Whitlockite Tsirlin A A, Dikarev E V, Shpanchenko R V, Antipov E V Acta Crystallographica C62 (2006) i13-i15 A new whitlockite, Ca8.42Na1.16V(PO4)7 Locality: synthetic _database_code_amcsd 0010333 CELL PARAMETERS: 10.3273 10.3273 37.0980 90.000 90.000 120.000 SPACE GROUP: R3c X-RAY WAVELENGTH: 1.541838 Cell Volume: 3426.531 Density (g/cm3): 3.140 MAX. ABS. INTENSITY / VOLUME**2: 12.65021178 RIR: 1.312 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.98 23.99 8.0561 0 1 2 3 13.75 37.11 6.4379 1 0 4 3 14.32 11.18 6.1830 0 0 6 1 17.17 22.24 5.1637 1 1 0 6 20.43 2.27 4.3473 2 0 2 3 21.59 2.96 4.1168 0 1 8 3 22.07 18.17 4.0281 0 2 4 3 22.43 1.70 3.9633 1 1 6 6 26.00 18.75 3.4267 1 0 10 3 26.48 3.28 3.3665 2 1 1 6 26.81 3.55 3.3256 1 2 2 6 27.69 3.32 3.2215 1 1 9 6 28.10 48.09 3.1760 2 1 4 6 29.97 11.78 2.9812 3 0 0 3 31.33 100.00 2.8552 0 2 10 3 32.79 23.52 2.7317 1 2 8 6 33.37 4.55 2.6854 0 3 6 3 33.37 3.30 2.6854 3 0 6 3 33.79 5.70 2.6525 1 1 12 6 34.75 67.06 2.5818 2 2 0 6 35.33 3.12 2.5407 0 1 14 3 35.52 5.00 2.5273 2 2 3 6 35.94 11.29 2.4987 2 1 10 6 36.30 2.87 2.4750 1 3 1 6 37.53 1.56 2.3963 1 3 4 6 37.68 2.00 2.3875 1 2 11 6 37.76 9.52 2.3825 2 2 6 6 38.26 4.40 2.3525 3 1 5 6 39.53 1.20 2.2797 2 0 14 3 40.18 7.06 2.2444 1 0 16 3 40.44 2.51 2.2305 1 1 15 6 41.41 1.10 2.1806 2 1 13 6 41.55 8.82 2.1737 4 0 4 3 42.11 10.77 2.1460 3 0 12 3 43.39 4.17 2.0855 1 2 14 6 43.91 3.95 2.0620 1 3 10 6 43.93 2.74 2.0610 0 0 18 1 44.21 2.20 2.0487 3 2 1 6 44.42 5.45 2.0394 2 3 2 6 45.01 8.71 2.0140 0 4 8 3 45.26 5.34 2.0034 3 2 4 6 45.79 6.65 1.9817 2 2 12 6 46.53 1.15 1.9517 4 1 0 6 47.14 1.61 1.9278 1 4 3 6 47.48 21.91 1.9150 4 0 10 3 48.52 11.99 1.8764 2 3 8 6 48.94 7.94 1.8612 1 4 6 6 48.94 5.90 1.8612 4 1 6 6 50.23 4.47 1.8162 0 1 20 3 50.39 1.23 1.8109 3 1 14 6 50.85 5.13 1.7955 3 2 10 6 51.31 4.00 1.7805 5 0 2 3 51.83 3.18 1.7639 4 1 9 6 52.07 7.23 1.7564 0 5 4 3 53.22 2.27 1.7212 3 3 0 6 53.48 25.60 1.7134 2 0 20 3 54.10 6.28 1.6953 3 0 18 3 54.15 2.76 1.6939 1 3 16 6 54.25 1.22 1.6908 2 1 19 6 55.02 5.72 1.6689 5 0 8 3 55.24 2.00 1.6628 2 4 4 6 55.41 1.14 1.6582 3 3 6 6 55.70 1.27 1.6503 1 4 12 6 55.70 1.43 1.6503 4 1 12 6 56.60 1.77 1.6262 1 2 20 6 56.74 2.99 1.6223 2 3 14 6 57.17 1.36 1.6112 0 5 10 3 57.19 1.05 1.6107 2 2 18 6 57.24 2.06 1.6095 4 0 16 3 58.07 2.39 1.5883 3 3 9 6 58.09 2.25 1.5880 4 2 8 6 58.30 3.56 1.5828 5 1 4 6 58.50 1.37 1.5778 0 2 22 3 60.16 8.77 1.5381 2 4 10 6 60.23 7.40 1.5366 3 2 16 6 61.05 3.71 1.5179 1 5 8 6 61.45 2.89 1.5089 2 1 22 6 61.68 1.78 1.5038 3 3 12 6 62.29 3.77 1.4906 6 0 0 3 64.13 3.67 1.4522 4 3 4 6 65.14 1.78 1.4321 5 2 0 6 65.37 2.84 1.4276 0 4 20 3 65.91 2.61 1.4171 1 4 18 6 66.74 4.46 1.4016 3 4 8 6 67.08 1.46 1.3952 2 5 6 6 67.08 3.24 1.3952 5 2 6 6 68.15 4.30 1.3760 2 3 20 6 68.89 1.17 1.3630 1 6 1 6 71.08 1.35 1.3262 2 2 24 6 71.40 1.64 1.3211 3 3 18 6 71.81 1.94 1.3145 1 2 26 6 72.06 1.32 1.3106 1 0 28 3 72.56 1.48 1.3028 3 2 22 6 72.78 1.10 1.2995 5 2 12 6 73.34 3.55 1.2909 4 4 0 6 74.28 2.40 1.2769 3 5 1 6 74.43 3.37 1.2747 5 3 2 6 76.20 4.76 1.2493 4 2 20 6 76.76 1.13 1.2417 4 3 16 6 76.85 1.20 1.2405 5 1 19 6 77.07 1.88 1.2375 2 6 2 6 77.13 1.50 1.2366 0 0 30 1 77.49 1.96 1.2318 5 3 8 6 77.67 1.41 1.2293 6 2 4 6 79.31 1.02 1.2080 3 5 10 6 80.09 1.02 1.1982 2 6 8 6 80.66 1.56 1.1912 4 4 12 6 81.20 2.30 1.1846 7 1 0 6 81.90 1.02 1.1763 6 2 10 6 81.92 1.02 1.1761 5 2 18 6 81.92 1.88 1.1761 2 5 18 6 81.96 1.06 1.1756 1 6 16 6 82.31 1.15 1.1714 2 3 26 6 83.03 1.33 1.1631 5 1 22 6 87.09 3.36 1.1190 7 0 16 3 87.44 2.69 1.1154 5 0 26 3 87.46 5.91 1.1153 2 2 30 6 87.68 2.47 1.1130 3 2 28 6 88.36 1.72 1.1062 7 1 12 6 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.