Ru3(C12H15)(H)(C25H22As2)(CO)8 Fun H K, Bin Shawkataly O, Teohs S G Acta Crystallographica C46 (1990) 2329-2331 The structure of 1,1,1,2,2,2,3,3-octacarbonyl-u-(1-3-n-cyclododeca-1,6,9- trien-1-yl-3-ylidene)-2,3-u-hydrido-3-[(As,As,As',As'-tetraphenyl)methylenebis (arsine)-As]-triangula-triruthenium(0)(3 Ru-Ru) _database_code_amcsd 0010232 CELL PARAMETERS: 30.3850 10.0470 14.4020 90.000 90.000 90.000 SPACE GROUP: Pca2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 4396.615 Density (g/cm3): 1.694 MAX. ABS. INTENSITY / VOLUME**2: 14.10228543 RIR: 2.710 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.82 48.52 15.1925 2 0 0 2 8.46 100.00 10.4520 2 0 1 2 9.27 62.65 9.5391 1 1 0 4 10.56 2.24 8.3803 2 1 0 4 11.13 90.35 7.9528 1 1 1 4 11.65 4.94 7.5963 4 0 0 2 12.22 21.54 7.2433 2 1 1 4 12.29 7.30 7.2010 0 0 2 1 12.41 35.27 7.1329 3 1 0 4 13.18 10.80 6.7189 4 0 1 2 13.61 13.90 6.5071 2 0 2 2 13.85 2.60 6.3919 3 1 1 4 15.14 4.36 5.8529 0 1 2 2 15.42 7.65 5.7473 1 1 2 4 15.87 2.03 5.5851 4 1 1 4 16.23 3.93 5.4616 2 1 2 4 16.97 3.67 5.2260 4 0 2 2 17.05 1.01 5.1998 5 1 0 4 17.50 14.33 5.0676 3 1 2 4 17.66 5.10 5.0235 0 2 0 2 17.90 2.93 4.9562 1 2 0 4 18.14 1.68 4.8908 5 1 1 4 18.57 5.12 4.7774 6 0 1 2 18.94 10.40 4.6865 1 2 1 4 19.14 9.98 4.6363 4 1 2 4 19.39 1.30 4.5776 2 0 3 2 19.61 2.69 4.5277 2 2 1 4 19.63 2.27 4.5222 6 1 0 4 20.59 3.34 4.3145 6 1 1 4 20.68 1.05 4.2955 3 2 1 4 21.07 2.51 4.2156 5 1 2 4 21.45 1.41 4.1424 6 0 2 2 21.57 6.01 4.1200 0 2 2 2 21.77 3.88 4.0827 1 2 2 4 21.90 3.35 4.0582 4 0 3 2 22.09 2.04 4.0233 4 2 1 4 22.36 1.86 3.9764 2 2 2 4 23.16 2.81 3.8404 7 1 1 4 23.31 3.34 3.8164 3 2 2 4 23.64 1.08 3.7628 4 1 3 4 23.80 7.75 3.7391 5 2 1 4 24.23 7.90 3.6726 8 0 1 2 24.73 3.55 3.6005 0 0 4 1 25.25 3.77 3.5273 5 1 3 4 25.42 1.36 3.5035 2 0 4 2 25.55 2.41 3.4865 7 1 2 4 25.57 4.47 3.4840 6 0 3 2 25.84 2.83 3.4483 1 2 3 4 26.13 5.39 3.4102 5 2 2 4 26.29 2.49 3.3894 0 1 4 2 26.46 1.63 3.3685 1 1 4 4 26.53 1.18 3.3595 8 0 2 2 27.09 7.24 3.2917 6 1 3 4 27.16 9.65 3.2833 3 2 3 4 27.41 2.60 3.2535 4 0 4 2 27.50 2.14 3.2433 1 3 1 4 27.92 2.96 3.1959 6 2 2 4 28.01 3.33 3.1861 8 1 2 4 28.27 1.93 3.1568 4 2 3 4 28.57 1.60 3.1241 9 1 1 4 29.12 1.40 3.0661 7 1 3 4 29.56 1.02 3.0216 1 3 2 4 29.64 2.48 3.0138 5 2 3 4 29.90 5.56 2.9883 7 2 2 4 30.01 1.39 2.9778 2 3 2 4 30.06 3.34 2.9731 10 0 1 2 30.14 1.22 2.9648 8 2 1 4 30.55 1.72 2.9265 0 2 4 2 30.57 1.31 2.9245 9 1 2 4 31.12 1.66 2.8741 5 3 1 4 31.32 1.72 2.8558 8 1 3 4 31.73 5.73 2.8197 4 3 2 4 32.47 3.50 2.7574 1 1 5 4 32.65 1.71 2.7423 6 3 1 4 32.74 2.49 2.7355 1 3 3 4 32.88 1.10 2.7240 2 1 5 4 33.05 1.54 2.7107 7 2 3 4 33.22 1.59 2.6968 10 1 2 4 33.27 1.39 2.6933 4 0 5 2 33.55 1.82 2.6715 7 1 4 4 33.66 2.15 2.6628 9 1 3 4 33.80 1.26 2.6515 7 3 0 4 33.81 2.14 2.6509 3 3 3 4 34.00 4.54 2.6367 5 2 4 4 34.24 2.16 2.6190 11 1 1 4 34.32 3.11 2.6130 8 0 4 2 34.44 1.26 2.6043 6 3 2 4 34.73 1.34 2.5830 4 3 3 4 34.95 2.54 2.5674 10 0 3 2 36.01 1.36 2.4938 12 0 1 2 36.25 1.00 2.4781 2 4 0 4 37.06 1.44 2.4260 3 2 5 4 37.14 1.82 2.4209 2 3 4 4 37.15 2.67 2.4200 9 2 3 4 37.24 3.94 2.4144 6 3 3 4 37.60 1.11 2.3920 9 1 4 4 37.94 2.18 2.3718 8 3 2 4 37.94 1.68 2.3716 0 4 2 2 37.95 1.76 2.3709 2 0 6 2 38.37 1.36 2.3459 9 3 1 4 38.58 1.03 2.3336 4 3 4 4 38.66 1.01 2.3290 11 1 3 4 39.27 1.16 2.2943 11 2 2 4 39.41 1.31 2.2862 10 2 3 4 39.62 1.40 2.2750 3 1 6 4 39.63 1.18 2.2740 5 3 4 4 40.10 2.29 2.2486 13 1 1 4 40.58 1.08 2.2232 6 4 1 4 40.99 1.31 2.2020 2 4 3 4 41.43 2.61 2.1793 5 1 6 4 41.55 1.13 2.1737 3 4 3 4 41.61 1.14 2.1706 13 1 2 4 41.61 1.02 2.1704 14 0 0 2 42.20 2.43 2.1413 11 1 4 4 44.02 1.12 2.0570 13 1 3 4 44.47 1.52 2.0375 6 4 3 4 45.08 1.08 2.0112 1 1 7 4 45.14 1.37 2.0085 9 2 5 4 45.22 1.86 2.0053 6 3 5 4 45.63 1.08 1.9882 4 4 4 4 45.69 1.39 1.9859 4 0 7 2 45.69 1.17 1.9857 15 1 0 4 45.91 1.50 1.9768 3 1 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.