P(C6H5)4ReCl4(N2S2) Muller V U, Vogler S, Dehnicke K, Fenske D Acta Crystallographica C46 (1990) 1989-1992 Tetraphenylphosphonium- und natrium-15-krone-5-tetrachloro- cyclodithiadiazenorhenat _database_code_amcsd 0010187 CELL PARAMETERS: 7.6740 12.6970 14.6060 77.640 80.680 89.780 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1371.122 Density (g/cm3): 1.791 MAX. ABS. INTENSITY / VOLUME**2: 13.22174613 RIR: 2.404 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.28 1.28 14.0720 0 0 1 2 7.13 26.45 12.3964 0 1 0 2 8.42 57.99 10.4958 0 1 1 2 10.48 36.49 8.4403 0 -1 1 2 11.69 11.28 7.5688 1 0 0 2 12.33 36.90 7.1780 1 0 1 2 12.58 100.00 7.0360 0 0 2 2 13.06 4.25 6.7810 0 1 2 2 13.51 7.89 6.5538 -1 1 0 2 13.75 3.82 6.4392 1 1 1 2 13.90 12.46 6.3699 1 1 0 2 14.17 21.24 6.2496 -1 0 1 2 14.29 16.57 6.1982 0 2 0 2 14.31 35.62 6.1874 0 2 1 2 14.75 2.57 6.0069 1 -1 1 2 15.07 7.87 5.8773 -1 1 1 2 15.72 8.23 5.6379 1 0 2 2 15.77 8.59 5.6195 0 -1 2 2 16.27 13.70 5.4481 1 1 2 2 16.83 19.61 5.2676 0 -2 1 2 16.89 8.57 5.2479 0 2 2 2 18.15 14.96 4.8887 1 2 1 2 18.21 15.30 4.8724 -1 2 0 2 18.23 4.38 4.8653 1 -1 2 2 18.58 8.48 4.7754 -1 0 2 2 18.72 5.50 4.7395 0 1 3 2 18.76 18.59 4.7289 -1 1 2 2 18.79 10.05 4.7220 1 2 0 2 19.66 5.05 4.5160 1 -2 1 2 20.52 5.73 4.3289 1 1 3 2 20.57 3.51 4.3188 1 0 3 2 21.02 9.28 4.2258 -1 -1 2 2 21.05 1.93 4.2202 0 -2 2 2 21.14 9.04 4.2033 0 2 3 2 21.39 16.09 4.1538 -1 -2 1 2 21.51 5.45 4.1321 0 3 0 2 21.51 5.05 4.1310 -1 2 2 2 21.66 12.92 4.1032 0 -1 3 2 22.47 26.13 3.9563 0 3 2 2 22.85 16.13 3.8911 1 -2 2 2 22.87 3.32 3.8887 1 2 3 2 23.00 2.89 3.8668 1 -1 3 2 23.51 11.69 3.7844 2 0 0 2 23.64 3.52 3.7640 -1 1 3 2 24.22 5.25 3.6743 2 1 1 2 24.37 2.52 3.6523 -2 1 0 2 24.59 2.99 3.6202 2 -1 1 2 24.81 8.25 3.5890 2 0 2 2 25.32 1.36 3.5180 0 0 4 2 25.36 5.54 3.5122 -2 0 1 2 25.50 1.22 3.4925 -1 2 3 2 25.69 3.55 3.4682 1 1 4 2 25.78 1.03 3.4558 -2 1 1 2 26.11 1.90 3.4126 1 0 4 2 26.19 1.51 3.4029 0 -2 3 2 26.26 1.05 3.3937 -1 -1 3 2 26.29 1.33 3.3905 0 2 4 2 26.40 1.80 3.3760 2 -1 2 2 26.96 7.53 3.3074 -2 -1 1 2 27.74 2.62 3.2160 2 0 3 2 27.80 1.44 3.2088 2 1 3 2 28.02 3.23 3.1850 2 2 0 2 28.11 6.63 3.1742 0 4 1 2 28.45 6.33 3.1371 1 -1 4 2 28.57 1.99 3.1248 -2 0 2 2 28.59 2.57 3.1220 -2 1 2 2 28.86 2.14 3.0937 0 4 2 2 29.53 2.88 3.0251 2 -1 3 2 29.57 4.46 3.0205 0 3 4 2 30.77 3.94 2.9053 1 4 2 2 30.95 10.70 2.8890 0 4 3 2 31.54 1.27 2.8364 -2 3 0 2 31.69 3.17 2.8239 -1 4 2 2 31.69 1.39 2.8238 2 3 2 2 31.74 1.86 2.8189 2 0 4 2 31.85 1.83 2.8098 0 -2 4 2 31.99 2.99 2.7978 -1 -1 4 2 32.05 2.09 2.7927 1 0 5 2 32.32 7.76 2.7696 1 -2 4 2 32.37 1.15 2.7659 1 -4 1 2 32.38 1.88 