crystallographica C46 (1990) 957-960 Structure of disodium triaquatri-u-sulfato-thorate(IV) trihydrate _database_code_amcsd 0010135 CELL PARAMETERS: 5.5670 16.8100 15.7600 90.000 91.925 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1474.008 Density (g/cm3): 2.984 MAX. ABS. INTENSITY / VOLUME**2: 29.67225619 RIR: 3.238 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.69 5.91 11.4938 0 1 1 4 10.53 29.67 8.4050 0 2 0 2 11.24 98.65 7.8756 0 0 2 2 11.93 100.00 7.4153 0 2 1 4 15.42 29.01 5.7469 0 2 2 4 16.78 3.54 5.2820 1 1 0 4 17.54 18.28 5.0568 -1 1 1 4 17.70 1.70 5.0116 0 1 3 4 17.88 9.60 4.9605 1 1 1 4 19.13 3.49 4.6394 1 2 0 4 19.22 5.69 4.6179 -1 0 2 2 19.44 4.91 4.5657 0 3 2 4 19.80 1.23 4.4846 -1 2 1 4 19.94 16.27 4.4530 0 2 3 4 19.94 9.86 4.4530 -1 1 2 4 20.10 7.60 4.4170 1 2 1 4 20.54 12.96 4.3235 1 1 2 4 21.14 4.70 4.2025 0 4 0 2 21.89 11.03 4.0605 0 4 1 4 22.51 2.62 3.9493 1 2 2 4 22.52 34.44 3.9481 1 3 0 4 22.58 5.34 3.9378 0 0 4 2 23.09 1.21 3.8514 -1 3 1 4 23.51 18.58 3.7846 -1 1 3 4 24.00 3.39 3.7077 0 4 2 4 24.28 24.51 3.6657 1 1 3 4 24.97 8.25 3.5658 0 2 4 4 24.99 42.57 3.5636 -1 3 2 4 25.26 1.83 3.5260 -1 2 3 4 25.48 37.12 3.4962 1 3 2 4 25.98 2.07 3.4293 1 2 3 4 27.18 7.89 3.2809 0 4 3 4 27.30 12.92 3.2665 1 4 1 4 27.30 12.66 3.2664 -1 0 4 2 27.82 6.12 3.2064 -1 1 4 4 28.71 12.26 3.1099 1 1 4 4 28.83 2.07 3.0963 0 1 5 4 28.87 2.29 3.0920 0 5 2 4 29.15 1.08 3.0631 1 4 2 4 29.34 2.10 3.0445 -1 2 4 4 30.30 7.28 2.9498 0 2 5 4 31.08 7.19 2.8775 1 5 0 4 31.13 1.42 2.8735 0 4 4 4 31.51 8.61 2.8394 -1 5 1 4 31.60 2.29 2.8313 0 5 3 4 31.71 1.77 2.8220 1 5 1 4 31.71 15.79 2.8219 -1 3 4 4 31.94 10.90 2.8017 0 6 0 2 31.96 7.79 2.8005 1 4 3 4 32.18 9.98 2.7819 2 0 0 2 32.49 4.27 2.7554 1 3 4 4 32.63 1.80 2.7446 2 1 0 4 32.63 3.29 2.7444 -1 1 5 4 32.94 5.21 2.7191 -2 1 1 4 32.95 6.66 2.7180 -1 5 2 4 33.32 3.80 2.6888 2 1 1 4 33.34 1.35 2.6877 1 5 2 4 33.59 8.38 2.6684 1 1 5 4 33.81 5.42 2.6512 -2 0 2 2 33.94 2.38 2.6410 2 2 0 4 33.96 7.61 2.6396 0 6 2 4 34.15 4.52 2.6252 0 0 6 2 34.24 1.18 2.6188 -2 1 2 4 34.25 2.06 2.6183 -2 2 1 4 34.55 1.55 2.5958 2 0 2 2 34.62 3.89 2.5912 2 2 1 4 35.31 