K2[Fe(CN)5NO].0.8H2O Marsh R E Acta Crystallographica C46 (1990) 1761-1763 On the structure of 'potassium nitroprusside 0.8 hydrate' _database_code_amcsd 0010183 CELL PARAMETERS: 30.0000 11.2720 16.0530 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 5428.482 Density (g/cm3): 1.850 MAX. ABS. INTENSITY / VOLUME**2: 4.779514095 RIR: 0.841 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.89 1.32 15.0000 2 0 0 2 6.24 2.35 14.1540 1 0 1 4 8.07 5.34 10.9600 2 0 1 4 9.59 3.91 9.2250 0 1 1 4 9.82 5.20 9.0113 2 1 0 4 10.03 10.95 8.8175 1 1 1 8 11.02 60.28 8.0265 0 0 2 2 11.41 16.69 7.7538 1 0 2 4 11.80 21.14 7.5000 4 0 0 2 12.51 15.06 7.0770 2 0 2 4 13.03 1.91 6.7950 4 0 1 4 13.06 15.46 6.7805 3 1 1 8 13.86 1.04 6.3883 1 1 2 8 14.15 2.28 6.2595 3 0 2 4 15.23 1.88 5.8194 4 1 1 8 15.72 9.85 5.6360 0 2 0 2 15.77 2.40 5.6203 5 0 1 4 16.17 22.55 5.4800 4 0 2 4 16.80 5.82 5.2759 2 2 0 4 16.83 1.16 5.2679 1 0 3 4 17.63 1.88 5.0297 5 1 1 8 17.70 3.96 5.0121 2 2 1 8 17.74 1.00 5.0000 6 0 0 2 18.00 2.22 4.9284 4 1 2 8 18.35 2.98 4.8340 0 1 3 4 18.46 1.32 4.8057 5 0 2 4 18.59 1.62 4.7724 1 1 3 8 19.24 11.94 4.6125 0 2 2 4 19.29 3.25 4.6010 2 1 3 8 19.70 52.63 4.5056 4 2 0 4 20.09 3.63 4.4207 5 1 2 8 20.14 3.16 4.4087 2 2 2 8 20.20 5.60 4.3958 6 1 1 8 20.47 1.46 4.3380 4 2 1 8 20.93 13.31 4.2439 6 0 2 4 22.15 34.09 4.0132 0 0 4 2 22.26 1.41 3.9935 5 0 3 4 22.35 9.16 3.9778 1 0 4 4 22.63 100.00 3.9289 4 2 2 8 22.94 1.79 3.8769 2 0 4 4 23.11 3.86 3.8485 1 2 3 8 23.64 7.41 3.7643 5 1 3 8 23.68 1.09 3.7569 2 2 3 8 23.73 15.43 3.7500 8 0 0 2 23.89 2.07 3.7245 3 0 4 4 24.51 2.67 3.6316 1 3 1 8 24.61 2.18 3.6177 3 2 3 8 24.84 7.79 3.5843 7 1 2 8 25.17 2.63 3.5385 4 0 4 4 26.29 5.14 3.3902 6 2 2 8 26.87 1.76 3.3186 2 3 2 8 27.37 3.00 3.2585 5 2 3 8 27.82 7.75 3.2069 7 1 3 8 27.93 15.88 3.1942 2 2 4 8 28.43 2.79 3.1395 2 0 5 4 28.47 4.68 3.1350 9 1 1 8 28.59 4.19 3.1221 8 2 0 4 28.73 4.37 3.1073 3 2 4 8 29.04 1.97 3.0750 0 3 3 4 29.19 4.24 3.0590 1 3 3 8 29.78 8.90 3.0000 10 0 0 2 29.81 3.39 2.9968 4 2 4 8 30.09 2.74 2.9697 9 1 2 8 30.16 2.43 2.9630 8 1 3 8 30.29 1.04 2.9503 3 1 5 8 30.41 4.37 2.9392 3 3 3 8 30.52 2.78 2.9294 7 0 4 4 30.73 8.25 2.9097 8 2 2 8 31.09 3.44 2.8766 7 2 3 8 31.33 7.36 2.8553 4 1 5 8 31.44 1.98 2.8451 4 3 3 8 31.56 3.84 2.8352 7 1 4 8 31.61 1.22 2.8308 5 0 5 4 31.75 12.47 2.8180 0 4 0 2 32.17 2.73 2.7825 7 3 1 8 32.65 1.18 2.7427 2 2 5 8 32.68 12.57 2.7400 8 0 4 4 32.73 82.44 2.7365 5 3 3 8 32.85 1.27 2.7267 10 1 2 8 33.34 1.11 2.6871 3 2 5 8 33.49 23.74 2.6755 0 0 6 2 33.63 4.41 2.6650 7 3 2 8 33.63 8.45 2.6649 1 0 6 4 33.71 1.61 2.6589 0 4 2 4 33.85 3.93 2.6482 10 2 