O10 P2 Pb V2 Grandin A, Chardon J, Borel M, Leclaire A, Raveau B Acta Crystallographica C48 (1992) 1913-1915 Structure of PbV2P2O10 _cod_database_code 1001534 _database_code_amcsd 0010277 CELL PARAMETERS: 5.2306 8.5805 16.7900 90.000 91.010 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 753.438 Density (g/cm3): 4.681 MAX. ABS. INTENSITY / VOLUME**2: 27.75403062 RIR: 1.931 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.54 59.98 8.3937 0 0 2 2 11.58 17.34 7.6403 0 1 1 4 14.76 41.80 6.0002 0 1 2 4 16.95 21.19 5.2298 1 0 0 2 18.93 5.20 4.6871 0 1 3 4 19.88 34.61 4.4657 1 1 0 4 20.16 39.91 4.4040 1 0 2 2 20.50 30.65 4.3318 -1 1 1 4 20.66 11.03 4.2996 1 1 1 4 20.70 28.75 4.2902 0 2 0 2 21.17 5.96 4.1968 0 0 4 2 21.38 18.22 4.1567 0 2 1 4 22.41 85.05 3.9673 -1 1 2 4 22.70 14.60 3.9181 1 1 2 4 23.60 75.69 3.7700 0 1 4 4 25.33 4.24 3.5163 -1 1 3 4 25.71 17.74 3.4651 1 1 3 4 26.17 7.65 3.4047 0 2 3 4 26.88 64.93 3.3169 1 2 0 4 27.35 25.03 3.2610 -1 2 1 4 27.47 9.71 3.2471 1 2 1 4 27.48 1.92 3.2454 1 0 4 2 28.55 4.50 3.1266 0 1 5 4 28.98 100.00 3.0815 -1 1 4 4 29.06 73.20 3.0731 1 2 2 4 29.42 73.09 3.0355 1 1 4 4 29.78 5.38 3.0001 0 2 4 4 31.19 1.99 2.8674 -1 2 3 4 31.51 30.28 2.8394 1 2 3 4 31.74 15.48 2.8195 0 3 1 4 31.99 31.72 2.7979 0 0 6 2 33.09 24.33 2.7073 0 3 2 4 33.69 11.40 2.6601 0 1 6 4 33.90 5.44 2.6441 0 2 5 4 34.27 13.86 2.6166 -1 2 4 4 34.29 7.77 2.6149 2 0 0 2 34.66 1.24 2.5883 1 2 4 4 35.24 20.49 2.5468 0 3 3 4 35.78 1.47 2.5094 1 3 0 4 35.79 2.28 2.5091 -2 0 2 2 36.14 3.71 2.4853 -1 0 6 2 36.15 18.77 2.4849 -1 3 1 4 36.16 30.63 2.4841 2 0 2 2 36.22 3.28 2.4801 -2 1 1 4 36.40 2.07 2.4680 2 1 1 4 37.31 2.20 2.4099 -1 3 2 4 37.34 33.69 2.4083 -2 1 2 4 37.92 18.22 2.3729 -1 2 5 4 38.07 6.47 2.3635 0 3 4 4 38.22 31.37 2.3551 1 1 6 4 38.41 6.93 2.3436 0 2 6 4 39.20 1.22 2.2980 -2 1 3 4 39.22 10.20 2.2970 -1 3 3 4 39.48 5.22 2.2825 1 3 3 4 40.32 10.02 2.2371 -2 0 4 2 40.40 4.82 2.2328 2 2 0 4 40.85 18.60 2.2090 2 2 1 4 40.99 2.01 2.2020 2 0 4 2 41.47 19.31 2.1773 0 3 5 4 41.72 6.15 2.1648 -2 1 4 4 41.78 6.03 2.1618 -1 3 4 4 42.01 17.30 2.1505 -1 2 6 4 42.03 19.46 2.1498 2 2 2 4 42.38 6.74 2.1329 2 1 4 4 42.48 20.03 2.1278 0 4 1 4 42.50 4.29 2.1270 1 2 6 4 42.52 3.35 2.1262 -1 1 7 4 43.08 1.99 2.0997 