3.03 2.5420 -1 5 3 4 35.51 1.48 2.5279 1 4 4 4 35.62 9.34 2.5207 0 4 5 4 35.84 6.88 2.5058 0 2 6 4 35.85 5.33 2.5051 1 5 3 4 36.22 1.83 2.4803 2 2 2 4 37.47 1.91 2.3999 2 1 3 4 37.53 4.49 2.3965 -2 3 2 4 37.63 1.55 2.3901 -2 2 3 4 37.78 4.81 2.3813 -1 1 6 4 37.89 1.71 2.3745 1 6 2 4 38.42 2.62 2.3428 -1 5 4 4 38.79 3.35 2.3215 1 1 6 4 38.82 1.70 2.3196 -1 4 5 4 39.01 1.42 2.3090 -2 0 4 2 39.09 4.14 2.3043 1 5 4 4 39.09 3.37 2.3043 -2 4 1 4 39.22 1.76 2.2970 0 7 2 4 39.39 1.85 2.2875 -2 1 4 4 39.42 5.15 2.2858 2 4 1 4 39.47 3.23 2.2828 0 6 4 4 40.32 2.67 2.2370 2 0 4 2 40.52 2.27 2.2265 0 4 6 4 40.52 1.86 2.2265 -2 2 4 4 40.82 3.53 2.2105 -1 3 6 4 40.93 1.98 2.2048 1 7 0 4 41.27 5.26 2.1875 -1 7 1 4 41.43 6.11 2.1796 1 7 1 4 41.55 3.64 2.1736 0 2 7 4 41.77 5.97 2.1624 1 3 6 4 41.79 1.12 2.1617 2 2 4 4 42.14 2.42 2.1442 -2 4 3 4 42.16 3.26 2.1432 -1 5 5 4 42.34 2.35 2.1348 -2 3 4 4 42.43 1.09 2.1306 -1 7 2 4 42.51 2.87 2.1266 -1 6 4 4 42.72 2.63 2.1164 2 5 1 4 42.73 1.40 2.1159 1 7 2 4 42.94 6.84 2.1064 1 5 5 4 42.98 3.31 2.1042 -2 1 5 4 43.05 1.88 2.1012 0 8 0 2 43.07 1.60 2.1002 2 4 3 4 43.20 3.77 2.0944 -1 1 7 4 43.45 3.50 2.0828 0 8 1 4 43.56 4.72 2.0775 2 3 4 4 44.03 2.24 2.0564 -2 2 5 4 44.07 1.50 2.0547 2 5 2 4 44.25 4.54 2.0467 1 1 7 4 44.35 3.62 2.0426 -1 7 3 4 44.63 2.58 2.0302 0 8 2 4 44.79 3.14 2.0236 -2 4 4 4 44.79 4.79 2.0233 1 7 3 4 45.52 3.71 1.9928 2 2 5 4 45.74 6.68 1.9837 0 4 7 4 45.97 4.12 1.9741 2 6 0 4 46.10 1.12 1.9689 0 0 8 2 46.16 1.17 1.9666 2 5 3 4 46.41 1.31 1.9564 -1 5 6 4 46.55 3.05 1.9508 0 8 3 4 46.77 1.15 1.9421 -2 0 6 2 47.20 5.99 1.9257 -2 6 2 4 47.43 1.57 1.9170 0 2 8 4 47.46 6.41 1.9156 0 6 6 4 47.77 3.72 1.9042 2 6 2 4 48.05 3.70 1.8934 -2 4 5 4 48.08 1.98 1.8923 -2 2 6 4 49.12 1.49 1.8546 3 0 0 2 49.44 2.65 1.8434 2 4 5 4 49.68 3.71 1.8350 -2 3 6 4 49.75 2.10 1.8329 2 2 6 4 50.01 1.12 1.8239 3 1 1 4 50.19 2.39 1.8178 -1 7 5 4 50.41 1.47 1.8104 -2 7 1 4 50.68 3.03 1.8013 2 7 1 4 50.86 3.40 1.7952 1 7 5 4 50.91 1.42 1.7938 -2 5 5 4 50.94 2.78 1.7925 3 2 1 4 50.96 1.79 1.7919 3 0 2 2 51.09 1.38 1.7877 -1 5 7 4 51.24 2.16 1.7829 0 4 8 4 51.27 3.02 1.7818 -2 6 4 4 51.27 1.12 