Wolfeite Hatert F Acta Crystallographica C63 (2007) i119-i121 Fe2(PO4)(OH), a synthetic analogue of wolfeite Sample: T = 1063 K, P = 2.5 GPa Locality: synthetic _database_code_amcsd 0010339 CELL PARAMETERS: 12.2650 13.1970 9.7385 90.000 108.630 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 1493.690 Density (g/cm3): 3.978 MAX. ABS. INTENSITY / VOLUME**2: 12.72585078 RIR: 1.042 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 19.24 2.66 4.6141 0 0 2 2 20.33 13.03 4.3682 -2 2 1 4 20.40 7.35 4.3538 -2 0 2 2 22.75 4.04 3.9095 -1 2 2 4 23.94 2.28 3.7172 3 1 0 4 24.58 44.59 3.6218 2 2 1 4 25.39 1.73 3.5074 2 3 0 4 26.63 32.28 3.3472 1 2 2 4 26.68 2.77 3.3409 3 2 0 4 27.03 6.33 3.2992 0 4 0 2 28.02 1.20 3.1839 0 3 2 4 28.28 71.67 3.1558 2 0 2 2 28.34 7.23 3.1493 -3 2 2 4 28.94 90.92 3.0852 -1 4 1 4 30.58 1.01 2.9239 1 4 1 4 30.68 100.00 2.9140 -4 0 2 2 30.71 1.07 2.9116 1 3 2 4 30.75 2.43 2.9074 3 3 0 4 30.77 10.96 2.9056 4 0 0 2 31.17 24.05 2.8691 2 4 0 4 31.31 1.60 2.8569 -2 2 3 4 31.53 1.82 2.8376 4 1 0 4 32.10 63.00 2.7880 0 2 3 4 32.19 23.36 2.7807 -4 2 1 4 33.39 16.97 2.6838 0 4 2 4 34.10 16.60 2.6295 -2 4 2 4 34.49 1.06 2.6001 3 3 1 4 35.03 43.93 2.5618 -3 4 1 4 37.05 22.06 2.4265 -2 0 4 2 37.33 2.50 2.4091 3 2 2 4 37.70 6.26 2.3863 -4 2 3 4 37.85 7.73 2.3770 4 2 1 4 38.96 1.79 2.3120 -1 4 3 4 39.04 12.86 2.3071 0 0 4 2 39.07 3.31 2.3056 3 4 1 4 39.52 7.05 2.2805 2 4 2 4 39.70 5.67 2.2704 2 2 3 4 39.74 16.75 2.2679 -1 2 4 4 39.85 5.45 2.2620 -5 2 2 4 40.96 3.56 2.2033 -3 2 4 4 41.34 4.86 2.1841 -4 4 2 4 41.69 1.30 2.1664 4 0 2 2 42.24 20.29 2.1396 0 6 1 4 42.68 9.93 2.1184 1 4 3 4 42.88 1.05 2.1089 1 1 4 4 44.00 13.12 2.0578 -2 6 1 4 44.57 12.32 2.0328 -6 0 2 2 45.13 1.45 2.0091 -6 1 2 4 45.18 1.54 2.0070 -6 1 1 4 45.26 5.86 2.0033 -1 6 2 4 46.29 3.11 1.9613 2 6 1 4 46.45 7.02 1.9548 -2 4 4 4 46.78 13.82 1.9420 2 0 4 2 46.81 21.02 1.9408 -6 2 1 4 46.90 2.71 1.9371 6 0 0 2 47.31 2.02 1.9213 2 1 4 4 47.51 1.43 1.9139 1 6 2 4 47.54 2.95 1.9127 3 6 0 4 48.13 2.70 1.8907 0 4 4 4 48.87 3.43 1.8636 -6 2 3 4 49.35 3.88 1.8466 -5 4 3 4 49.47 1.42 1.8426 -1 7 1 4 50.21 9.98 1.8170 -4 4 4 4 50.51 1.15 1.8070 -2 6 3 4 50.96 1.07 1.7919 -6 0 4 2 51.05 4.95 1.7892 0 6 3 4 51.11 19.99 1.7872 -4 6 1 4 51.24 1.24 1.7829 2 5 3 4 51.35 4.93 