H13 N2 O10 P2 Te0.5 Averbuch-Pouchot M, Durif A Acta Crystallographica C48 (1992) 973-975 Structure of an adduct between diammonium dihydrogenphosphate and telluric acid: (NH4)2H2P2O7. Te(OH)6 _cod_database_code 1007225 _database_code_amcsd 0015907 CELL PARAMETERS: 7.6510 21.7900 6.6890 90.000 113.850 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 1019.932 Density (g/cm3): 2.128 MAX. ABS. INTENSITY / VOLUME**2: 11.36791289 RIR: 1.739 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.12 15.24 10.8950 0 2 0 2 13.29 20.87 6.6625 1 1 0 4 14.89 2.04 5.9496 -1 0 1 2 15.04 34.50 5.8901 0 1 1 4 15.05 9.23 5.8878 1 2 0 4 15.44 9.63 5.7395 -1 1 1 4 16.27 17.94 5.4475 0 4 0 2 16.62 13.44 5.3344 0 2 1 4 16.98 87.72 5.2218 -1 2 1 4 17.60 100.00 5.0394 1 3 0 4 18.97 16.69 4.6792 0 3 1 4 19.28 8.89 4.6026 -1 3 1 4 22.12 7.44 4.0178 -1 4 1 4 22.85 14.10 3.8916 1 0 1 2 24.00 39.81 3.7080 -2 1 1 4 24.06 9.25 3.6993 1 5 0 4 24.29 38.47 3.6648 1 2 1 4 25.09 52.24 3.5495 0 5 1 4 25.33 3.61 3.5157 -1 5 1 4 25.46 11.82 3.4988 2 0 0 2 25.79 4.72 3.4546 2 1 0 4 25.98 1.12 3.4303 1 3 1 4 26.68 1.59 3.3411 -2 3 1 4 26.76 1.92 3.3313 2 2 0 4 26.99 25.11 3.3037 -1 1 2 4 27.67 2.08 3.2234 1 6 0 4 27.92 2.59 3.1954 -1 2 2 4 28.18 2.85 3.1666 1 4 1 4 28.58 6.22 3.1229 0 6 1 4 28.80 17.11 3.0998 -1 6 1 4 29.19 1.70 3.0589 0 0 2 2 29.42 11.14 3.0363 -1 3 2 4 30.32 1.96 2.9475 -2 1 2 4 30.36 8.52 2.9439 2 4 0 4 31.41 12.55 2.8481 -2 5 1 4 31.45 2.53 2.8441 1 7 0 4 31.74 2.59 2.8191 0 3 2 4 32.27 2.00 2.7744 0 7 1 4 32.46 1.30 2.7582 -1 7 1 4 32.83 2.65 2.7283 2 5 0 4 33.60 16.09 2.6672 0 4 2 4 33.76 6.28 2.6551 1 6 1 4 34.32 2.68 2.6131 -2 6 1 4 34.35 6.61 2.6109 -2 4 2 4 34.54 5.11 2.5968 2 1 1 4 36.18 5.13 2.4825 -3 2 1 4 36.27 5.63 2.4766 -1 8 1 4 36.51 4.23 2.4608 2 3 1 4 36.98 4.41 2.4309 1 7 1 4 38.48 5.47 2.3396 0 6 2 4 38.83 14.83 2.3193 3 1 0 4 39.01 4.91 2.3091 -3 4 1 4 39.14 16.50 2.3013 -2 6 2 4 39.51 1.00 2.2809 3 2 0 4 39.56 8.39 2.2779 -1 7 2 4 39.94 1.30 2.2571 -3 3 2 4 40.05 4.92 2.2512 0 9 1 4 40.21 4.05 2.2426 2 5 1 4 40.62 1.40 2.2208 3 3 0 4 41.47 2.99 2.1774 -2 1 3 4 42.17 2.98 2.1431 1 5 2 4 44.05 1.66 2.0557 1 9 1 4 44.18 4.81 2.0502 -1 4 3 4 44.27 3.16 2.0461 -1 10 1 4 44.50 1.10 2.0361 -2 9 1 4 44.54 3.05 2.0342 0 8 2 4 44.63 1.82 2.0304 0 1 3 4 46.30 4.39 1.9607 -1 9 2 4 46.43 4.98 1.9557 -2 5 3 4 46.55 1.51 1.9511 -3 2 3 4 46.68 1.12 1.9458 2 0 