1.7818 3 1 2 4 51.31 1.56 1.7807 2 3 6 4 51.36 3.63 1.7790 -1 3 8 4 51.62 1.65 1.7707 1 9 0 4 51.67 1.92 1.7691 -2 1 7 4 51.93 1.95 1.7607 3 3 0 4 52.20 1.08 1.7525 3 2 2 4 52.24 1.40 1.7511 2 5 5 4 52.34 1.52 1.7481 2 6 4 4 52.34 1.19 1.7481 0 8 5 4 52.42 3.36 1.7454 1 3 8 4 52.58 1.36 1.7404 -2 2 7 4 52.88 2.15 1.7315 -1 9 2 4 52.92 3.61 1.7301 -3 3 2 4 52.94 2.98 1.7296 -3 2 3 4 53.14 2.87 1.7236 1 9 2 4 53.21 1.83 1.7215 3 1 3 4 53.48 1.85 1.7134 0 2 9 4 53.72 1.56 1.7062 2 7 3 4 53.93 2.16 1.7000 -3 0 4 2 54.11 2.15 1.6950 3 2 3 4 54.19 1.15 1.6925 -3 4 1 4 54.40 3.00 1.6864 2 2 7 4 54.58 2.58 1.6815 3 4 1 4 54.72 2.62 1.6774 -1 1 9 4 54.75 2.07 1.6767 2 8 0 4 54.93 4.30 1.6715 0 10 1 4 55.21 1.81 1.6637 2 8 1 4 55.83 1.06 1.6468 -2 8 2 4 55.87 2.62 1.6457 1 1 9 4 56.57 1.13 1.6268 -3 3 4 4 56.78 3.44 1.6214 -1 9 4 4 57.00 1.91 1.6156 0 4 9 4 57.18 2.33 1.6109 0 6 8 4 57.28 2.67 1.6085 1 9 4 4 57.57 1.06 1.6009 0 10 3 4 57.60 1.56 1.6002 3 4 3 4 57.76 1.80 1.5961 -2 6 6 4 57.89 2.78 1.5930 2 4 7 4 58.19 1.43 1.5854 -1 7 7 4 58.32 1.03 1.5822 2 0 8 2 58.61 1.31 1.5751 0 0 10 2 58.90 1.14 1.5679 -2 3 8 4 59.05 1.18 1.5645 1 7 7 4 59.23 1.22 1.5600 2 6 6 4 59.24 1.04 1.5597 2 7 5 4 59.80 1.35 1.5465 3 6 0 4 60.26 1.73 1.5358 0 8 7 4 61.25 1.03 1.5134 -3 4 5 4 61.54 1.87 1.5069 -1 5 9 4 62.60 1.35 1.4839 1 5 9 4 62.64 1.66 1.4831 0 10 5 4 63.01 1.39 1.4751 -1 3 10 4 63.09 1.06 1.4736 1 11 0 4 63.71 1.50 1.4607 1 9 6 4 64.07 1.53 1.4534 -3 6 4 4 64.18 1.24 1.4511 1 3 10 4 64.20 1.92 1.4508 -1 11 2 4 65.65 1.51 1.4221 -1 11 3 4 66.00 1.03 1.4155 1 11 3 4 66.21 1.63 1.4116 0 2 11 4 67.58 1.06 1.3862 4 1 0 4 67.65 2.26 1.3849 -4 1 1 4 67.94 1.55 1.3797 -1 7 9 4 68.10 1.27 1.3769 4 1 1 4 68.43 1.55 1.3710 1 1 11 4 68.95 1.20 1.3620 1 7 9 4 69.33 1.32 1.3554 0 4 11 4 69.70 1.15 1.3491 -3 6 6 4 69.84 1.87 1.3467 0 10 7 4 71.24 1.35 1.3236 -1 9 8 4 71.48 1.09 1.3198 0 12 4 4 73.40 1.06 1.2900 -4 3 4 4 76.92 1.01 1.2394 3 10 1 4 77.19 1.43 1.2359 0 12 6 4 78.63 1.25 1.2168 -4 3 6 4 80.15 1.29 1.1975 4 7 1 4 81.17 1.08 1.1849 4 3 6 4 85.97 1.03 1.1307 -4 3 8 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.