H42 N8 O32 P8 Te Averbuch-Pouchot M, Durif A Acta Crystallographica C49 (1993) 361-363 Ammonium cyclo-octaphosphate-telluric acid dihydrate adduct _cod_database_code 1007210 _database_code_amcsd 0010281 CELL PARAMETERS: 15.1460 11.0490 12.1890 117.150 109.720 90.540 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1675.779 Density (g/cm3): 2.064 MAX. ABS. INTENSITY / VOLUME**2: 4.342776124 RIR: 0.685 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.66 33.84 10.2060 -1 0 1 2 10.08 45.35 8.7789 -1 1 0 2 12.12 39.01 7.3006 1 1 0 2 12.66 8.09 6.9919 2 0 0 2 12.70 99.43 6.9723 1 0 1 2 14.25 100.00 6.2151 -2 -1 1 2 14.68 1.06 6.0349 -1 -1 2 2 15.56 8.81 5.6946 0 1 1 2 16.47 39.45 5.3811 -2 1 1 2 16.88 1.04 5.2519 2 -1 1 2 17.19 46.09 5.1583 1 -2 1 2 17.33 32.08 5.1174 -1 -2 1 2 17.38 4.35 5.1030 -2 0 2 2 17.64 12.49 5.0289 -3 0 1 2 17.71 19.53 5.0071 0 0 2 2 18.28 1.36 4.8527 0 -2 2 2 18.40 60.47 4.8213 0 2 0 2 18.53 66.56 4.7885 1 -1 2 2 19.47 26.50 4.5596 -3 1 0 2 20.23 9.30 4.3895 -2 2 0 2 20.29 44.55 4.3763 -3 -1 2 2 20.36 27.56 4.3622 -2 -2 2 2 22.15 33.15 4.0124 -1 1 2 2 22.40 39.25 3.9684 -2 -1 3 2 22.42 1.28 3.9655 -2 1 2 2 22.75 31.39 3.9085 3 1 0 2 22.94 55.11 3.8765 -1 -2 3 2 23.03 2.37 3.8618 -1 2 1 2 23.68 1.20 3.7566 0 1 2 2 23.95 26.71 3.7151 3 0 1 2 24.09 10.53 3.6939 2 -2 2 2 24.38 9.94 3.6503 2 2 0 2 24.43 22.08 3.6443 -3 1 2 2 24.54 1.01 3.6270 0 -3 2 2 24.61 10.04 3.6171 0 -3 1 2 24.84 1.68 3.5845 -4 0 2 2 24.93 18.72 3.5713 -1 0 3 2 25.00 3.29 3.5614 -1 -3 2 2 25.05 35.77 3.5546 -4 1 1 2 25.14 2.43 3.5422 -3 -2 1 2 25.48 2.51 3.4960 4 0 0 2 25.52 9.10 3.4906 -4 -1 1 2 25.73 19.38 3.4623 1 -3 2 2 26.19 1.10 3.4020 -3 0 3 2 26.68 45.20 3.3408 1 2 1 2 26.72 4.07 3.3363 1 1 2 2 26.82 1.23 3.3241 2 -3 1 2 27.23 5.14 3.2751 -1 3 0 2 27.57 12.87 3.2352 0 -3 3 2 28.32 3.56 3.1516 3 -1 2 2 28.46 8.44 3.1358 -4 2 0 2 28.62 11.92 3.1188 4 -1 1 2 29.61 18.02 3.0174 -2 -2 4 2 29.67 3.72 3.0112 -2 2 2 2 29.68 19.41 3.0097 -5 0 1 2 29.71 8.37 3.0071 1 3 0 2 29.81 2.85 2.9973 1 0 3 2 29.98 12.32 2.9802 -2 1 3 2 30.33 14.72 2.9466 -3 -3 2 2 30.55 45.87 2.9263 -3 3 0 2 30.68 17.09 