1 1 7 4 43.11 10.35 2.0984 0 0 8 2 43.22 7.63 2.0933 0 2 7 4 43.41 1.61 2.0847 -2 2 3 4 43.55 3.63 2.0783 0 4 2 4 43.88 4.15 2.0632 2 2 3 4 44.45 3.88 2.0384 0 1 8 4 44.82 3.78 2.0223 -2 1 5 4 44.91 11.01 2.0182 -1 3 5 4 45.27 3.27 2.0030 0 4 3 4 45.30 3.81 2.0019 1 3 5 4 45.34 1.43 2.0001 0 3 6 4 45.74 2.48 1.9836 -2 2 4 4 46.01 15.30 1.9725 -1 4 1 4 46.09 14.21 1.9694 1 4 1 4 46.34 9.55 1.9595 -1 0 8 2 46.35 6.53 1.9590 2 2 4 4 46.48 2.94 1.9538 -1 2 7 4 46.94 8.74 1.9357 1 0 8 2 47.00 7.12 1.9332 1 2 7 4 47.09 3.46 1.9299 2 3 0 4 47.15 20.11 1.9275 -2 0 6 2 47.34 20.28 1.9201 -2 3 1 4 47.49 1.98 1.9145 2 3 1 4 47.60 5.58 1.9103 -1 1 8 4 48.25 7.78 1.8862 -2 3 2 4 48.28 10.22 1.8850 0 2 8 4 48.40 1.51 1.8806 -2 1 6 4 48.63 8.15 1.8723 -2 2 5 4 48.79 4.33 1.8666 1 4 3 4 48.96 2.60 1.8603 1 3 6 4 49.27 15.83 1.8493 2 1 6 4 49.78 2.67 1.8318 -2 3 3 4 50.21 11.72 1.8172 2 3 3 4 50.49 7.21 1.8077 0 4 5 4 51.26 2.84 1.7824 -1 2 8 4 51.81 10.86 1.7645 1 2 8 4 51.89 1.34 1.7621 -2 3 4 4 52.01 4.53 1.7582 -2 2 6 4 52.44 5.69 1.7448 2 3 4 4 52.91 2.39 1.7304 -1 1 9 4 53.04 6.49 1.7265 1 3 7 4 53.37 4.25 1.7167 2 1 7 4 53.48 7.89 1.7135 -1 4 5 4 53.65 12.03 1.7084 3 1 0 4 53.69 1.60 1.7072 0 5 1 4 53.81 2.48 1.7035 1 4 5 4 53.85 1.30 1.7025 -3 1 1 4 53.85 2.43 1.7024 0 4 6 4 53.90 4.71 1.7009 3 0 2 2 54.05 1.31 1.6966 3 1 1 4 54.21 3.89 1.6919 0 3 8 4 54.58 1.09 1.6813 0 5 2 4 54.64 13.02 1.6797 -3 1 2 4 55.20 5.36 1.6639 2 3 5 4 55.76 5.55 1.6486 2 4 1 4 55.80 2.23 1.6475 0 1 10 4 56.01 2.04 1.6419 -3 1 3 4 56.05 4.90 1.6407 0 5 3 4 56.32 1.71 1.6336 -1 2 9 4 56.60 2.46 1.6261 3 1 3 4 56.69 6.84 1.6238 -1 5 1 4 56.73 3.66 1.6227 2 0 8 2 56.75 6.31 1.6221 2 2 7 4 56.79 2.25 1.6211 -2 1 8 4 56.90 2.66 1.6181 1 2 9 4 57.02 1.31 1.6150 3 2 0 4 57.49 1.26 1.6031 1 3 8 4 57.61 3.47 1.5999 3 0 4 2 57.65 2.18 1.5990 1 5 2 4 57.65 8.84 1.5988 0 4 7 4 57.98 2.71 1.5908 -3 2 2 4 58.00 2.09 1.5903 1 0 10 2 58.07 2.89 1.5884 0 5 4 4 58.20 4.71 1.5853 2 4 3 4 58.36 6.08 1.5812 3 2 2 4 58.44 10.15 1.5792 -1 1 10 4 58.45 1.77 1.5791 2 3 6 4 58.91 10.21 1.5678 -1 5 3 4 59.08 3.04 1.5636 1 1 10 4 59.09 4.49 1.5633 0 2 10 4 59.10 5.98 1.5631 1 5 3 4 59.13 7.27 1.5624 0 3 9 4 59.29 3.29 1.5585 -3 2 3 4 59.72 2.70 1.5483 -2 4 4 4 59.87 