K3V2F3O8HF.2H2O Lapshin A E, Smolin Y I, Shepelev Y F, Schwendt P, Gyepesova D Acta Crystallographica C46 (1990) 1753-1755 Structure of tripotassium u-fluoro-u-peroxo-bis(fluorooxoperoxovanadate)(3-) hydrogen fluoride dihydrate _database_code_amcsd 0010178 CELL PARAMETERS: 8.5180 12.4600 5.9810 92.300 90.900 102.700 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 618.564 Density (g/cm3): 2.488 MAX. ABS. INTENSITY / VOLUME**2: 9.094431582 RIR: 1.190 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.28 100.00 12.1430 0 1 0 2 10.65 10.45 8.3070 1 0 0 2 11.50 19.81 7.6928 -1 1 0 2 14.18 16.35 6.2440 1 1 0 2 14.59 25.54 6.0715 0 2 0 2 14.83 11.04 5.9743 0 0 1 2 16.07 3.46 5.5159 -1 2 0 2 16.24 50.28 5.4581 0 -1 1 2 16.83 18.07 5.2682 0 1 1 2 18.07 17.21 4.9091 -1 0 1 2 18.51 13.93 4.7934 1 0 1 2 18.85 1.78 4.7071 -1 1 1 2 19.93 4.74 4.4557 1 2 0 2 20.14 8.23 4.4099 -1 -1 1 2 21.33 1.71 4.1664 0 2 1 2 21.39 3.27 4.1535 2 0 0 2 21.67 3.49 4.1018 1 -2 1 2 21.96 28.29 4.0477 0 3 0 2 22.19 2.56 4.0053 -1 2 1 2 22.21 1.86 4.0032 -1 3 0 2 23.12 15.90 3.8464 -2 2 0 2 24.13 6.29 3.6886 2 1 0 2 24.36 2.51 3.6537 -1 -2 1 2 25.49 3.50 3.4950 1 2 1 2 25.70 30.51 3.4665 -2 1 1 2 25.81 5.03 3.4512 -2 0 1 2 25.95 11.43 3.4338 2 -1 1 2 26.03 31.27 3.4228 0 -3 1 2 26.40 5.18 3.3760 1 -3 1 2 26.44 21.85 3.3708 2 0 1 2 26.54 4.49 3.3585 1 3 0 2 27.16 27.39 3.2836 0 3 1 2 27.52 4.89 3.2415 2 -2 1 2 28.59 4.23 3.1220 2 2 0 2 29.00 1.80 3.0788 -1 4 0 2 29.90 6.55 2.9886 -1 -3 1 2 29.91 2.92 2.9871 0 0 2 2 30.50 10.60 2.9312 0 -1 2 2 30.86 4.00 2.8976 2 -3 1 2 31.30 1.41 2.8579 -2 3 1 2 31.51 3.00 2.8389 -3 1 0 2 31.57 6.30 2.8337 -1 0 2 2 31.78 2.17 2.8158 -2 -2 1 2 32.09 4.41 2.7893 1 -1 2 2 32.10 1.28 2.7887 1 0 2 2 32.20 1.32 2.7799 -1 1 2 2 32.33 1.55 2.7690 3 0 0 2 32.44 2.24 2.7598 -3 2 0 2 32.46 14.48 2.7579 -2 4 0 2 32.48 4.12 2.7566 0 -4 1 2 34.04 1.53 2.6341 0 2 2 2 34.17 4.62 2.6238 2 3 0 2 34.78 1.87 2.5791 3 1 0 2 35.38 2.00 2.5367 -3 0 1 2 35.77 2.64 2.5099 -3 2 1 2 36.17 2.29 2.4833 -1 5 0 2 36.20 6.41 2.4815 -2 4 1 2 36.58 2.91 2.4565 0 -3 2 2 36.67 1.87 2.4509 -2 1 2 2 36.79 3.83 2.4430 -2 -3 1 2 36.97 8.80 2.4317 1 -3 2 2 37.02 2.15 2.4286 0 5 0 2 37.57 1.85 2.3941 1 4 1 2 38.05 2.39 2.3650 2 -2 2 2 38.07 4.28 2.3636 2 3 1 2 38.08 3.61 2.3633 -2 -1 2 2 38.24 2.22 2.3538 0 3 2 2 38.24 7.63 2.3535 -2 2 2 2 38.47 11.71 2.3400 3 1 1 2 38.59 8.87 2.3328 -2 5 0 2 38.60 