data_global _amcsd_formula_title 'Dy4(SiS4)3' loop_ _publ_author_name 'Hatscher S T' 'Urland W' _journal_name_full 'Acta Crystallographica, Section E' _journal_volume 58 _journal_year 2002 _journal_page_first i74 _journal_page_last i75 _publ_section_title ; Dysprosium thiosilicate, Dy4(SiS4)3 ; _database_code_amcsd 0010383 _chemical_formula_sum 'Dy4 Si3 S12' _cell_length_a 9.813 _cell_length_b 10.9387 _cell_length_c 16.360 _cell_angle_alpha 90 _cell_angle_beta 102.86 _cell_angle_gamma 90 _cell_volume 1712.057 _exptl_crystal_density_diffrn 4.341 _symmetry_space_group_name_H-M 'P 1 21/n 1' loop_ _space_group_symop_operation_xyz 'x,y,z' '1/2+x,1/2-y,1/2+z' '1/2-x,1/2+y,1/2-z' '-x,-y,-z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv Dy1 0.61037 0.98387 0.12499 0.01090 Dy2 0.87638 0.65205 0.05968 0.01025 Dy3 0.53109 0.37677 0.13105 0.01181 Dy4 0.32137 0.76108 0.28899 0.01307 Si1 0.22185 0.55471 0.11744 0.01030 Si2 0.70047 0.88347 0.93948 0.01030 Si3 0.70889 0.71649 0.23333 0.00960 S1 0.50347 0.77960 0.18937 0.01300 S2 0.41939 0.15310 0.18410 0.01130 S3 0.74682 0.21352 0.13550 0.01150 S4 0.84701 0.83727 0.18728 0.00990 S5 0.61230 0.75951 0.01329 0.01100 S6 0.91010 0.84639 0.94613 0.01370 S7 0.04205 0.43674 0.09416 0.01230 S8 0.34970 0.48068 0.22872 0.01410 S9 0.66502 0.47329 0.97688 0.01300 S10 0.15065 0.73252 0.12650 0.01150 S11 0.65770 0.05886 0.97265 0.01210 S12 0.75600 0.54329 0.18751 0.01150 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Dy1 0.01038 0.00939 0.01267 0.00096 0.00202 0.00137 Dy2 0.00816 0.01019 0.01199 0.00129 0.00136 0.00045 Dy3 0.00955 0.01044 0.01395 0.00056 -0.00058 -0.00045 Dy4 0.01157 0.01701 0.01117 -0.00360 0.00366 -0.00137 Si1 0.01050 0.00950 0.01000 0.00160 0.00060 -0.00050 Si2 0.00970 0.01080 0.00980 0.00160 0.00080 -0.00070 Si3 0.00860 0.00990 0.01010 0.00030 0.00160 0.00150 S1 0.00810 0.01630 0.01500 0.00130 0.00340 0.00450 S2 0.00890 0.01390 0.01060 0.00060 0.00070 -0.00140 S3 0.01250 0.01190 0.01030 0.00020 0.00250 -0.00120 S4 0.00810 0.00950 0.01170 0.00040 0.00140 -0.00070 S5 0.01040 0.01070 0.01180 0.00050 0.00210 0.00120 S6 0.00960 0.01480 0.01610 0.00160 0.00130 0.00130 S7 0.01180 0.00960 0.01460 0.00090 0.00140 0.00220 S8 0.01240 0.01540 0.01290 0.00350 -0.00080 0.00270 S9 0.01240 0.01380 0.01310 0.00270 0.00350 -0.00080 S10 0.00930 0.00960 0.01410 0.00150 -0.00050 -0.00110 S11 0.01320 0.01000 0.01290 0.00030 0.00260 -0.00120 S12 0.01200 0.00890 0.01380 -0.00150 0.00300 -0.00130