2.50 1.5450 3 2 3 4 60.05 3.14 1.5407 -2 2 8 4 60.34 4.61 1.5340 -1 4 7 4 60.60 3.95 1.5281 0 5 5 4 60.78 6.53 1.5240 1 4 7 4 61.05 1.95 1.5178 2 2 8 4 61.15 4.18 1.5156 -3 2 4 4 61.26 6.51 1.5132 -2 3 7 4 61.31 1.60 1.5121 3 1 5 4 61.51 1.74 1.5075 -2 1 9 4 61.64 1.01 1.5046 -1 2 10 4 61.71 5.74 1.5031 -1 3 9 4 61.74 1.39 1.5025 0 1 11 4 61.90 2.62 1.4991 3 2 4 4 62.13 2.94 1.4941 2 3 7 4 62.15 6.91 1.4936 -2 4 5 4 62.25 3.91 1.4914 -3 0 6 2 62.56 1.34 1.4847 -3 3 1 4 62.63 1.29 1.4833 2 1 9 4 62.75 5.32 1.4808 3 3 1 4 62.77 4.23 1.4804 2 4 5 4 63.26 1.66 1.4699 -1 5 5 4 63.29 4.20 1.4694 -3 1 6 4 63.57 11.71 1.4636 1 5 5 4 64.35 1.16 1.4478 0 3 10 4 64.39 7.12 1.4470 3 1 6 4 64.43 3.77 1.4462 3 2 5 4 64.54 1.50 1.4439 -3 3 3 4 64.88 1.05 1.4371 1 4 8 4 65.21 3.87 1.4307 -2 5 1 4 65.24 1.20 1.4301 0 6 0 2 65.26 4.47 1.4298 -2 3 8 4 65.51 5.44 1.4249 0 6 1 4 65.55 2.81 1.4241 -2 0 10 2 65.95 1.45 1.4165 -2 5 2 4 66.22 1.30 1.4114 2 3 8 4 66.36 4.50 1.4087 -3 2 6 4 66.42 4.06 1.4076 0 4 9 4 66.56 4.09 1.4049 -2 1 10 4 66.67 1.59 1.4029 -3 1 7 4 66.74 4.05 1.4015 2 0 10 2 66.78 1.95 1.4008 -1 3 10 4 67.20 3.09 1.3930 -2 5 3 4 67.56 1.08 1.3865 2 5 3 4 67.88 8.73 1.3807 0 1 12 4 67.89 2.24 1.3806 1 2 11 4 67.95 2.46 1.3794 1 6 0 4 68.24 3.22 1.3743 1 6 1 4 68.42 1.99 1.3713 -2 4 7 4 69.05 2.24 1.3602 1 6 2 4 69.24 2.25 1.3570 2 4 7 4 69.37 1.50 1.3547 1 4 9 4 69.45 1.26 1.3533 3 3 5 4 69.65 2.78 1.3500 -2 3 9 4 69.82 2.70 1.3470 3 4 1 4 69.86 3.35 1.3464 0 3 11 4 69.95 1.37 1.3450 1 5 7 4 70.20 2.22 1.3407 -1 1 12 4 70.37 1.62 1.3379 1 6 3 4 70.47 3.86 1.3362 -3 1 8 4 70.72 3.43 1.3322 2 2 10 4 70.89 3.50 1.3293 1 1 12 4 71.22 1.57 1.3239 -2 5 5 4 71.52 4.19 1.3191 -3 4 3 4 71.74 1.59 1.3157 0 6 5 4 71.80 1.66 1.3147 2 5 5 4 71.86 2.42 1.3138 3 1 8 4 72.04 5.53 1.3109 3 4 3 4 72.17 1.47 1.3088 -1 3 11 4 72.26 1.28 1.3074 4 0 0 2 72.35 1.53 1.3060 3 3 6 4 72.80 5.54 1.2991 1 3 11 4 73.12 3.26 1.2942 -1 2 12 4 73.23 5.64 1.2925 4 1 0 4 73.50 3.08 1.2884 4 0 2 2 73.95 1.40 1.2817 -2 5 6 4 74.01 1.42 1.2808 -4 1 2 4 74.52 2.77 1.2734 -3 3 7 4 74.63 1.78 1.2717 2 5 6 4 74.76 1.34 1.2699 3 2 8 4 75.24 1.67 1.2629 0 5 9 4 75.39 4.54 1.2608 -3 4 5 4 75.71 2.59 1.2563 3 3 7 4 75.83 3.64 1.2546 -4 0 4 2 76.13 6.79 1.2504 2 