2.9142 2 -1 3 2 30.70 23.81 2.9126 -5 -1 2 2 30.81 10.49 2.9020 -3 -1 4 2 31.20 17.93 2.8667 0 -2 4 2 32.14 5.21 2.7852 3 -3 2 2 32.20 8.54 2.7800 -5 1 2 2 32.41 1.87 2.7620 0 -4 2 2 32.47 11.81 2.7571 2 -3 3 2 32.95 1.45 2.7185 -5 0 3 2 33.17 2.71 2.7008 0 3 1 2 33.30 6.38 2.6905 -4 2 2 2 33.39 2.77 2.6833 -4 -2 4 2 33.61 8.85 2.6666 1 -4 1 2 33.62 1.61 2.6657 -1 -4 3 2 34.11 3.63 2.6289 -5 2 1 2 34.30 1.93 2.6147 -4 -3 3 2 34.34 7.49 2.6117 -5 -2 3 2 34.76 1.04 2.5808 3 -2 3 2 34.80 3.70 2.5778 1 -4 3 2 35.07 5.06 2.5587 -2 -4 2 2 35.11 7.24 2.5561 3 2 1 2 35.82 7.33 2.5070 5 -2 1 2 35.87 8.58 2.5035 0 0 4 2 36.17 7.48 2.4836 -5 -2 1 2 36.18 2.88 2.4825 -4 3 1 2 36.21 2.15 2.4809 -5 -1 4 2 36.46 2.87 2.4643 -6 1 1 2 36.94 15.02 2.4335 3 3 0 2 37.00 3.13 2.4299 3 -4 1 2 37.05 2.42 2.4264 0 -4 4 2 37.18 13.46 2.4180 -4 -3 1 2 37.30 3.85 2.4107 0 4 0 2 37.33 3.08 2.4090 -3 -2 5 2 37.59 5.08 2.3926 -1 -2 5 2 37.77 1.86 2.3816 -1 2 3 2 38.09 5.17 2.3625 -6 -1 1 2 38.28 15.15 2.3512 -2 -1 5 2 38.32 1.92 2.3489 -5 3 0 2 38.43 1.33 2.3423 -3 1 4 2 38.63 1.98 2.3306 6 0 0 2 38.74 1.21 2.3241 3 0 3 2 39.38 2.04 2.2880 -1 1 4 2 39.53 3.95 2.2798 -6 2 0 2 39.53 5.40 2.2797 -5 -3 2 2 39.61 5.05 2.2751 -4 -1 5 2 39.75 6.72 2.2679 0 -3 5 2 39.97 1.90 2.2555 -5 -3 4 2 40.46 7.08 2.2296 3 -4 3 2 40.47 3.30 2.2290 -4 -3 5 2 40.95 1.16 2.2038 -3 -4 1 2 41.06 5.16 2.1984 -6 2 2 2 41.13 7.28 2.1947 -4 4 0 2 41.21 1.18 2.1904 -1 -4 5 2 41.30 1.56 2.1860 1 -5 2 2 41.38 7.05 2.1818 -5 2 3 2 41.40 2.67 2.1811 -4 -4 4 2 41.43 10.43 2.1796 4 -4 2 2 41.43 1.19 2.1793 -1 4 1 2 41.83 1.08 2.1596 -5 1 4 2 41.96 3.87 2.1533 2 4 0 2 42.13 1.66 2.1450 -3 4 1 2 42.19 2.64 2.1420 1 -2 5 2 42.48 2.84 2.1282 1 2 3 2 42.48 3.13 2.1280 3 -3 4 2 42.61 2.87 2.1216 -7 0 1 2 42.78 1.05 2.1136 -1 -5 4 2 42.79 5.24 2.1134 2 0 4 2 43.09 2.74 2.0992 -5 3 2 2 43.53 4.28 2.0789 2 -5 3 2 44.01 1.96 2.0576 -6 3 1 2 44.26 2.04 2.0464 1 -5 4 2 44.28 1.84 2.0455 5 -4 1 2 44.39 3.50 2.0407 1 -4 5 2 45.00 1.10 2.0146 -6 -1 5 2 45.07 5.31 2.0116 -3 -3 6 2 45.20 1.17 2.0062 -2 2 4 2 45.73 1.85 1.9842 -4 -2 6 2 46.05 1.16 1.9710 5 2 1 2 