Pd(C3H3NS2)4Cl2C3H3NS2 Raper E S, Britton A M, Clegg W Acta Crystallographica C46 (1990) 2344-2346 Structure of tetrakis(2,3-dihydro-1,3-thiazole-2-thione)palladium(II) dichloride 2,3-dihydro-1,3-thiazole-2-thione solvate _database_code_amcsd 0010238 CELL PARAMETERS: 11.5460 17.7490 13.7240 90.000 100.910 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2761.625 Density (g/cm3): 1.799 MAX. ABS. INTENSITY / VOLUME**2: 8.052554255 RIR: 1.457 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.80 100.00 11.3373 1 0 0 2 9.97 9.19 8.8745 0 2 0 2 11.94 79.10 7.4117 0 2 1 4 12.18 1.63 7.2665 1 1 1 4 12.67 2.25 6.9882 1 2 0 4 13.14 16.13 6.7380 0 0 2 2 13.58 19.56 6.5224 -1 2 1 4 13.96 4.37 6.3435 -1 0 2 2 14.95 30.40 5.9275 1 2 1 4 15.63 8.70 5.6687 2 0 0 2 16.52 8.89 5.3665 0 2 2 4 17.18 41.38 5.1607 -1 2 2 4 18.45 6.00 4.8093 -2 0 2 2 18.57 6.36 4.7772 2 2 0 4 18.69 6.39 4.7475 -2 2 1 4 20.01 1.18 4.4373 0 4 0 2 20.69 81.49 4.2922 2 2 1 4 22.06 7.90 4.0292 -1 4 1 4 22.18 23.38 4.0078 0 2 3 4 22.24 8.56 3.9967 -1 2 3 4 22.32 10.64 3.9823 2 0 2 2 23.36 1.18 3.8073 -2 1 3 4 23.84 1.48 3.7318 -2 3 2 4 24.48 5.16 3.6360 -1 4 2 4 24.73 2.02 3.5995 -3 0 2 2 24.78 1.15 3.5928 1 2 3 4 24.95 2.03 3.5689 -2 2 3 4 25.32 5.27 3.5182 -3 2 1 4 25.49 30.97 3.4941 2 4 0 4 25.58 20.45 3.4824 -2 4 1 4 25.62 4.04 3.4770 3 2 0 4 26.06 1.03 3.4189 1 4 2 4 26.13 3.18 3.4105 -1 0 4 2 26.46 3.32 3.3690 0 0 4 2 26.73 2.58 3.3356 -3 2 2 4 26.77 1.25 3.3302 -1 5 1 4 26.94 1.70 3.3099 0 1 4 4 27.10 3.94 3.2903 2 4 1 4 27.35 2.41 3.2612 -2 4 2 4 27.74 1.66 3.2164 -3 3 1 4 28.02 2.56 3.1848 3 3 0 4 28.03 1.36 3.1835 -1 2 4 4 28.13 1.32 3.1717 -2 0 4 2 28.32 1.46 3.1513 -1 4 3 4 29.04 18.63 3.0744 1 0 4 2 29.20 1.04 3.0583 3 0 2 2 29.39 9.76 3.0395 2 2 3 4 29.63 11.58 3.0154 -3 2 3 4 30.15 1.95 2.9637 2 4 2 4 30.21 1.68 2.9582 0 6 0 2 30.53 9.12 2.9285 -2 4 3 4 30.83 1.32 2.9003 -3 4 1 4 30.93 2.15 2.8915 3 2 2 4 31.09 23.42 2.8771 3 4 0 4 31.64 2.89 2.8275 -1 6 1 4 32.02 3.94 2.7954 -3 4 2 4 32.63 1.13 2.7444 -4 2 1 4 32.75 2.88 2.7344 3 4 1 4 33.07 1.35 2.7086 0 6 2 4 33.13 12.38 2.7040 -1 4 4 4 33.41 9.23 2.6818 2 0 4 2 34.30 1.72 2.6141 2 4 3 4 34.51 2.52 2.5988 -3 