Co3(C2H3)(CO)7(C18H15O3P)2 Maginn S J Acta Crystallographica C46 (1990) 2339-2341 Structure of 1,1,1,2,2,3,3-heptacarbonyl-1,2,3-u3-ethylidyne-2,3- bis(triphenyl-phosphite)-triangulo-tricobalt(0) _database_code_amcsd 0010236 CELL PARAMETERS: 11.3110 11.5410 18.8050 99.610 103.210 70.930 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 2247.310 Density (g/cm3): 1.459 MAX. ABS. INTENSITY / VOLUME**2: 8.376901245 RIR: 1.870 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 4.85 3.38 18.2151 0 0 1 2 8.42 12.79 10.5023 1 0 0 2 8.90 16.43 9.9364 -1 0 1 2 9.06 29.57 9.7638 0 -1 1 2 9.71 100.00 9.1076 0 0 2 2 9.80 4.84 9.0235 1 1 0 2 9.82 70.90 9.0062 -1 -1 1 2 9.90 21.74 8.9375 0 1 1 2 10.48 6.77 8.4418 1 0 1 2 11.61 31.99 7.6209 -1 0 2 2 11.96 9.76 7.3999 1 1 1 2 12.01 5.69 7.3713 -1 -1 2 2 12.04 1.17 7.3488 0 -1 2 2 13.38 3.68 6.6180 -1 1 0 2 13.98 1.48 6.3361 -1 1 1 2 14.59 2.95 6.0717 0 0 3 2 15.43 2.79 5.7414 -1 0 3 2 15.48 22.50 5.7253 -1 -1 3 2 15.97 2.93 5.5489 1 2 0 2 16.00 2.69 5.5409 0 -1 3 2 16.39 9.13 5.4070 2 1 0 2 16.57 4.80 5.3493 0 -2 1 2 16.88 7.46 5.2511 2 0 0 2 16.92 3.03 5.2397 -2 -1 2 2 16.96 8.45 5.2292 -1 -2 2 2 17.44 6.61 5.0859 0 1 3 2 17.62 1.63 5.0333 1 2 1 2 17.85 4.64 4.9682 -2 0 2 2 18.17 6.06 4.8819 0 -2 2 2 19.15 1.08 4.6336 -2 -1 3 2 19.38 4.09 4.5806 -1 -2 3 2 19.68 2.01 4.5118 2 2 0 2 19.87 3.83 4.4687 0 2 2 2 20.38 1.42 4.3579 0 -1 4 2 20.56 1.88 4.3202 -1 2 0 2 20.83 3.68 4.2640 0 -2 3 2 21.05 2.23 4.2209 2 0 2 2 21.41 1.35 4.1497 2 2 1 2 21.48 1.38 4.1362 -2 -2 3 2 21.99 2.69 4.0419 2 -1 1 2 22.63 1.87 3.9291 -1 -2 4 2 23.35 1.82 3.8104 -2 0 4 2 23.83 1.02 3.7341 -1 -3 2 2 24.15 7.98 3.6856 -2 -2 4 2 24.32 2.07 3.6599 -1 0 5 2 24.34 1.28 3.6563 1 -1 4 2 24.56 5.30 3.6253 2 1 3 2 24.61 1.18 3.6175 0 3 0 2 24.81 3.19 3.5883 1 3 1 2 25.58 2.89 3.4821 0 3 1 2 25.97 2.59 3.4307 -2 -1 5 2 26.91 2.39 3.3132 2 -1 3 2 26.94 1.21 3.3090 -2 2 0 2 27.35 2.84 3.2608 2 2 3 2 28.10 1.46 3.1756 0 -2 5 2 28.24 1.81 3.1606 2 0 4 2 28.52 2.99 3.1296 2 1 4 2 28.80 1.29 3.0996 -3 1 1 2 28.99 3.85 3.0800 -1 3 1 2 29.06 6.21 3.0727 -3 1 0 2 29.21 1.26 3.0574 2 3 2 2 29.39 1.62 3.0389 -3 1 2 2 30.02 2.02 2.9771 -2 2 3 2 30.14 4.06 2.9648 3 -1 1 2 30.32 1.88 2.9477 2 -1 4 2 30.38 1.71 2.9419 -1 3 2 2 30.96 2.40 2.8888 -3 -2 5 2 31.19 1.31 2.8673 -2 -3 5 2 31.39 2.17 2.8495 -3 -3 4 2 31.48 2.12 2.8420 1 4 0 2 32.15 1.53 2.7843 2 3 3 2 32.18 1.61 2.7812 1 0 6 2 32.42 1.20 2.7615 2 0 5 2 32.87 1.12 2.7248 3 2 3 2 33.89 1.65 2.6452 0 4 1 2 34.31 1.06 2.6136 -3 2 1 2 34.45 2.10 2.6032 3 -1 3 2 34.49 1.03 2.6004 1 4 2 2 35.21 1.00 2.5491 -1 3 4 2 35.24 1.63 2.5471 2 2 5 2 36.57 1.28 2.4571 -3 -3 6 2 37.11 1.32 2.4224 1 0 7 2 37.32 1.03 2.4097 2 1 6 2 37.42 1.21 2.4034 -4 1 2 2 37.59 1.75 2.3928 -4 1 0 2 37.64 1.36 2.3894 0 4 3 2 41.15 1.12 2.1939 2 5 1 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.