1.7794 -4 2 5 4 51.41 3.69 1.7774 0 2 5 4 51.52 3.97 1.7739 3 4 3 4 51.58 6.75 1.7720 5 4 1 4 51.59 1.43 1.7717 4 2 3 4 53.13 1.01 1.7239 1 1 5 4 54.18 8.44 1.6928 3 2 4 4 54.77 2.31 1.6759 3 6 2 4 54.97 2.98 1.6704 6 4 0 4 55.33 1.03 1.6604 -3 4 5 4 55.36 4.01 1.6596 -1 4 5 4 55.89 1.04 1.6452 3 5 3 4 56.56 19.12 1.6271 2 6 3 4 56.80 2.03 1.6208 -1 8 1 4 57.15 13.98 1.6117 6 0 2 2 57.21 3.77 1.6101 7 2 0 4 57.54 8.01 1.6018 -3 6 4 4 57.62 1.09 1.5998 6 1 2 4 58.13 9.60 1.5869 2 8 0 4 58.22 8.36 1.5847 -4 0 6 2 58.71 9.19 1.5726 -6 2 5 4 58.82 12.81 1.5700 2 2 5 4 58.90 1.92 1.5679 -7 2 4 4 59.51 6.66 1.5533 0 8 2 4 59.74 2.16 1.5479 -1 2 6 4 59.97 5.62 1.5426 -2 8 2 4 60.07 4.86 1.5401 -5 4 5 4 60.32 4.11 1.5345 -7 4 1 4 60.38 4.95 1.5331 -8 0 2 2 61.14 11.24 1.5158 -7 4 3 4 62.44 4.69 1.4873 -5 2 6 4 63.01 3.41 1.4753 -8 2 3 4 63.25 2.04 1.4701 -1 8 3 4 63.33 7.72 1.4685 3 8 1 4 63.65 1.29 1.4619 2 8 2 4 63.83 6.32 1.4582 -2 6 5 4 63.89 1.88 1.4570 -8 0 4 2 63.94 8.22 1.4561 -6 6 3 4 63.96 2.86 1.4556 5 4 3 4 64.02 1.54 1.4544 -2 4 6 4 64.10 4.19 1.4528 8 0 0 2 64.17 4.12 1.4513 -6 0 6 2 64.33 1.45 1.4482 6 4 2 4 64.96 2.48 1.4356 -4 8 2 4 65.23 2.65 1.4303 1 2 6 4 65.33 3.28 1.4284 -4 4 6 4 65.58 4.84 1.4235 4 4 4 4 66.03 6.44 1.4148 -4 6 5 4 66.09 11.52 1.4138 0 6 5 4 66.24 5.84 1.4109 4 6 3 4 66.24 1.85 1.4108 6 2 3 4 67.18 1.38 1.3934 5 2 4 4 67.26 2.07 1.3920 7 2 2 4 67.35 2.27 1.3903 -8 4 2 4 67.60 4.22 1.3858 6 6 1 4 69.35 4.77 1.3551 -2 2 7 4 69.89 1.79 1.3459 -8 2 5 4 70.34 4.03 1.3384 -7 2 6 4 70.95 1.45 1.3284 -6 4 6 4 71.11 2.90 1.3258 -5 8 3 4 71.80 3.16 1.3148 -4 8 4 4 72.02 1.02 1.3113 1 10 0 4 72.58 2.34 1.3025 2 6 5 4 74.45 1.07 1.2744 2 4 6 4 75.73 5.40 1.2559 6 8 0 4 76.83 3.04 1.2407 -9 4 1 4 77.00 1.87 1.2384 -3 10 2 4 79.37 2.03 1.2073 6 6 3 4 79.63 1.22 1.2039 -10 0 4 2 80.25 1.87 1.1962 5 6 4 4 80.35 1.36 1.1950 -7 8 1 4 80.88 1.79 1.1885 8 4 2 4 81.80 3.19 1.1775 -5 2 8 4 82.65 4.87 1.1674 -4 6 7 4 83.11 1.15 1.1622 10 0 0 2 83.46 2.23 1.1582 8 2 3 4 83.47 2.04 1.1581 -1 10 4 4 84.24 1.63 1.1494 9 4 1 4 84.45 2.13 1.1471 -10 4 2 4 85.08 1.73 1.1403 4 8 4 4 85.60 1.32 1.1346 9 2 2 4 87.83 1.34 1.1115 5 2 6 4 89.01 1.70 1.0997 0 12 0 2 89.91 1.08 1.0911 -1 12 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.