46.77 7.79 1.9424 -3 -1 6 2 46.87 1.67 1.9382 -2 -4 6 2 46.92 2.45 1.9363 -2 -5 1 2 47.02 2.40 1.9326 -5 -4 5 2 47.05 1.52 1.9315 5 3 0 2 47.34 2.95 1.9204 -4 1 5 2 47.37 1.21 1.9192 -3 5 0 2 47.43 3.25 1.9167 4 2 2 2 47.62 1.54 1.9098 4 -5 1 2 47.92 1.98 1.8982 0 3 3 2 48.10 3.23 1.8918 -8 0 2 2 48.12 7.35 1.8908 -6 -3 1 2 48.21 1.78 1.8875 0 -2 6 2 48.23 2.39 1.8870 -4 -5 3 2 48.32 2.94 1.8837 1 0 5 2 48.53 2.42 1.8759 -1 -1 6 2 48.75 1.32 1.8679 -7 3 0 2 48.77 1.35 1.8672 -5 -1 6 2 48.91 1.69 1.8624 -7 2 3 2 49.06 2.97 1.8568 4 1 3 2 49.16 2.44 1.8535 -8 1 1 2 49.31 1.37 1.8482 5 -4 3 2 49.31 2.89 1.8481 -7 -3 4 2 49.34 2.42 1.8470 4 -4 4 2 49.86 2.94 1.8290 7 0 1 2 50.16 1.17 1.8187 3 3 2 2 50.23 4.62 1.8163 1 -3 6 2 50.83 3.04 1.7962 -2 5 1 2 50.89 1.00 1.7944 -7 -3 2 2 50.95 3.47 1.7923 -8 0 4 2 50.97 3.10 1.7916 6 -4 2 2 51.08 1.05 1.7882 3 -4 5 2 51.14 2.08 1.7863 2 -6 2 2 51.31 1.71 1.7807 -2 -6 4 2 51.41 3.71 1.7773 -8 2 2 2 51.42 3.65 1.7770 -5 -5 4 2 51.54 1.71 1.7733 5 -5 2 2 51.61 1.47 1.7711 -6 -4 2 2 51.68 3.22 1.7686 3 4 1 2 51.69 3.61 1.7685 -8 -2 4 2 52.06 1.60 1.7568 -8 2 0 2 52.09 2.89 1.7558 -5 5 0 2 52.25 2.27 1.7506 6 -3 3 2 52.43 5.59 1.7453 -8 -2 2 2 52.52 1.04 1.7424 0 5 1 2 52.55 1.87 1.7415 1 -6 1 2 53.28 1.85 1.7194 3 -6 3 2 53.28 1.15 1.7193 -3 -2 7 2 53.34 1.46 1.7176 -2 -6 2 2 53.47 1.04 1.7137 -8 -1 5 2 53.57 1.64 1.7108 -6 4 2 2 53.78 2.26 1.7045 1 -1 6 2 53.80 1.27 1.7038 -6 -4 6 2 53.94 1.48 1.7000 -4 -5 1 2 54.11 1.81 1.6949 1 -5 6 2 54.23 3.52 1.6914 7 -4 1 2 54.52 4.93 1.6832 -5 -5 2 2 54.58 1.97 1.6815 -7 4 1 2 54.67 3.41 1.6789 -7 -3 6 2 54.70 1.30 1.6779 -5 2 5 2 54.76 1.14 1.6763 -9 0 3 2 54.85 1.48 1.6739 -7 -4 3 2 54.97 1.85 1.6704 2 4 2 2 55.02 2.33 1.6690 0 0 6 2 55.05 1.34 1.6681 2 2 4 2 55.27 1.76 1.6621 4 -6 2 2 55.32 1.43 1.6607 -1 -2 7 2 55.73 1.70 1.6494 -4 -6 4 2 55.85 1.01 1.6462 -3 1 6 2 56.00 1.79 1.6421 -5 4 3 2 56.04 2.14 1.6410 -5 -4 7 2 56.18 1.72 1.6372 0 -3 7 2 56.44 1.68 1.6304 -2 -5 7 2 56.55 1.94 1.6274 3 0 5 2 56.59 1.88 1.6264 -2 -1 7 2 56.66 1.12 1.6246 -6 -3 7 2 56.71 1.01 1.6231 -3 5 2 2 57.33 1.26 1.6071 0 6 0 2 