5.81 2.3325 3 2 0 2 38.89 1.93 2.3160 -3 4 0 2 39.50 9.24 2.2816 2 1 2 2 40.49 2.30 2.2278 2 4 0 2 40.49 1.88 2.2278 2 -3 2 2 40.73 4.02 2.2155 0 5 1 2 40.93 3.83 2.2050 -2 -2 2 2 40.95 1.32 2.2037 1 5 0 2 40.99 2.72 2.2016 -3 -2 1 2 41.19 4.12 2.1918 -2 3 2 2 42.02 5.86 2.1500 -3 4 1 2 42.13 2.54 2.1451 3 2 1 2 42.51 9.82 2.1265 -4 1 0 2 42.76 3.63 2.1145 2 2 2 2 42.80 3.88 2.1129 -4 2 0 2 43.07 1.03 2.1000 -1 -5 1 2 43.48 1.00 2.0813 3 3 0 2 43.63 1.20 2.0744 -1 6 0 2 43.82 7.19 2.0658 -3 5 0 2 44.16 2.54 2.0509 2 -4 2 2 44.45 2.84 2.0383 -1 -4 2 2 44.78 1.33 2.0238 0 6 0 2 44.95 4.59 2.0167 -2 -3 2 2 45.28 8.48 2.0026 -2 4 2 2 45.31 1.49 2.0016 -2 6 0 2 45.73 1.46 1.9841 1 -6 1 2 45.93 1.82 1.9759 4 1 0 2 46.66 1.04 1.9465 4 0 1 2 46.74 1.85 1.9434 0 -6 1 2 46.82 5.07 1.9404 3 3 1 2 47.12 2.82 1.9289 2 3 2 2 47.32 2.85 1.9211 3 1 2 2 47.33 2.13 1.9207 -1 -1 3 2 47.40 1.25 1.9178 0 -2 3 2 48.05 1.64 1.8936 -4 -1 1 2 48.21 1.82 1.8875 1 -2 3 2 48.59 3.28 1.8736 -3 -2 2 2 48.60 2.03 1.8735 1 6 0 2 48.76 6.06 1.8677 0 2 3 2 48.84 3.56 1.8648 2 -5 2 2 49.19 2.11 1.8524 3 4 0 2 49.89 1.81 1.8280 -4 4 1 2 50.31 1.23 1.8136 -2 0 3 2 50.56 1.23 1.8051 3 2 2 2 51.10 1.01 1.7875 1 2 3 2 51.57 2.68 1.7721 2 -2 3 2 51.67 1.97 1.7692 3 -6 1 2 52.08 1.93 1.7561 0 3 3 2 52.29 2.12 1.7496 -1 -3 3 2 52.42 2.29 1.7456 -3 6 1 2 52.49 1.31 1.7434 -2 7 0 2 52.52 1.14 1.7423 -3 -3 2 2 52.77 1.54 1.7347 0 7 0 2 53.53 1.20 1.7118 -2 -2 3 2 53.88 2.57 1.7015 4 3 0 2 53.92 1.83 1.7003 0 -4 3 2 54.44 1.13 1.6854 4 0 2 2 54.49 2.16 1.6840 -3 5 2 2 54.91 1.16 1.6720 -5 3 0 2 56.00 2.52 1.6422 -3 1 3 2 56.01 1.76 1.6418 0 6 2 2 56.33 1.86 1.6334 -1 -4 3 2 56.33 1.60 1.6331 2 -4 3 2 56.67 1.23 1.6242 5 -1 1 2 57.11 2.57 1.6129 -3 -5 1 2 57.70 2.72 1.5978 3 0 3 2 57.75 1.26 1.5965 -2 4 3 2 58.54 1.17 1.5767 3 -3 3 2 58.59 1.10 1.5756 3 5 1 2 58.72 1.50 1.5724 -3 7 1 2 58.86 1.05 1.5690 -3 3 3 2 59.19 1.51 1.5610 4 4 0 2 59.27 1.09 1.5590 5 -4 1 2 60.94 1.24 1.5202 1 -8 1 2 61.52 1.09 1.5072 0 5 3 2 61.68 1.63 1.5038 2 -8 1 2 62.08 1.86 1.4951 4 4 1 2 62.15 1.58 1.4936 0 0 4 2 62.29 2.10 1.4905 0 -1 4 2 63.26 1.63 1.4700 -3 -3 3 2 63.83 2.44 1.4583 -1 -7 2 2 64.99 1.17 1.4349 2 -6 3 2 66.23 1.49 1.4111 -6 1 0 2 69.12 1.30 1.3590 -5 7 0 2 73.40 1.85 1.2900 -2 7 3 2 76.39 1.18 1.2468 1 9 1 2 77.01 1.03 1.2383 -3 -3 4 2 78.54 1.07 1.2179 -3 -6 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.