0 4 34.23 1.20 2.6193 6 3 3 8 34.24 1.55 2.6187 8 3 1 8 34.25 1.14 2.6181 2 4 2 8 34.29 3.04 2.6154 11 1 1 8 34.59 3.31 2.5934 1 1 6 8 35.21 1.22 2.5490 10 1 3 8 35.50 2.81 2.5286 9 2 3 8 35.63 1.10 2.5200 8 3 2 8 35.63 1.10 2.5200 4 0 6 4 35.83 11.07 2.5061 4 4 2 8 35.92 1.23 2.5003 9 1 4 8 35.92 4.10 2.5000 12 0 0 2 36.46 1.68 2.4642 8 2 4 8 36.47 6.22 2.4640 9 3 1 8 36.82 1.34 2.4409 0 3 5 4 37.69 5.74 2.3869 12 0 2 4 37.74 1.05 2.3837 8 1 5 8 37.78 1.81 2.3813 9 3 2 8 37.94 2.85 2.3713 3 3 5 8 38.15 1.68 2.3590 6 0 6 4 38.31 1.42 2.3493 3 2 6 8 38.34 7.79 2.3476 6 4 2 8 38.55 1.82 2.3351 12 1 2 8 38.80 1.13 2.3210 4 3 5 8 38.99 1.26 2.3102 7 3 4 8 39.06 7.80 2.3062 0 4 4 4 39.16 10.50 2.3005 4 2 6 8 39.71 1.16 2.2696 7 0 6 4 39.89 1.99 2.2602 9 3 3 8 40.02 23.42 2.2528 8 4 0 4 40.52 1.49 2.2263 1 5 1 8 40.59 1.81 2.2224 2 1 7 8 40.83 7.85 2.2104 10 2 4 8 40.94 1.22 2.2044 4 4 4 8 41.07 11.94 2.1979 12 2 2 8 41.64 1.04 2.1690 8 4 2 8 43.01 1.41 2.1032 2 2 7 8 43.72 7.31 2.0703 14 0 2 4 44.54 3.22 2.0341 3 5 3 8 44.62 1.00 2.0309 7 4 4 8 44.99 1.48 2.0147 12 3 2 8 45.19 2.14 2.0066 0 0 8 2 45.29 2.20 2.0022 1 0 8 4 45.42 1.15 1.9968 10 0 6 4 45.69 3.11 1.9859 12 2 4 8 45.83 1.02 1.9800 7 5 1 8 46.21 9.81 1.9645 8 4 4 8 48.14 3.97 1.8903 14 0 4 4 48.45 2.79 1.8787 0 6 0 2 48.54 1.22 1.8755 2 2 8 8 48.56 2.91 1.8750 16 0 0 2 48.92 1.09 1.8618 12 2 5 8 49.04 2.71 1.8575 3 2 8 8 49.74 4.47 1.8331 4 2 8 8 50.08 1.37 1.8213 12 4 2 8 50.45 1.34 1.8089 11 2 6 8 50.45 1.86 1.8089 6 4 6 8 50.63 1.37 1.8030 5 2 8 8 50.76 1.67 1.7986 10 1 7 8 50.97 1.59 1.7916 4 5 5 8 51.42 6.59 1.7771 4 6 2 8 51.66 1.15 1.7695 1 6 3 8 51.72 1.09 1.7676 7 4 6 8 52.67 2.46 1.7377 12 2 6 8 53.01 1.63 1.7275 11 5 1 8 53.15 3.90 1.7233 8 4 6 8 53.98 1.78 1.6987 16 0 4 4 54.26 1.14 1.6906 2 6 4 8 54.35 1.60 1.6880 8 2 8 8 55.04 2.12 1.6685 14 4 2 8 55.37 2.66 1.6593 4 6 4 8 56.28 1.91 1.6346 0 4 8 4 56.59 2.55 1.6265 16 2 4 8 57.05 2.17 1.6142 9 5 5 8 57.47 1.44 1.6034 14 2 6 8 57.49 2.13 1.6030 1 0 10 4 57.64 1.19 1.5993 10 2 8 8 57.68 1.88 1.5982 18 2 0 4 57.92 3.76 1.5922 10 6 0 4 59.19 2.02 1.5610 16 4 0 4 59.50 1.85 1.5537 11 2 8 8 59.91 1.02 1.5439 0 2 10 4 60.27 1.52 1.5355 16 0 6 4 60.63 1.26 1.5273 7 4 8 8 61.30 1.16 1.5122 4 2 10 8 61.50 1.20 1.5078 12 2 8 8 61.57 2.08 1.5062 4 6 6 8 61.77 2.45 1.5019 12 6 0 4 62.56 4.91 1.4848 18 2 4 8 62.78 2.08 1.4800 10 6 4 8 62.96 1.51 1.4763 12 6 2 8 66.34 1.25 1.4090 0 8 0 2 70.88 1.43 1.3294 0 8 4 4 72.12 1.50 1.3096 12 6 6 8 75.94 1.33 1.2530 8 8 4 8 78.89 1.37 1.2134 22 4 2 8 82.88 1.21 1.1648 14 8 2 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.