2.7649 1 2 5 2 32.59 1.51 2.7477 1 -3 3 2 32.77 3.49 2.7332 -2 0 3 2 32.89 7.16 2.7230 2 -2 3 2 33.64 2.91 2.6640 2 -1 4 2 33.66 8.48 2.6623 -2 -2 2 2 33.78 1.60 2.6536 -2 3 2 2 34.00 2.13 2.6368 -1 4 3 2 34.32 3.87 2.6132 1 -1 5 2 34.64 7.04 2.5892 -2 -1 3 2 34.88 1.09 2.5720 -2 -3 1 2 34.94 1.21 2.5680 1 3 5 2 35.11 3.07 2.5563 1 4 4 2 35.38 1.54 2.5372 0 5 1 2 35.58 1.74 2.5229 3 0 0 2 35.70 1.13 2.5151 0 5 2 2 35.77 1.80 2.5101 3 0 2 2 35.78 1.74 2.5099 2 3 4 2 35.90 2.09 2.5015 3 -1 1 2 35.99 1.78 2.4956 2 1 5 2 36.57 3.23 2.4570 3 1 0 2 36.61 1.10 2.4543 -2 3 3 2 36.88 1.12 2.4373 2 4 1 2 36.97 1.33 2.4316 0 -3 4 2 37.14 2.96 2.4209 -2 1 4 2 37.17 3.52 2.4187 0 5 3 2 37.23 1.65 2.4151 -3 0 1 2 37.40 1.73 2.4044 1 1 6 2 37.42 1.01 2.4035 1 5 1 2 37.45 1.84 2.4013 -3 1 1 2 37.72 1.50 2.3851 3 1 3 2 37.80 1.34 2.3802 2 4 3 2 37.82 1.34 2.3787 -1 5 0 2 37.96 1.05 2.3701 3 2 1 2 38.00 1.63 2.3680 -1 5 2 2 38.02 1.59 2.3668 -1 3 5 2 38.12 1.17 2.3610 2 4 0 2 38.16 1.30 2.3586 3 -2 1 2 38.18 1.39 2.3574 -2 -3 2 2 38.27 2.49 2.3520 0 4 5 2 38.38 1.02 2.3453 0 0 6 2 38.46 1.95 2.3407 1 5 3 2 38.47 1.53 2.3399 2 -1 5 2 38.70 2.27 2.3264 1 -4 3 2 38.90 1.73 2.3151 3 -1 3 2 39.69 2.23 2.2710 0 5 4 2 39.88 1.11 2.2603 0 3 6 2 39.93 1.59 2.2580 2 -4 2 2 40.35 1.98 2.2354 -2 3 4 2 40.48 1.36 2.2284 1 -1 6 2 41.02 1.96 2.2005 -3 -2 1 2 41.23 1.06 2.1898 3 3 2 2 41.31 2.66 2.1853 -3 -1 2 2 41.33 1.08 2.1846 -3 3 0 2 41.38 1.17 2.1818 2 -3 4 2 41.48 1.35 2.1771 -1 4 5 2 41.70 1.68 2.1657 2 -2 5 2 41.73 1.13 2.1645 2 2 6 2 41.94 1.09 2.1540 1 -5 2 2 42.43 1.94 2.1304 -1 5 4 2 42.59 1.63 2.1227 1 -3 5 2 42.63 1.34 2.1208 2 5 2 2 42.80 1.14 2.1129 -2 -2 4 2 42.87 3.14 2.1095 0 6 2 2 43.09 1.81 2.0992 0 5 5 2 43.14 1.55 2.0968 -3 1 3 2 43.20 1.83 2.0943 1 4 6 2 43.64 1.95 2.0740 2 3 6 2 43.83 1.08 2.0655 -2 4 4 2 43.84 1.44 2.0651 2 -1 6 2 43.90 1.74 2.0624 1 -2 6 2 43.98 1.74 2.0589 1 2 7 2 44.08 1.37 2.0543 2 -5 1 2 44.14 1.44 2.0516 0 -2 6 2 44.31 2.60 2.0441 2 5 0 2 44.47 2.24 2.0374 -1 6 1 2 44.62 1.41 2.0306 3 -2 4 2 44.66 1.01 2.0291 1 6 1 2 44.80 1.11 2.0231 -2 3 5 2 45.09 1.73 2.0108 -2 -1 5 2 45.09 1.15 2.0107 1 6 3 2 45.51 1.15 1.9930 1 3 7 2 45.70 1.28 1.9852 3 -1 5 2 45.87 2.23 1.9782 0 6 4 2 46.71 1.93 1.9445 1 -6 1 2 47.03 1.63 1.9323 -2 -3 4 2 47.41 1.07 1.9176 4 0 1 2 48.61 1.22 1.8732 0 -3 6 2 49.38 1.02 1.8457 -3 -1 4 2 49.62 1.11 1.8373 2 6 1 2 49.83 1.42 1.8299 -2 3 6 2 50.87 1.46 1.7949 3 5 3 2 51.15 1.05 1.7858 2 -3 6 2 51.79 1.02 1.7652 -2 5 5 2 52.02 1.08 1.7580 -3 5 2 2 52.08 1.06 1.7562 4 -1 4 2 53.71 1.24 1.7066 1 4 8 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.