[Co(C2H4N2)(C3H6N2)(C4H8N2)][Co(CN)6].H20 Takazawa H, Ohba S, Saito Y, Ichida H, Rasmussen K Acta Crystallographica C46 (1990) 2354-2357 Structure of (ethylenediamine)(tetramethylenediamine)(trimethylenediamine)- cobalt(III) hexacyanocobaltate(III)monohydrate,-(+)589[Co(en)(tn)(tmd)]- [Co(CN)6].H20 _database_code_amcsd 0010242 CELL PARAMETERS: 9.5990 15.3440 8.9440 100.470 113.930 81.370 SPACE GROUP: P1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1179.773 Density (g/cm3): 1.357 MAX. ABS. INTENSITY / VOLUME**2: 6.378758470 RIR: 1.531 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.12 7.57 8.7422 1 0 0 1 10.92 11.53 8.1018 0 0 1 1 11.65 1.49 7.5962 -1 0 1 1 11.69 2.27 7.5672 0 -1 1 1 11.77 1.55 7.5170 0 2 0 1 11.96 2.26 7.3990 -1 -1 1 1 12.14 100.00 7.2930 -1 1 0 1 13.09 81.56 6.7643 0 1 1 1 14.07 1.71 6.2940 -1 1 1 1 14.84 95.16 5.9707 -1 -2 1 1 14.88 2.94 5.9552 1 2 0 1 14.97 1.55 5.9193 0 -2 1 1 16.19 4.62 5.4745 -1 2 0 1 17.13 2.87 5.1761 0 2 1 1 17.58 28.88 5.0438 1 0 1 1 18.18 14.90 4.8792 -1 2 1 1 18.36 1.18 4.8320 1 -1 1 1 18.87 13.52 4.7016 -2 -1 1 1 19.54 6.42 4.5423 0 -3 1 1 19.66 24.63 4.5163 1 3 0 1 20.01 9.37 4.4374 -1 -1 2 1 20.32 2.31 4.3711 2 0 0 1 20.59 1.61 4.3141 -2 -2 1 1 20.79 4.23 4.2718 -2 1 1 1 21.17 1.42 4.1966 -1 3 0 1 21.55 2.25 4.1235 1 2 1 1 22.07 2.29 4.0277 0 3 1 1 22.65 3.30 3.9264 2 2 0 1 23.13 1.97 3.8457 -1 3 1 1 23.42 6.80 3.7981 -2 0 2 1 23.50 1.05 3.7862 0 1 2 1 23.51 14.64 3.7836 0 -2 2 1 23.67 4.57 3.7585 0 4 0 1 23.72 1.60 3.7510 -2 -3 1 1 24.02 8.05 3.7049 -2 2 1 1 24.61 4.96 3.6175 1 -3 1 1 26.38 1.96 3.3790 0 -3 2 1 26.47 2.15 3.3670 -2 -3 2 1 27.40 2.55 3.2553 2 -1 1 1 27.46 1.30 3.2477 0 4 1 1 27.99 1.38 3.1882 -3 -1 1 1 28.21 1.35 3.1637 -2 3 0 1 28.22 2.64 3.1618 -3 0 1 1 28.23 2.10 3.1607 -1 -4 2 1 28.36 1.93 3.1470 -2 2 2 1 28.72 1.67 3.1079 1 1 2 1 29.14 1.81 3.0647 2 2 1 1 29.14 1.05 3.0645 1 -4 1 1 29.36 5.94 3.0425 2 -2 1 1 29.48 2.86 3.0300 -1 3 2 1 29.71 1.52 3.0068 0 5 0 1 30.01 3.24 2.9779 -3 0 2 1 30.14 7.10 2.9655 1 4 1 1 30.14 4.08 2.9647 -1 -1 3 1 30.16 1.65 2.9627 -3 -2 2 1 30.29 1.16 2.9506 0 -5 1 1 30.68 7.22 2.9141 3 0 0 1 30.81 1.09 2.9017 -2 -1 3 1 30.96 6.28 2.8880 1 2 2 1 31.44 1.27 2.8453 -2 0 3 1 31.69 3.66 2.8232 -3 1 2 1 31.77 1.58 2.8165 -3 1 0 1 31.83 1.04 2.8113 1 -3 2 1 31.98 2.38 2.7983 3 2 0 1 32.05 2.70 2.7929 2 3 1 1 32.29 1.40 2.7727 -2 3 2 1 32.71 1.26 2.7378 -1 -3 3 1 32.81 3.80 2.7294 -1 -5 2 1 32.90 1.76 2.7221 0 -1 3 1 33.01 6.44 2.7134 -2 -3 3 1 33.14 8.46 2.7035 0 5 1 1 33.17 2.98 2.7006 0 0 3 1 34.19 1.47 2.6225 1 -5 1 1 34.70 3.53 2.5855 0 -5 2 1 35.07 4.12 2.5587 -3 -2 3 1 35.42 2.94 2.5345 -1 -6 1 1 35.51 2.55 2.5278 -1 -4 3 1 35.59 1.62 2.5224 0 -3 3 1 35.78 1.49 2.5095 2 4 1 1 36.08 1.12 2.4896 0 -6 1 1 36.14 1.21 2.4853 2 -4 1 1 36.61 1.01 2.4547 3 0 1 1 36.84 3.39 2.4396 -2 4 2 1 36.92 2.04 2.4346 3 1 1 1 38.02 1.20 2.3666 2 2 2 1 38.29 1.67 2.3508 -4 -2 2 1 38.95 1.04 2.3123 3 -2 1 1 39.69 1.02 2.2712 0 -6 2 1 39.76 1.51 2.2669 -3 2 3 1 39.92 1.45 2.2582 2 6 0 1 40.08 1.64 2.2500 -1 6 1 1 40.59 1.17 2.2224 2 3 2 1 40.66 2.17 2.2187 -2 -2 4 1 41.09 2.28 2.1965 -4 -1 3 1 41.23 1.43 2.1894 4 1 0 1 42.06 1.01 2.1484 0 -7 1 1 42.06 1.08 2.1481 4 2 0 1 42.32 1.04 2.1359 -4 2 2 1 42.35 1.15 2.1342 -1 4 3 1 42.48 1.84 2.1280 1 7 0 1 42.54 2.91 2.1252 -3 -1 4 1 42.61 1.46 2.1219 1 5 2 1 43.40 1.13 2.0850 3 4 1 1 45.02 1.50 2.0139 0 6 2 1 45.21 1.95 2.0055 -2 2 4 1 45.90 1.09 1.9772 2 -1 3 1 47.79 1.12 1.9031 -2 -7 3 1 47.87 1.45 1.9002 -3 -5 4 1 49.26 1.23 1.8498 -4 -4 4 1 49.37 1.11 1.8460 -5 1 2 1 49.66 1.35 1.8360 -2 -8 2 1 50.27 1.00 1.8148 2 7 1 1 51.55 1.11 1.7729 1 -3 4 1 52.55 1.18 1.7416 1 8 1 1 55.18 1.03 1.6645 -2 -9 1 1 55.25 1.83 1.6625 -4 -3 5 1 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.