data_global
_amcsd_formula_title 'K6[Mo8O26F2].6H2O'
loop_
_publ_author_name
'Kamenar B'
'Kaitner B'
'Strukan N'
_journal_name_full 'Acta Crystallographica, Section C'
_journal_volume 46 
_journal_year 1990
_journal_page_first 2249
_journal_page_last 2251
_publ_section_title
;
 Structure of potassium difluorooctamolybdate hexahydrate
;
_database_code_amcsd 0010209
_chemical_formula_sum 'Mo4 F O16 K3 H6'
_cell_length_a 10.497
_cell_length_b 10.403
_cell_length_c 8.001
_cell_angle_alpha 107.16
_cell_angle_beta 95.77
_cell_angle_gamma 105.53
_cell_volume 788.896
_exptl_crystal_density_diffrn      3.292
_symmetry_space_group_name_H-M 'P -1'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  '-x,-y,-z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Mo1   0.48951   0.47980   0.27535   0.12060
Mo2   0.17756   0.24346   0.14397   0.17990
Mo3   0.50144   0.79143   0.60542   0.17920
Mo4   0.20806   0.56085   0.40707   0.19820
F   0.26980   0.19190  -0.05660   0.03510
O1   0.55570   0.41150   0.09490   0.02040
O2   0.05020   0.25910   0.00530   0.02910
O3   0.11570   0.08160   0.16600   0.03230
O4   0.44080   0.86280   0.79160   0.03160
O5   0.60310   0.93530   0.56770   0.02920
O6   0.15470   0.60900   0.60410   0.03710
O7   0.09270   0.57410   0.24950   0.03350
O8   0.56870   0.66340   0.34410   0.02220
O9   0.15010   0.35800   0.36340   0.01920
O10   0.34270   0.73810   0.42660   0.02300
O11   0.37370   0.27870   0.28620   0.01660
O12   0.31130   0.46430   0.18540   0.01610
O13   0.40330   0.55980   0.54020   0.01840
K1   0.48910   0.14830   0.82560   0.03470
K2   0.86460   0.11580   0.66260   0.03830
K3   0.17050   0.50600   0.89900   0.03670
Wat1   0.75780   0.19260   0.99390   0.04930
Wat2   0.12980   0.22630   0.62540   0.06410
Wat3   0.85060   0.08820   0.31090   0.06580