Pb4Sb4Se10 Skowron A, Brown I D Acta Crystallographica C46 (1990) 2287-2291 Structure of antimony lead selenide, Pb4Sb4Se10, a selenium analogue of cosalite _database_code_amcsd 0010214 CELL PARAMETERS: 24.5910 19.7570 4.1660 90.000 90.000 90.000 SPACE GROUP: Pnam X-RAY WAVELENGTH: 1.541838 Cell Volume: 2024.028 Density (g/cm3): 6.791 MAX. ABS. INTENSITY / VOLUME**2: 98.40755802 RIR: 4.719 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.74 1.61 15.4019 1 1 0 4 9.65 5.89 9.1665 1 2 0 4 11.49 1.78 7.7009 2 2 0 4 11.69 1.20 7.5712 3 1 0 4 13.92 5.71 6.3615 1 3 0 4 15.26 2.74 5.8054 2 3 0 4 16.99 1.16 5.2195 4 2 0 4 19.37 3.62 4.5833 2 4 0 4 19.76 1.59 4.4940 4 3 0 4 21.00 7.97 4.2306 3 4 0 4 21.68 4.02 4.0985 6 0 0 2 21.80 5.26 4.0764 0 1 1 4 22.15 13.07 4.0131 6 1 0 4 22.56 1.21 3.9406 5 3 0 4 23.10 3.44 3.8505 4 4 0 4 23.46 2.12 3.7927 1 2 1 8 23.65 1.72 3.7619 2 5 0 4 24.29 5.42 3.6642 2 2 1 8 25.02 30.33 3.5594 3 5 0 4 25.56 6.99 3.4852 1 3 1 8 25.56 4.98 3.4851 5 4 0 4 25.60 2.76 3.4797 6 3 0 4 25.76 2.93 3.4587 7 1 0 4 25.83 4.47 3.4487 4 0 1 4 26.33 8.72 3.3847 2 3 1 8 27.08 1.46 3.2928 0 6 0 2 27.39 6.67 3.2560 4 2 1 8 28.05 5.38 3.1807 2 6 0 4 28.30 1.67 3.1541 6 4 0 4 28.44 14.96 3.1385 5 1 1 8 28.99 9.35 3.0804 5 5 0 4 29.23 23.26 3.0555 3 6 0 4 29.52 100.00 3.0260 5 2 1 8 30.11 5.59 2.9684 3 4 1 8 30.46 1.02 2.9351 8 2 0 4 30.60 16.92 2.9216 6 0 1 4 30.80 19.91 2.9027 4 6 0 4 30.94 7.71 2.8902 6 1 1 8 31.24 30.61 2.8628 5 3 1 8 31.64 8.73 2.8277 4 4 1 8 31.94 15.94 2.8017 6 2 1 8 32.55 2.27 2.7509 2 7 0 4 32.73 3.11 2.7362 5 6 0 4 33.10 1.29 2.7062 3 5 1 8 33.52 1.83 2.6731 5 4 1 8 34.61 1.63 2.5915 7 2 1 8 34.92 1.64 2.5692 1 6 1 8 34.98 3.71 2.5650 4 7 0 4 35.71 3.91 2.5147 6 4 1 8 36.12 2.58 2.4868 7 3 1 8 36.47 4.57 2.4639 3 6 1 8 37.62 2.07 2.3909 9 4 0 4 37.70 1.09 2.3863 10 2 0 4 38.05 2.91 2.3646 3 8 0 4 38.14 8.35 2.3594 7 4 1 8 38.53 17.46 2.3367 0 7 1 4 38.71 1.98 2.3262 1 7 1 8 38.89 6.95 2.3155 8 3 1 8 39.10 3.31 2.3037 10 3 0 4 39.25 5.21 2.2956 2 7 1 8 39.32 1.73 2.2916 4 8 0 4 40.13 6.35 2.2471 3 7 1 8 40.80 9.88 2.2116 8 4 1 8 40.89 1.68 2.2070 5 8 0 4 41.00 16.87 2.2014 10 4 0 4 41.02 1.84 2.2003 7 7 0 4 41.41 1.78 2.1804 11 2 0 4 41.85 4.02 2.1586 9 3 1 8 42.72 10.69 2.1165 1 8 1 8 43.02 4.81 2.1027 9 6 0 4 43.22 13.60 2.0934 