RuC10H13N2O8H2O Okamoto K, Hidaka J, Iida I, Higashino K, Kanamori K Acta Crystallographica C46 (1990) 2327-2329 Structure of aqua(ethylenediaminetetraacetato)ruthenium(III) _database_code_amcsd 0010231 CELL PARAMETERS: 8.4150 8.8310 17.6330 90.000 99.660 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1291.779 Density (g/cm3): 2.043 MAX. ABS. INTENSITY / VOLUME**2: 13.92564244 RIR: 2.220 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.18 2.67 8.6915 0 0 2 2 10.66 10.01 8.2957 1 0 0 2 11.24 19.37 7.8732 0 1 1 4 13.46 31.46 6.5775 -1 0 2 2 14.30 100.00 6.1945 0 1 2 4 14.65 60.70 6.0463 1 1 0 4 14.91 7.90 5.9406 -1 1 1 4 15.96 39.27 5.5536 1 0 2 2 16.81 13.53 5.2751 -1 1 2 4 18.31 2.50 4.8446 0 1 3 4 20.11 34.76 4.4155 0 2 0 2 20.44 5.70 4.3457 0 0 4 2 20.76 2.58 4.2796 0 2 1 4 21.42 9.85 4.1478 2 0 0 2 21.43 6.82 4.1461 -1 0 4 2 22.14 4.41 4.0144 -2 0 2 2 22.81 1.39 3.8992 0 1 4 4 23.70 2.78 3.7543 2 1 0 4 23.71 1.51 3.7531 -1 1 4 4 23.79 3.03 3.7409 1 2 1 4 24.36 27.06 3.6545 -2 1 2 4 24.67 1.02 3.6087 1 0 4 2 25.01 3.46 3.5599 2 1 1 4 25.30 1.89 3.5208 2 0 2 2 25.36 1.81 3.5120 0 2 3 4 26.25 5.30 3.3949 -2 1 3 4 26.54 6.54 3.3591 -1 2 3 4 26.69 35.10 3.3405 1 1 4 4 28.00 3.91 3.1870 -1 1 5 4 28.59 1.64 3.1221 1 2 3 4 28.97 5.74 3.0820 -2 1 4 4 29.36 3.71 3.0419 -2 2 1 4 30.09 1.35 2.9703 -2 2 2 4 30.81 7.47 2.9023 0 3 1 4 30.94 4.97 2.8903 -1 0 6 2 31.21 1.12 2.8662 1 1 5 4 32.24 1.86 2.7768 2 0 4 2 32.27 1.05 2.7742 1 3 0 4 32.39 10.24 2.7638 -1 3 1 4 32.60 1.54 2.7469 -1 1 6 4 32.98 1.67 2.7159 1 3 1 4 33.15 1.47 2.7025 -1 2 5 4 33.35 2.41 2.6869 -1 3 2 4 33.52 1.98 2.6733 -3 1 1 4 33.88 3.83 2.6456 -3 1 2 4 34.17 7.54 2.6244 0 3 3 4 34.46 14.05 2.6026 1 0 6 2 34.48 1.95 2.6009 1 3 2 4 34.66 1.01 2.5877 -2 0 6 2 35.12 2.66 2.5552 2 2 3 4 35.43 8.80 2.5335 -3 0 4 2 35.69 4.06 2.5159 3 0 2 2 35.97 2.06 2.4964 1 1 6 4 36.94 5.17 2.4334 -2 2 5 4 37.85 1.76 2.3772 2 1 5 4 37.90 3.35 2.3739 -2 3 2 4 38.35 1.15 2.3473 2 3 1 4 39.20 3.68 2.2981 -2 3 3 4 39.37 4.35 2.2887 -3 2 3 4 39.42 2.92 2.2856 -3 1 5 4 39.51 1.06 2.2810 1 3 4 4 39.73 1.22 2.2684 3 1 3 4 40.40 1.53 2.2326 -2 2 6 4 40.44 1.85 2.2303 -1 3 5 4 41.08 2.12 2.1974 -3 2 4 4 41.22 3.65 2.1902 0 4 1 4 41.30 1.73 2.1860 3 2 2 4 42.20 4.70 2.1417 2 1 6 4 42.46 1.32 2.1287 -1 4 1 4 42.48 6.68 2.1279 -3 1 6 4 42.83 2.23 2.1114 1 3 5 4 42.85 2.22 2.1106 3 1 4 4 42.86 1.61 2.1099 0 1 8 4 42.93 5.59 2.1066 1 4 1 4 43.11 3.19 2.0983 -4 0 2 2 44.28 1.01 2.0455 -2 2 7 4 44.62 3.38 2.0307 -1 4 3 4 44.62 2.73 2.0306 -3 3 1 4 44.79 2.42 2.0233 1 2 7 4 44.89 1.22 2.0190 4 1 0 4 44.91 1.73 2.0182 -2 1 8 4 45.96 2.04 1.9746 1 4 3 4 46.08 3.56 1.9696 1 1 8 4 46.20 1.03 1.9649 -1 2 8 4 46.39 3.25 1.9573 -4 1 4 4 46.48 3.78 1.9539 -2 4 1 4 46.70 1.54 1.9450 4 0 2 2 47.93 1.35 1.8981 0 3 7 4 48.11 1.96 1.8914 2 3 5 4 48.76 1.06 1.8675 -3 0 8 2 48.87 2.27 1.8637 0 4 5 4 49.22 2.17 1.8512 3 0 6 2 49.42 1.93 1.8442 -3 3 5 4 49.58 1.45 1.8387 -4 0 6 2 49.68 1.26 1.8352 3 3 3 4 49.93 1.15 1.8266 3 2 5 4 50.58 1.13 1.8047 2 4 3 4 50.59 3.92 1.8043 2 0 8 2 50.71 1.75 1.8001 -4 1 6 4 51.95 2.42 1.7602 -2 4 5 4 52.90 1.65 1.7308 0 5 2 4 53.09 1.54 1.7250 -1 5 1 4 53.55 1.55 1.7112 4 2 3 4 53.64 1.23 1.7087 -2 0 10 2 53.74 1.09 1.7058 -1 5 2 4 53.83 1.91 1.7031 -3 4 3 4 54.98 1.08 1.6703 2 2 8 4 55.06 1.59 1.6679 -3 3 7 4 55.15 1.28 1.6655 4 3 1 4 55.38 1.18 1.6591 5 0 0 2 55.79 1.17 1.6478 2 3 7 4 55.87 1.04 1.6456 2 4 5 4 56.51 1.29 1.6285 -1 3 9 4 56.81 1.60 1.6205 -4 2 7 4 57.08 1.04 1.6136 -4 3 5 4 58.21 2.09 1.5848 1 4 7 4 59.37 1.97 1.5568 5 1 2 4 59.87 1.73 1.5450 1 3 9 4 62.56 1.20 1.4848 3 4 5 4 62.84 1.13 1.4789 3 3 7 4 65.44 1.12 1.4262 -2 1 12 4 65.72 1.19 1.4208 4 4 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.