2 2 46.88 1.83 1.9381 2 1 2 4 47.07 5.26 1.9307 1 7 2 4 47.46 1.25 1.9155 2 2 2 4 47.72 1.93 1.9060 1 11 0 4 47.75 3.68 1.9048 3 2 1 4 48.15 2.55 1.8898 -4 1 1 4 48.15 9.37 1.8897 -1 6 3 4 48.20 7.30 1.8880 -3 7 2 4 48.29 2.19 1.8846 0 11 1 4 48.38 1.71 1.8814 -4 0 2 2 48.79 3.57 1.8666 3 7 0 4 48.87 1.37 1.8636 -3 4 3 4 48.93 1.38 1.8613 -3 8 1 4 49.26 1.94 1.8496 2 10 0 4 49.67 1.54 1.8354 -4 3 1 4 49.76 2.45 1.8324 2 4 2 4 50.03 1.87 1.8231 3 4 1 4 50.24 1.33 1.8158 0 12 0 2 51.01 1.91 1.7903 -2 7 3 4 51.38 1.30 1.7784 -4 4 2 4 51.43 1.29 1.7767 2 9 1 4 51.49 1.43 1.7748 0 10 2 4 52.02 4.07 1.7579 -2 10 2 4 52.23 1.28 1.7515 1 2 3 4 52.62 2.82 1.7393 -4 5 1 4 52.70 2.40 1.7367 -1 12 1 4 53.02 2.20 1.7273 4 2 0 4 53.34 1.31 1.7175 -1 8 3 4 53.68 2.57 1.7075 3 6 1 4 53.79 3.23 1.7041 -1 11 2 4 54.94 2.76 1.6712 -2 0 4 2 54.96 1.30 1.6706 -4 6 2 4 55.14 4.56 1.6656 4 4 0 4 55.64 2.38 1.6519 -2 2 4 4 56.28 1.05 1.6347 -4 4 3 4 56.45 1.58 1.6300 1 13 0 4 56.70 5.05 1.6235 -2 9 3 4 56.96 1.09 1.6166 0 13 1 4 57.48 1.51 1.6032 -3 8 3 4 57.66 1.06 1.5986 -1 3 4 4 57.82 3.23 1.5948 -4 5 3 4 57.83 1.74 1.5944 1 6 3 4 57.91 1.22 1.5923 3 10 0 4 58.28 3.20 1.5833 2 8 2 4 58.65 1.22 1.5741 -3 3 4 4 59.24 3.76 1.5597 0 9 3 4 59.74 1.18 1.5480 -4 8 2 4 59.94 2.47 1.5432 1 11 2 4 60.18 1.93 1.5376 3 3 2 4 60.82 1.71 1.5230 4 1 1 4 60.90 1.18 1.5211 -3 11 2 4 61.30 1.04 1.5123 -3 5 4 4 61.40 1.31 1.5099 3 11 0 4 62.09 1.92 1.4949 -5 3 2 4 62.17 2.13 1.4932 -4 9 1 4 62.83 2.43 1.4790 -3 12 1 4 63.14 1.12 1.4725 0 4 4 4 64.17 1.22 1.4514 2 10 2 4 64.23 1.16 1.4501 -1 7 4 4 64.27 1.60 1.4493 -5 2 3 4 64.66 1.23 1.4416 -5 5 2 4 65.18 2.57 1.4313 2 5 3 4 65.55 2.59 1.4241 -4 10 2 4 65.64 1.01 1.4223 1 15 0 4 66.22 1.37 1.4112 2 13 1 4 66.60 1.19 1.4041 3 7 2 4 66.62 3.12 1.4037 -1 12 3 4 67.01 1.18 1.3967 5 1 0 4 67.97 1.02 1.3791 -2 14 2 4 68.41 1.28 1.3714 -5 7 2 4 68.95 1.17 1.3619 0 16 0 2 69.27 1.31 1.3565 -5 6 3 4 70.71 1.13 1.3323 -1 15 2 4 71.68 1.22 1.3167 -3 2 5 4 73.31 1.10 1.2914 4 9 1 4 73.51 1.39 1.2884 -5 8 3 4 73.70 1.61 1.2854 1 16 1 4 74.28 1.70 1.2768 -2 5 5 4 75.22 1.15 1.2632 1 7 4 4 76.12 1.39 1.2505 -3 11 4 4 77.47 1.06 1.2320 3 11 2 4 82.33 1.63 1.1712 3 8 3 4 83.05 1.26 1.1628 4 14 0 4 83.29 1.17 1.1601 -6 4 4 4 85.20 1.07 1.1390 -2 14 4 4 86.59 1.07 1.1242 1 2 5 4 86.74 1.26 1.1227 -3 16 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.