PbCl4 Maley I J, Parsons S, Pulham C R Acta Crystallographica E58 (2002) i79-i81 Lead(IV) chloride at 150 K Note: sample at T = 150 K _database_code_amcsd 0010384 CELL PARAMETERS: 10.5420 5.3590 11.9580 90.000 115.830 90.000 SPACE GROUP: I2/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 608.067 Density (g/cm3): 3.812 MAX. ABS. INTENSITY / VOLUME**2: 67.64655274 RIR: 5.778 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 16.47 66.23 5.3816 0 0 2 2 18.70 51.67 4.7444 2 0 0 2 18.79 51.26 4.7232 -2 0 2 2 19.02 100.00 4.6662 1 1 0 4 22.38 72.89 3.9718 -1 1 2 4 27.86 38.84 3.2022 1 1 2 4 28.92 21.12 3.0869 2 1 1 4 29.04 15.92 3.0752 -2 1 3 4 30.05 17.15 2.9737 2 0 2 2 30.21 16.96 2.9581 -2 0 4 2 30.73 31.98 2.9097 -3 1 2 4 32.88 24.93 2.7239 3 1 0 4 33.30 1.25 2.6908 0 0 4 2 33.44 1.20 2.6795 0 2 0 2 34.02 1.20 2.6355 -4 0 2 2 34.73 22.65 2.5828 -1 1 4 4 37.12 18.80 2.4218 -3 1 4 4 37.50 18.88 2.3986 0 2 2 4 37.93 8.84 2.3722 4 0 0 2 38.11 9.44 2.3616 -4 0 4 2 38.59 16.82 2.3331 2 2 0 4 38.63 16.60 2.3306 -2 2 2 4 42.21 12.82 2.1409 1 1 4 4 42.45 11.94 2.1296 3 1 2 4 45.42 5.12 1.9968 2 0 4 2 45.57 9.44 1.9906 2 2 2 4 45.61 5.02 1.9889 -2 0 6 2 45.68 9.28 1.9859 -2 2 4 4 46.45 9.45 1.9548 -5 1 2 4 47.91 21.44 1.8987 0 2 4 4 48.15 7.92 1.8900 -5 1 4 4 48.19 10.60 1.8882 4 0 2 2 48.45 20.66 1.8789 -4 2 2 4 48.49 10.32 1.8775 -4 0 6 2 49.23 7.43 1.8507 -3 1 6 4 50.44 6.81 1.8093 -1 1 6 4 50.90 4.11 1.7939 0 0 6 2 51.06 7.01 1.7889 5 1 0 4 51.45 6.39 1.7761 4 2 0 4 51.59 5.87 1.7717 -4 2 4 4 52.10 6.70 1.7555 1 3 0 4 52.74 3.35 1.7356 -6 0 2 2 52.84 3.28 1.7325 -6 0 4 2 53.59 5.13 1.7101 -1 3 2 4 55.71 4.95 1.6501 -5 1 6 4 56.36 5.00 1.6324 3 1 4 4 56.43 5.17 1.6306 1 3 2 4 56.78 1.30 1.6214 2 1 5 4 56.97 1.78 1.6164 -2 1 7 4 57.10 2.36 1.6131 -2 3 3 4 57.57 4.34 1.6011 2 2 4 4 57.73 4.36 1.5970 -2 2 6 4 57.73 1.23 1.5970 -6 1 1 4 57.92 1.68 1.5921 -6 1 5 4 58.10 3.98 1.5877 -3 3 2 4 58.35 1.97 1.5815 6 0 0 2 58.64 1.91 1.5744 -6 0 6 2 58.99 4.25 1.5658 1 1 6 4 59.42 4.31 1.5554 3 3 0 4 60.61 3.48 1.5277 -1 3 4 4 60.91 3.61 1.5209 5 1 2 4 62.21 3.13 1.4923 -3 3 4 4 62.28 2.83 1.4907 0 2 6 4 62.46 1.47 1.4869 4 0 4 2 62.83 1.33 1.4791 -4 0 8 2 62.86 1.61 1.4783 2 0 6 2 63.08 1.58 1.4738 -2 0 8 2 63.91 2.82 1.4567 -6 2 2 4 64.00 2.87 1.4549 -6 2 4 4 64.43 2.97 1.4460 -7 1 4 4 64.75 2.93 1.4397 -3 1 8 4 65.63 2.92 1.4226 -7 1 2 4 65.82 2.56 1.4189 1 3 4 4 66.00 2.92 1.4155 3 3 2 4 67.82 2.63 1.3819 -5 1 8 4 68.29 2.44 1.3735 -1 1 8 4 68.39 2.42 1.3717 -7 1 6 4 68.78 1.11 1.3649 6 0 2 2 68.95 2.58 1.3619 6 2 0 4 69.03 2.19 1.3605 -5 3 2 4 69.21 2.60 1.3574 -6 2 6 4 69.21 1.11 1.3574 -6 0 8 2 69.92 2.69 1.3454 0 0 8 2 70.26 2.59 1.3398 0 4 0 2 70.36 2.42 1.3381 -5 3 4 4 71.22 2.27 1.3239 -3 3 6 4 71.61 2.48 1.3177 -8 0 4 2 71.84 2.12 1.3141 7 1 0 4 72.19 2.20 1.3085 -1 3 6 4 72.69 1.78 1.3007 5 3 0 4 72.74 2.26 1.3001 4 2 4 4 72.74 1.82 1.3001 0 4 2 4 73.08 2.36 1.2949 -4 2 8 4 73.11 2.00 1.2944 2 2 6 4 73.27 1.97 1.2920 3 1 6 4 73.31 2.00 1.2914 -2 2 8 4 73.44 1.79 1.2893 2 4 0 4 73.47 1.83 1.2889 -2 4 2 4 74.84 1.76 1.2687 5 1 4 4 76.56 1.73 1.2443 -5 3 6 4 77.11 1.67 1.2368 -7 1 8 4 77.13 1.47 1.2367 3 3 4 4 78.02 1.53 1.2248 1 1 8 4 78.27 1.53 1.2215 2 4 2 4 78.35 1.56 1.2204 -2 4 4 4 78.67 1.65 1.2162 6 2 2 4 79.09 1.58 1.2109 -6 2 8 4 79.39 1.36 1.2070 1 3 6 4 81.08 1.47 1.1860 5 3 2 4 82.61 1.28 1.1680 7 1 2 4 82.73 1.29 1.1666 4 4 0 4 82.84 1.37 1.1653 -4 4 4 4 84.52 1.28 1.1463 -3 3 8 4 87.73 1.11 1.1125 2 4 4 4 87.78 1.13 1.1120 -1 3 8 4 87.86 1.07 1.1112 -2 4 6 4 89.40 2.37 1.0960 4 2 6 4 89.75 2.30 1.0926 4 4 2 4 89.97 2.28 1.0906 -4 4 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.