Ag3 H14 N3 O19 P6 Averbuch-Pouchot M Acta Crystallographica C47 (1991) 930-932 Crystal chemistry of cyclo-hexaphosphates. XIV. Structure of silver ammonium cyclo-hexaphosphate monohydrate _cod_database_code 1008854 _database_code_amcsd 0016720 CELL PARAMETERS: 15.1720 15.1720 13.9940 90.000 90.000 120.000 SPACE GROUP: R-3 X-RAY WAVELENGTH: 1.541838 Cell Volume: 2789.704 Density (g/cm3): 3.098 MAX. ABS. INTENSITY / VOLUME**2: 16.38548330 RIR: 1.722 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.23 12.51 9.5788 1 0 1 6 11.67 65.69 7.5860 1 1 0 6 14.34 17.03 6.1759 0 1 2 6 14.90 47.91 5.9469 0 2 1 6 18.53 22.65 4.7894 2 0 2 6 18.96 74.53 4.6802 2 1 1 6 18.96 25.47 4.6802 3 -1 1 6 19.03 2.20 4.6647 0 0 3 2 21.95 12.42 4.0498 1 2 2 6 22.37 25.26 3.9736 1 1 3 6 22.37 46.57 3.9736 2 -1 3 6 23.45 25.23 3.7930 2 2 0 6 25.25 7.98 3.5266 -1 4 1 6 26.36 28.16 3.3807 1 0 4 6 27.60 6.31 3.2321 3 1 2 6 27.60 45.70 3.2321 4 -1 2 6 27.94 3.21 3.1929 0 3 3 6 27.94 1.54 3.1929 3 0 3 6 28.91 4.15 3.0880 0 2 4 6 30.05 33.70 2.9735 0 4 2 6 30.33 29.62 2.9468 3 2 1 6 30.37 32.12 2.9429 4 -2 3 6 30.37 19.00 2.9429 2 2 3 6 31.19 42.10 2.8672 1 4 0 6 31.19 14.27 2.8672 4 1 0 6 31.27 32.50 2.8601 2 1 4 6 32.34 3.82 2.7684 -2 5 2 6 34.73 26.17 2.5827 0 5 1 6 34.84 1.80 2.5749 2 0 5 6 35.57 72.89 2.5237 1 3 4 6 35.57 8.81 2.5237 -1 4 4 6 36.52 1.12 2.4601 5 0 2 6 36.76 3.34 2.4449 -2 6 1 6 36.76 24.00 2.4449 2 4 1 6 36.79 4.19 2.4427 4 1 3 6 36.86 4.06 2.4383 1 2 5 6 36.86 18.47 2.4383 -1 3 5 6 37.56 9.13 2.3947 4 0 4 6 38.47 3.26 2.3401 6 -2 2 6 38.47 1.89 2.3401 4 2 2 6 38.60 3.81 2.3323 0 0 6 2 38.69 2.22 2.3270 6 -1 1 6 38.69 2.25 2.3270 5 1 1 6 39.46 3.69 2.2836 3 2 4 6 40.33 9.19 2.2361 1 5 2 6 40.33 2.51 2.2361 -1 6 2 6 40.46 10.38 2.2293 1 1 6 6 40.58 1.40 2.2230 6 -3 3 6 40.58 1.75 2.2230 3 3 3 6 40.65 1.27 2.2197 3 1 5 6 40.65 2.56 2.2197 4 -1 5 6 42.34 2.19 2.1348 4 3 1 6 42.99 15.03 2.1040 5 2 0 6 43.86 15.76 2.0640 -3 7 2 6 43.86 4.19 2.0640 3 4 2 6 43.98 2.04 2.0586 0 3 6 6 43.98 7.45 2.0586 3 0 6 6 44.16 2.94 2.0510 -2 5 5 6 44.76 2.30 2.0249 2 4 4 6 45.77 13.42 1.9823 0 6 3 6 45.77 9.36 1.9823 6 0 3 6 46.41 6.04 1.9564 5 1 4 6 47.18 1.86 1.9263 7 -1 2 6 47.40 3.30 1.9179 2 5 3 6 47.40 3.76 1.9179 7 -2 3 6 47.40 4.89 1.9179 5 2 3 6 47.46 4.52 1.9158 5 0 5 6 47.54 2.23 1.9126 0 2 7 6 48.96 5.50 1.8604 3 5 1 6 48.96 1.68 1.8604 7 0 1 6 49.04 13.72 1.8574 6 -2 5 6 49.60 9.90 1.8380 4 3 4 6 50.33 3.30 1.8129 8 -3 2 6 50.33 2.48 1.8129 5 3 2 6 50.44 1.24 1.8093 -1 5 6 6 50.44 2.53 1.8093 5 -1 6 6 50.51 2.60 1.8068 6 2 1 6 50.59 3.31 1.8042 -1 6 5 6 51.85 4.70 1.7633 2 6 2 6 52.06 1.01 1.7568 8 -4 3 6 