4 3 4 34.77 10.98 2.5803 -2 4 4 4 34.79 8.14 2.5789 0 2 5 4 34.95 2.29 2.5671 2 2 4 4 35.05 8.67 2.5599 4 2 1 4 35.29 1.54 2.5435 3 2 3 4 35.44 3.07 2.5330 2 6 1 4 35.52 2.29 2.5271 1 4 4 4 35.54 1.80 2.5261 -2 2 5 4 35.63 3.26 2.5197 -2 6 2 4 36.36 2.20 2.4706 0 6 3 4 36.40 2.19 2.4680 -1 6 3 4 36.65 1.34 2.4520 4 0 2 2 37.13 4.40 2.4216 1 2 5 4 37.40 3.35 2.4046 -4 0 4 2 37.66 1.91 2.3886 4 4 0 4 37.89 2.52 2.3747 2 6 2 4 37.90 1.80 2.3737 -4 4 2 4 38.09 2.09 2.3624 -3 4 4 4 38.44 2.83 2.3417 -3 6 1 4 38.65 2.90 2.3294 3 6 0 4 39.04 1.79 2.3072 3 0 4 2 39.34 2.24 2.2900 4 4 1 4 39.43 4.53 2.2854 -3 6 2 4 40.04 1.72 2.2517 3 6 1 4 40.15 1.58 2.2460 0 0 6 2 40.58 1.60 2.2229 0 6 4 4 41.24 2.10 2.1892 0 8 1 4 41.47 1.05 2.1773 1 8 0 4 41.54 3.14 2.1741 -3 6 3 4 41.75 2.95 2.1633 -2 6 4 4 42.10 1.59 2.1461 4 4 2 4 42.29 1.90 2.1373 1 8 1 4 42.52 1.02 2.1263 3 6 2 4 42.53 1.40 2.1257 -3 4 5 4 42.76 1.14 2.1145 -3 0 6 2 42.77 3.98 2.1141 -4 4 4 4 42.91 1.19 2.1078 5 2 1 4 43.70 1.02 2.0714 -5 0 4 2 43.83 2.30 2.0657 -4 6 1 4 43.87 1.24 2.0636 -2 8 1 4 44.22 1.54 2.0480 -5 4 1 4 44.26 2.38 2.0466 4 6 0 4 44.47 4.96 2.0372 -4 6 2 4 44.51 1.45 2.0357 5 0 2 2 44.63 2.99 2.0305 -5 4 2 4 44.84 1.37 2.0214 2 8 1 4 45.60 2.15 1.9892 0 8 3 4 45.74 1.34 1.9835 4 6 1 4 46.06 1.87 1.9705 3 2 5 4 46.13 1.75 1.9677 -2 6 5 4 46.16 2.81 1.9665 -4 6 3 4 46.21 1.90 1.9646 2 0 6 2 46.59 1.12 1.9493 5 4 1 4 47.13 1.19 1.9282 -2 8 3 4 47.34 2.00 1.9201 -3 8 1 4 47.52 1.03 1.9133 3 8 0 4 48.05 1.08 1.8934 -2 2 7 4 48.16 1.24 1.8896 6 0 0 2 49.75 3.30 1.8327 -6 2 3 4 50.22 2.03 1.8166 4 4 4 4 51.18 1.87 1.7849 -2 6 6 4 51.99 1.64 1.7589 -4 8 1 4 52.16 1.26 1.7535 1 10 0 4 52.29 2.38 1.7496 5 6 1 4 53.10 1.21 1.7246 -1 8 5 4 53.22 1.03 1.7210 -4 2 7 4 53.25 1.48 1.7202 -3 6 6 4 53.38 2.38 1.7164 0 10 2 4 53.62 1.04 1.7093 -1 10 2 4 54.45 1.87 1.6850 1 10 2 4 54.74 1.50 1.6770 5 6 2 4 55.03 1.41 1.6687 3 6 5 4 55.81 1.32 1.6472 -7 0 2 2 56.79 1.74 1.6212 2 10 2 4 56.79 1.43 1.6211 -2 6 7 4 56.96 1.87 1.6166 6 4 2 4 57.58 1.54 1.6007 -5 2 7 4 58.62 2.48 1.5748 0 4 8 4 58.91 1.19 1.5676 4 8 3 4 63.25 1.22 1.4703 0 12 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.