Flinkite Kolitsch U Acta Crystallographica E57 (2001) i115-i118 Redetermination of the mixed-valence manganese arsenate flinkite, MnII2MnIII(OH)4(AsO4) Locality: synthetic _database_code_amcsd 0010370 CELL PARAMETERS: 9.4830 13.0300 5.3390 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 659.705 Density (g/cm3): 3.743 MAX. ABS. INTENSITY / VOLUME**2: 20.50678415 RIR: 1.784 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.59 1.46 6.5150 0 2 0 2 18.71 87.78 4.7415 2 0 0 2 19.93 24.65 4.4557 2 1 0 4 20.27 91.36 4.3814 1 1 1 8 23.20 32.84 3.8337 2 2 0 4 23.50 4.92 3.7861 1 2 1 8 25.12 1.25 3.5453 2 0 1 4 26.45 2.99 3.3693 0 3 1 4 27.38 2.92 3.2575 0 4 0 2 27.86 36.20 3.2027 2 3 0 4 28.11 36.42 3.1748 1 3 1 8 28.67 1.32 3.1140 2 2 1 8 32.93 27.28 2.7200 3 0 1 4 33.37 11.54 2.6849 2 4 0 4 33.57 28.15 2.6695 0 0 2 2 33.58 100.00 2.6684 1 4 1 8 33.66 9.61 2.6626 3 1 1 8 34.92 11.31 2.5696 1 0 2 4 35.61 4.44 2.5211 1 1 2 8 35.77 40.52 2.5100 3 2 1 8 36.37 3.49 2.4702 0 2 2 4 37.49 15.46 2.3987 2 4 1 8 38.44 1.40 2.3419 0 5 1 4 38.60 2.25 2.3325 4 1 0 4 38.71 14.58 2.3262 2 0 2 4 39.46 3.77 2.2838 2 5 0 4 39.64 5.03 2.2736 1 5 1 8 40.49 8.79 2.2278 4 2 0 4 41.21 13.01 2.1907 2 2 2 8 43.34 20.50 2.0879 3 4 1 8 44.17 5.58 2.0506 2 3 2 8 44.42 2.67 2.0395 3 0 2 4 45.97 11.55 1.9744 2 6 0 4 47.43 7.13 1.9168 4 4 0 4 48.06 8.33 1.8930 2 4 2 8 48.37 1.50 1.8817 3 5 1 8 49.37 2.96 1.8461 3 3 2 8 50.59 1.85 1.8041 4 4 1 8 51.56 8.55 1.7726 4 0 2 4 52.07 8.38 1.7564 4 1 2 8 52.75 6.68 1.7354 2 5 2 8 52.81 5.02 1.7336 1 1 3 8 52.98 5.01 1.7282 1 7 1 8 53.14 3.65 1.7235 5 2 1 8 53.58 11.39 1.7104 4 2 2 8 54.03 10.18 1.6971 3 6 1 8 54.30 1.13 1.6893 1 2 3 8 55.12 1.32 1.6662 2 0 3 4 55.12 1.08 1.6661 4 5 1 8 55.61 15.47 1.6527 5 3 1 8 55.61 1.17 1.6527 2 1 3 8 55.83 2.77 1.6468 0 3 3 4 56.50 15.03 1.6287 0 8 0 2 56.74 1.32 1.6225 1 3 3 8 57.56 6.38 1.6014 4 6 0 4 58.11 6.07 1.5874 2 6 2 8 58.39 4.80 1.5805 6 0 0 2 58.86 2.81 1.5690 6 1 0 4 58.95 16.56 1.5669 5 4 1 8 59.36 4.07 1.5570 4 4 2 8 59.62 2.03 1.5508 3 0 3 4 59.82 1.25 1.5461 5 0 2 4 60.03 32.90 1.5410 1 4 3 8 60.06 5.27 1.5404 2 8 0 4 61.46 8.36 1.5086 3 2 3 8 63.07 8.78 1.4739 5 5 1 8 63.28 1.90 1.4697 0 5 3 4 64.12 3.19 1.4523 1 5 3 8 65.20 1.06 1.4309 6 3 1 8 66.03 1.47 1.4149 4 1 3 8 66.81 1.30 1.4002 3 4 3 8 66.97 3.65 1.3974 3 8 1 8 67.35 8.08 1.3904 0 8 2 4 67.66 2.05 1.3847 2 9 0 4 67.79 3.79 1.3824 1 9 1 8 68.30 6.48 1.3732 4 6 2 8 69.06 9.58 1.3600 6 0 2 4 69.49 2.10 1.3527 6 1 2 8 70.56 3.22 1.3348 0 0 4 2 70.59 3.40 1.3342 2 8 2 8 72.32 3.13 1.3065 7 1 1 8 73.05 1.24 1.2953 1 2 4 8 73.74 2.07 1.2848 2 0 4 4 73.82 1.58 1.2837 4 7 2 8 74.20 1.16 1.2780 3 9 1 8 74.43 1.78 1.2747 1 7 3 8 75.30 1.53 1.2620 3 6 3 8 75.35 1.12 1.2614 1 9 2 8 75.41 1.34 1.2605 2 2 4 8 75.80 1.37 1.2550 6 4 2 8 76.63 2.00 1.2435 5 3 3 8 77.47 1.17 1.2320 2 3 4 8 78.54 7.65 1.2179 7 4 1 8 79.50 1.65 1.2056 5 4 3 8 80.00 2.02 1.1993 4 8 2 8 82.00 4.50 1.1751 3 10 1 8 83.15 3.33 1.1617 5 5 3 8 83.44 1.17 1.1585 4 1 4 8 83.98 1.95 1.1524 2 5 4 8 84.65 2.17 1.1450 4 2 4 8 84.78 1.93 1.1436 8 3 0 4 85.64 2.35 1.1343 6 8 0 4 86.69 2.26 1.1231 3 8 3 8 86.87 1.69 1.1213 4 9 2 8 87.77 1.00 1.1120 3 5 4 8 88.40 1.24 1.1058 2 6 4 8 89.47 1.45 1.0954 4 4 4 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.