52.06 1.89 1.7568 4 4 3 6 52.19 5.62 1.7527 -1 4 7 6 52.19 1.63 1.7527 1 3 7 6 52.59 5.57 1.7403 1 7 0 6 52.59 4.00 1.7403 7 1 0 6 52.64 4.58 1.7387 1 6 4 6 52.80 1.80 1.7340 0 1 8 6 53.59 2.82 1.7100 -3 7 5 6 54.27 3.61 1.6904 2 0 8 6 54.97 4.26 1.6703 9 -4 1 6 55.13 12.55 1.6660 3 2 7 6 55.51 2.97 1.6554 3 6 0 6 55.56 4.99 1.6540 -3 8 4 6 56.43 7.98 1.6306 -1 8 3 6 56.43 7.96 1.6306 7 1 3 6 56.48 1.28 1.6292 7 -1 5 6 56.48 1.46 1.6292 6 1 5 6 56.98 7.08 1.6161 8 -2 4 6 57.75 2.69 1.5965 6 0 6 6 57.96 2.91 1.5911 0 5 7 6 58.53 5.86 1.5770 4 -1 8 6 59.14 1.92 1.5622 5 2 6 6 59.14 1.87 1.5622 -2 7 6 6 59.23 2.86 1.5601 -3 9 3 6 59.23 2.91 1.5601 3 6 3 6 59.23 1.29 1.5601 6 3 3 6 59.23 2.49 1.5601 9 -3 3 6 59.35 1.28 1.5572 2 4 7 6 59.91 4.86 1.5440 0 4 8 6 60.57 1.20 1.5286 9 -1 1 6 60.64 2.64 1.5270 -2 8 5 6 60.72 4.90 1.5254 5 1 7 6 60.81 4.97 1.5232 2 -1 9 6 61.12 4.14 1.5161 9 -4 4 6 61.27 5.59 1.5130 -2 5 8 6 61.76 1.82 1.5020 1 8 2 6 61.92 6.77 1.4985 -4 10 1 6 63.10 2.86 1.4734 6 4 2 6 63.26 3.38 1.4701 10 -3 1 6 63.26 1.18 1.4701 7 3 1 6 63.39 2.11 1.4672 4 3 7 6 63.39 2.07 1.4672 7 -3 7 6 63.49 2.90 1.4653 3 0 9 6 63.75 2.14 1.4599 9 0 0 6 63.93 1.93 1.4561 5 0 8 6 64.64 1.08 1.4419 4 5 5 6 65.06 1.41 1.4336 2 8 0 6 65.06 7.28 1.4336 8 2 0 6 67.10 1.69 1.3948 -1 8 6 6 67.10 3.67 1.3948 1 7 6 6 67.10 2.16 1.3948 8 -1 6 6 67.19 1.12 1.3933 0 9 3 6 67.19 1.59 1.3933 9 0 3 6 67.23 1.68 1.3925 7 2 5 6 68.44 1.85 1.3708 1 9 1 6 68.47 1.15 1.3704 2 8 3 6 68.47 1.83 1.3704 10 -2 3 6 68.58 3.28 1.3684 3 5 7 6 69.10 1.43 1.3594 -3 7 8 6 69.56 5.03 1.3514 5 6 2 6 69.78 2.77 1.3478 1 8 5 6 69.83 2.78 1.3469 2 1 10 6 72.28 1.89 1.3072 3 7 5 6 72.33 1.02 1.3064 -1 4 10 6 73.58 4.55 1.2872 9 -4 7 6 75.91 1.03 1.2535 -5 12 1 6 76.12 2.14 1.2505 -2 7 9 6 76.36 1.39 1.2471 1 10 0 6 76.41 2.49 1.2465 -3 11 4 6 77.13 2.66 1.2367 8 4 1 6 77.19 1.68 1.2358 5 6 5 6 77.62 1.60 1.2300 10 0 4 6 78.19 1.36 1.2225 4 8 2 6 78.19 1.02 1.2225 -4 12 2 6 78.28 1.29 1.2213 8 2 6 6 78.45 1.02 1.2191 2 4 10 6 78.79 1.87 1.2147 3 9 0 6 78.83 1.61 1.2142 9 2 4 6 78.83 2.00 1.2142 11 -2 4 6 79.61 1.18 1.2043 11 -3 5 6 79.67 1.50 1.2035 -4 10 7 6 79.86 2.21 1.2011 3 1 11 6 79.86 1.04 1.2011 4 -1 11 6 81.36 1.20 1.1827 9 -2 8 6 83.34 1.62 1.1595 7 1 9 6 83.34 2.07 1.1595 8 -1 9 6 83.95 1.98 1.1526 1 1 12 6 84.39 2.40 1.1478 7 5 5 6 84.93 1.10 1.1418 6 4 8 6 85.51 1.22 1.1356 11 1 1 6 85.58 1.13 1.1349 4 8 5 6 85.83 1.62 1.1322 6 -2 11 6 86.12 1.87 1.1291 3 7 8 6 86.33 1.24 1.1269 0 3 12 6 87.01 2.16 1.1198 -1 6 11 6 87.18 4.22 1.1181 2 10 4 6 89.13 2.04 1.0986 11 0 5 6 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.