6 1 4 76.47 1.04 1.2456 4 2 1 4 76.69 1.29 1.2427 -2 0 12 2 76.73 2.43 1.2421 4 0 4 2 76.92 1.28 1.2395 -1 6 6 4 77.14 1.49 1.2365 -2 5 7 4 77.33 1.10 1.2340 4 2 2 4 77.43 2.46 1.2326 2 4 9 4 77.55 5.13 1.2310 -1 5 9 4 77.75 2.24 1.2283 0 6 7 4 77.89 1.13 1.2265 -2 6 3 4 77.92 2.80 1.2260 2 5 7 4 78.00 2.50 1.2250 -4 2 3 4 78.17 1.24 1.2228 -3 3 8 4 78.22 2.34 1.2221 2 6 3 4 78.32 4.66 1.2208 -3 5 1 4 78.49 2.79 1.2186 3 5 1 4 78.98 2.50 1.2123 2 1 12 4 79.06 1.50 1.2112 3 2 9 4 79.32 4.20 1.2079 -1 2 13 4 79.32 1.71 1.2079 -3 1 10 4 79.62 2.20 1.2041 -4 2 4 4 80.02 1.47 1.1991 0 0 14 2 80.05 2.28 1.1987 3 0 10 2 80.10 4.32 1.1982 -1 6 7 4 80.12 1.54 1.1978 -3 5 3 4 80.16 3.09 1.1974 0 7 3 4 80.46 1.19 1.1936 -2 2 12 4 80.48 1.14 1.1933 1 6 7 4 80.79 1.22 1.1896 2 3 11 4 80.83 1.26 1.1891 4 3 0 4 80.96 2.67 1.1875 -4 3 1 4 81.19 3.33 1.1848 4 3 1 4 81.40 2.20 1.1822 -1 7 2 4 81.48 1.63 1.1812 -4 1 6 4 81.70 4.28 1.1786 -2 6 5 4 81.71 1.17 1.1785 -4 2 5 4 81.87 2.02 1.1766 0 7 4 4 82.15 1.04 1.1733 -1 0 14 2 82.25 1.78 1.1721 -3 3 9 4 82.59 1.92 1.1682 -1 7 3 4 82.81 1.98 1.1657 4 1 6 4 82.92 1.31 1.1643 1 0 14 2 83.73 1.55 1.1552 -1 6 8 4 83.74 2.39 1.1550 3 3 9 4 83.76 1.78 1.1548 0 2 14 4 83.79 2.10 1.1545 3 2 10 4 83.86 2.13 1.1537 1 1 14 4 84.17 1.31 1.1502 1 6 8 4 84.27 1.48 1.1491 -1 7 4 4 84.33 1.32 1.1485 -2 6 6 4 84.49 2.55 1.1467 1 7 4 4 84.68 1.66 1.1446 3 5 5 4 84.71 1.37 1.1443 1 3 13 4 84.86 1.31 1.1426 -2 5 9 4 85.06 2.14 1.1404 0 5 11 4 85.13 2.19 1.1396 2 1 13 4 85.57 1.47 1.1349 0 6 9 4 85.60 1.36 1.1347 4 2 6 4 86.10 2.67 1.1293 -2 4 11 4 86.36 1.15 1.1266 -4 3 5 4 86.44 1.06 1.1257 2 3 12 4 86.49 1.69 1.1252 -2 2 13 4 86.70 1.94 1.1231 1 7 5 4 86.73 1.59 1.1228 0 7 6 4 87.15 2.08 1.1184 -3 2 11 4 87.26 2.09 1.1173 -1 5 11 4 87.31 3.35 1.1168 2 4 11 4 87.42 1.21 1.1156 -2 6 7 4 87.86 3.35 1.1112 1 5 11 4 87.99 1.33 1.1099 2 7 0 4 88.06 1.50 1.1092 -4 1 8 4 88.18 1.17 1.1080 -2 7 1 4 88.19 2.16 1.1079 2 6 7 4 88.31 2.63 1.1066 1 6 9 4 88.34 2.58 1.1063 0 4 13 4 88.91 1.40 1.1007 -4 3 6 4 88.93 1.53 1.1006 -3 0 12 2 89.19 2.11 1.0980 -4 4 3 4 89.51 2.42 1.0950 -3 5 7 4 89.55 1.58 1.0946 3 6 2 4 89.81 3.37 1.0920 4 1 8 4 89.85 1.29 1.0917 4 4 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.