57.58 1.82 1.6007 -9 -2 3 2 57.76 1.76 1.5962 3 -3 6 2 57.86 1.75 1.5936 -6 5 1 2 58.34 2.31 1.5817 -1 1 6 2 58.71 2.51 1.5725 0 -7 3 2 58.91 1.34 1.5677 -1 -7 4 2 58.96 1.69 1.5666 -9 2 3 2 59.01 1.39 1.5653 7 3 0 2 59.11 4.06 1.5629 3 -6 5 2 59.26 1.06 1.5594 8 -2 2 2 59.28 1.83 1.5589 -7 2 5 2 59.80 1.83 1.5465 -3 -6 1 2 59.81 2.20 1.5464 -7 5 0 2 60.04 2.85 1.5409 1 -7 2 2 60.14 1.22 1.5386 0 -7 5 2 60.30 1.13 1.5349 -7 -5 4 2 60.39 1.63 1.5328 6 4 0 2 60.76 1.11 1.5244 -7 1 6 2 60.87 2.16 1.5219 1 2 5 2 60.96 1.69 1.5199 -9 3 0 2 61.15 1.01 1.5157 -3 6 1 2 61.54 1.67 1.5068 1 5 2 2 61.63 1.79 1.5049 -10 0 2 2 61.71 4.05 1.5032 -2 -4 8 2 62.36 1.35 1.4890 9 1 0 2 62.40 1.71 1.4882 6 -6 2 2 62.71 2.73 1.4816 4 -4 6 2 62.93 1.06 1.4769 -10 1 1 2 63.04 1.41 1.4746 4 3 3 2 63.26 1.70 1.4700 5 1 4 2 63.29 1.90 1.4693 -8 -4 2 2 63.33 1.59 1.4685 -2 -2 8 2 63.53 1.03 1.4645 -6 -5 1 2 63.84 2.32 1.4580 -7 0 7 2 63.96 2.35 1.4557 2 -5 7 2 64.21 1.57 1.4506 -6 2 6 2 64.82 1.01 1.4383 -5 -5 8 2 64.85 2.35 1.4378 8 -5 1 2 66.39 1.14 1.4081 -2 -7 7 2 66.95 1.05 1.3978 -1 7 0 2 67.43 1.04 1.3890 -8 -5 3 2 67.61 1.10 1.3857 -10 -2 6 2 68.00 2.94 1.3786 4 -6 6 2 68.50 1.17 1.3698 4 -7 5 2 68.74 1.08 1.3657 -8 3 5 2 68.81 1.23 1.3644 1 -5 8 2 68.95 1.38 1.3620 3 2 5 2 68.95 1.53 1.3619 -11 -1 4 2 69.16 1.30 1.3583 -8 -2 8 2 69.77 3.33 1.3479 -9 -4 7 2 69.88 1.10 1.3461 -7 -6 3 2 69.95 1.46 1.3449 -9 5 0 2 70.17 1.63 1.3413 10 -3 1 2 70.20 1.52 1.3407 -11 1 4 2 70.39 1.43 1.3375 -3 3 6 2 70.49 1.12 1.3360 3 -6 7 2 71.97 1.80 1.3121 2 4 4 2 72.24 2.40 1.3078 8 2 2 2 73.17 1.36 1.2935 -11 1 0 2 73.47 1.11 1.2889 2 -8 6 2 73.58 1.53 1.2873 -3 6 3 2 73.68 1.85 1.2858 1 -8 1 2 73.88 1.07 1.2828 0 7 1 2 73.90 1.04 1.2825 -11 -3 4 2 74.11 1.34 1.2794 -4 -8 4 2 75.29 1.80 1.2622 1 -7 8 2 75.47 2.18 1.2596 -1 -2 9 2 76.42 1.46 1.2463 -12 -1 3 2 77.03 1.58 1.2380 4 -1 7 2 77.44 1.05 1.2324 -2 -8 8 2 77.46 1.11 1.2322 -12 2 2 2 77.72 1.10 1.2287 -5 -8 7 2 77.96 1.35 1.2255 7 -7 4 2 80.86 1.45 1.1887 9 -5 4 2 83.12 1.09 1.1620 6 0 6 2 86.27 1.09 1.1275 3 4 5 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.