CaB8O11(OH)4 Wiggin S B, Weller M T Acta Crystallographica E61 (2005) i243-i245 Redetermination of CaB8O11(OH)4 at low temperature Note: T = 120 K Locality: synthetic _database_code_amcsd 0010461 CELL PARAMETERS: 7.4810 8.2693 9.8590 90.000 108.760 90.000 SPACE GROUP: P2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 577.502 Density (g/cm3): 2.131 MAX. ABS. INTENSITY / VOLUME**2: 6.394964650 RIR: 0.977 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.47 7.05 9.3352 0 0 1 2 12.50 100.00 7.0836 1 0 0 2 14.31 4.70 6.1900 0 1 1 2 16.48 51.17 5.3797 1 1 0 2 16.89 7.24 5.2485 -1 1 1 2 19.01 1.02 4.6676 0 0 2 2 21.49 76.54 4.1347 0 2 0 1 21.87 2.86 4.0648 0 1 2 2 21.95 1.10 4.0489 -1 1 2 2 23.53 8.89 3.7804 0 2 1 2 23.83 6.09 3.7336 -2 0 1 2 24.94 19.53 3.5709 1 2 0 2 25.14 17.48 3.5418 2 0 0 2 25.22 15.93 3.5317 -1 2 1 2 26.19 3.21 3.4028 -2 1 1 2 27.35 1.23 3.2612 -1 0 3 2 27.39 18.12 3.2557 2 1 0 2 28.17 4.20 3.1682 1 2 1 2 28.85 4.56 3.0950 0 2 2 2 28.91 7.60 3.0880 -1 2 2 2 29.44 2.82 3.0338 -1 1 3 2 29.72 4.21 3.0063 2 0 1 2 30.70 11.89 2.9124 0 1 3 2 31.59 4.59 2.8326 -2 0 3 2 31.67 1.84 2.8254 2 1 1 2 32.31 1.08 2.7710 -2 2 1 2 33.31 1.35 2.6898 2 2 0 2 33.44 5.78 2.6798 -2 1 3 2 33.91 16.59 2.6436 0 3 1 2 33.99 1.66 2.6373 1 2 2 2 34.17 1.12 2.6243 -2 2 2 2 34.93 2.99 2.5688 1 3 0 2 35.03 3.99 2.5617 1 0 3 2 35.04 1.41 2.5606 -1 2 3 2 35.14 1.70 2.5541 -1 3 1 2 36.11 4.49 2.4871 -3 0 1 2 36.44 2.88 2.4654 2 0 2 2 36.72 2.03 2.4478 -3 0 2 2 37.77 1.27 2.3817 -3 1 1 2 37.91 1.12 2.3735 0 3 2 2 38.09 1.76 2.3626 2 1 2 2 38.11 10.56 2.3612 3 0 0 2 38.35 2.30 2.3471 -3 1 2 2 38.53 4.80 2.3368 -2 2 3 2 38.58 1.17 2.3338 0 0 4 2 38.78 1.26 2.3218 -2 0 4 2 39.70 10.13 2.2704 3 1 0 2 40.15 2.94 2.2461 0 1 4 2 40.35 3.66 2.2354 -2 1 4 2 41.35 2.56 2.1836 -3 1 3 2 41.47 5.78 2.1776 1 2 3 2 41.51 11.41 2.1753 2 3 0 2 42.40 3.55 2.1319 3 0 1 2 42.41 1.79 2.1313 -3 2 1 2 42.71 17.95 2.1171 -1 2 4 2 43.79 10.55 2.0673 0 4 0 1 43.86 4.46 2.0644 3 1 1 2 43.88 1.37 2.0633 0 3 3 2 44.58 12.72 2.0324 0 2 4 2 44.77 13.70 2.0245 -2 2 4 2 44.91 2.75 2.0184 0 4 1 2 45.69 1.23 1.9858 -3 2 3 2 45.72 4.74 1.9845 1 4 0 2 45.88 2.11 1.9777 -1 4 1 2 45.94 1.04 1.9755 -2 3 3 2 46.02 8.08 1.9723 1 1 4 2 46.38 6.10 1.9579 -3 1 4 2 48.51 1.94 1.8765 1 3 3 2 49.61 1.19 1.8376 2 3 2 2 49.94 1.03 1.8262 2 2 3 2 50.04 1.36 1.8229 1 2 4 2 50.37 1.48 1.8115 -3 2 4 2 50.49 2.38 1.8076 -4 1 1 2 50.92 7.18 1.7932 3 3 0 2 51.16 3.84 1.7854 2 4 0 2 51.71 1.05 1.7676 -4 1 3 2 52.29 1.11 1.7495 -3 3 3 2 52.87 2.34 1.7316 4 1 0 2 54.75 1.77 1.6766 2 1 4 2 55.23 2.09 1.6633 -4 1 4 2 56.26 2.20 1.6351 1 3 4 2 56.51 2.43 1.6285 0 5 1 2 56.53 1.07 1.6279 4 2 0 2 56.57 2.41 1.6268 -3 3 4 2 56.65 2.19 1.6247 -3 2 5 2 58.01 1.16 1.5898 -3 4 1 2 58.79 1.26 1.5707 -4 2 4 2 60.19 1.24 1.5375 -4 3 1 2 60.56 1.01 1.5290 4 2 1 2 61.30 1.46 1.5121 -2 5 1 2 62.59 1.01 1.4841 3 4 1 2 73.90 1.04 1.2824 1 5 4 2 74.17 1.00 1.2784 -3 5 4 2 77.45 3.30 1.2323 -2 0 8 2 77.57 1.57 1.2307 -6 1 3 2 79.71 1.56 1.2029 -1 6 4 2 81.03 2.09 1.1867 0 6 4 2 81.16 2.04 1.1851 -2 6 4 2 81.50 1.22 1.1810 -2 2 8 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.