2 8 1 8 43.34 4.04 2.0878 10 5 0 4 43.44 32.80 2.0830 0 0 2 2 43.65 16.19 2.0737 9 4 1 8 43.72 2.54 2.0706 10 2 1 8 44.03 4.41 2.0565 3 8 1 8 44.48 2.22 2.0366 11 4 0 4 44.96 10.23 2.0160 10 3 1 8 45.16 1.29 2.0079 4 8 1 8 45.19 3.47 2.0065 12 2 0 4 45.23 1.29 2.0046 5 9 0 4 45.93 2.11 1.9757 0 10 0 2 46.07 2.63 1.9703 10 6 0 4 46.57 4.22 1.9502 5 8 1 8 46.78 1.82 1.9421 0 9 1 4 47.04 2.85 1.9318 11 2 1 8 47.39 2.06 1.9183 2 9 1 8 48.34 1.74 1.8830 13 1 0 4 48.50 4.48 1.8772 9 6 1 8 48.73 1.37 1.8688 3 4 2 8 48.93 1.73 1.8616 7 9 0 4 48.97 3.69 1.8602 8 7 1 8 49.03 2.12 1.8579 13 2 0 4 49.20 1.06 1.8519 4 9 1 8 49.29 2.55 1.8488 6 1 2 8 49.80 1.66 1.8309 12 1 1 8 50.78 7.22 1.7978 3 5 2 8 51.08 1.19 1.7880 5 4 2 8 51.34 3.07 1.7797 6 10 0 4 51.75 3.10 1.7666 2 10 1 8 52.51 1.53 1.7426 2 6 2 8 52.95 3.17 1.7294 14 2 0 4 53.07 2.70 1.7255 5 5 2 8 53.19 3.52 1.7220 7 10 0 4 53.22 6.84 1.7211 3 6 2 8 54.20 6.26 1.6923 4 6 2 8 55.44 1.01 1.6574 5 6 2 8 56.31 2.18 1.6338 15 1 0 4 56.95 1.51 1.6170 4 7 2 8 59.10 1.26 1.5630 3 8 2 8 59.18 1.48 1.5613 5 12 0 4 59.86 1.50 1.5451 10 3 2 8 60.61 1.02 1.5278 6 12 0 4 61.26 8.16 1.5130 10 4 2 8 61.62 1.28 1.5051 3 12 1 8 61.81 1.23 1.5009 9 11 0 4 62.79 2.41 1.4798 9 6 2 8 63.04 2.10 1.4746 10 5 2 8 63.45 1.98 1.4661 11 9 1 8 63.65 1.75 1.4620 5 12 1 8 63.86 1.74 1.4576 15 4 1 8 63.93 1.21 1.4562 11 4 2 8 64.48 1.95 1.4451 12 2 2 8 65.02 2.98 1.4343 6 12 1 8 65.07 1.17 1.4335 0 10 2 4 65.17 1.44 1.4314 10 6 2 8 65.49 1.24 1.4253 1 13 1 8 65.60 1.91 1.4232 15 5 1 8 66.99 1.07 1.3969 13 1 2 8 67.10 1.33 1.3950 11 10 1 8 67.33 1.03 1.3907 4 13 1 8 67.48 1.04 1.3881 7 9 2 8 67.56 1.27 1.3865 13 2 2 8 67.69 5.83 1.3842 15 6 1 8 67.69 1.20 1.3842 16 4 1 8 69.47 1.98 1.3531 6 10 2 8 70.57 2.72 1.3346 1 14 1 8 70.82 2.13 1.3306 14 2 2 8 71.02 2.39 1.3272 7 10 2 8 71.20 4.97 1.3244 5 2 3 8 71.42 1.31 1.3208 16 6 1 8 72.12 1.64 1.3097 5 3 3 8 72.57 1.35 1.3027 14 9 1 8 72.86 2.27 1.2981 18 0 1 4 72.88 1.19 1.2979 15 8 1 8 73.70 1.54 1.2855 15 1 2 8 75.22 1.38 1.2633 11 12 1 8 76.21 1.15 1.2493 5 12 2 8 76.44 1.48 1.2460 0 7 3 4 77.89 1.34 1.2264 19 2 1 8 79.24 1.11 1.2090 1 8 3 8 79.58 1.46 1.2046 2 8 3 8 79.88 1.74 1.2008 9 4 3 8 80.81 1.19 1.1893 10 3 3 8 82.35 1.14 1.1709 20 2 1 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.