Borax Gainsford G J, Kemmitt T, Higham C Acta Crystallographica E64 (2008) i24-i25 Redetermination of the borax structure from laboratory X-ray data at 145 K Note T = 145 K Locality: synthetic _database_code_amcsd 0019359 CELL PARAMETERS: 11.8843 10.6026 12.2111 90.000 106.790 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1473.060 Density (g/cm3): 1.719 MAX. ABS. INTENSITY / VOLUME**2: 3.040832017 RIR: 0.576 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.41 5.85 7.7567 1 1 0 4 12.39 20.12 7.1440 -1 1 1 4 14.90 14.41 5.9464 1 1 1 4 15.16 4.19 5.8453 0 0 2 2 15.58 41.60 5.6888 2 0 0 2 16.72 3.85 5.3013 0 2 0 2 17.10 17.40 5.1847 -1 1 2 4 18.38 82.32 4.8281 0 2 1 4 22.64 25.02 3.9268 0 2 2 4 22.69 16.13 3.9189 -2 2 1 4 22.93 1.07 3.8784 2 2 0 4 24.79 4.52 3.5911 2 0 2 2 24.93 4.81 3.5710 3 1 0 4 25.45 1.46 3.5001 -3 1 2 4 25.58 2.70 3.4819 2 2 1 4 26.41 2.11 3.3751 1 3 0 4 26.86 4.51 3.3194 -1 3 1 4 28.04 5.15 3.1820 3 1 1 4 28.14 1.79 3.1711 1 3 1 4 29.11 8.75 3.0675 -2 2 3 4 30.06 15.84 2.9732 2 2 2 4 30.07 28.48 2.9719 -2 0 4 2 30.49 1.71 2.9321 -1 1 4 4 30.59 7.21 2.9226 0 0 4 2 31.45 26.08 2.8444 4 0 0 2 31.73 59.70 2.8201 1 3 2 4 32.75 1.28 2.7344 3 1 2 4 33.82 5.19 2.6507 0 4 0 2 33.94 3.20 2.6410 -3 1 4 4 34.00 2.07 2.6364 -3 3 1 4 34.69 1.57 2.5856 3 3 0 4 34.70 3.01 2.5850 0 4 1 4 34.87 35.70 2.5729 1 1 4 4 35.08 100.00 2.5583 -3 3 2 4 35.18 17.42 2.5507 -4 2 2 4 35.74 1.52 2.5126 2 2 3 4 36.69 12.80 2.4495 1 3 3 4 37.78 7.66 2.3813 -3 3 3 4 38.48 20.34 2.3394 2 0 4 2 38.55 2.01 2.3353 3 1 3 4 38.61 1.43 2.3321 4 2 1 4 38.74 15.11 2.3242 -2 4 2 4 39.01 1.17 2.3087 -5 1 1 4 39.04 2.80 2.3072 -5 1 2 4 40.85 6.98 2.2091 3 3 2 4 41.04 4.60 2.1992 -4 2 4 4 41.19 4.06 2.1917 0 4 3 4 41.69 1.24 2.1666 -2 4 3 4 41.84 4.42 2.1590 -3 3 4 4 42.22 9.33 2.1403 2 2 4 4 42.38 2.36 2.1326 2 4 2 4 43.41 1.05 2.0846 1 5 0 4 43.62 7.02 2.0752 -5 1 4 4 43.70 4.10 2.0713 -1 5 1 4 44.55 6.28 2.0337 1 5 1 4 44.59 3.52 2.0320 -2 0 6 2 45.12 8.78 2.0096 3 1 4 4 45.25 1.16 2.0040 -1 3 5 4 45.78 1.51 1.9821 3 3 3 4 45.90 1.43 1.9769 -4 4 1 4 46.18 2.47 1.9658 -5 3 1 4 46.20 2.14 1.9649 -5 3 2 4 46.34 1.01 1.9595 -4 4 2 4 46.61 3.59 1.9484 0 0 6 2 46.64 2.14 1.9475 -3 1 6 4 46.78 4.94 1.9420 2 4 3 4 46.98 1.40 1.9340 -3 3 5 4 47.05 2.08 1.9314 1 5 2 4 47.59 7.33 1.9108 -5 3 3 4 47.82 2.35 1.9022 -5 1 5 4 47.95 3.30 1.8974 -2 2 6 4 47.98 5.87 1.8963 6 0 0 2 48.12 4.56 1.8910 -4 4 3 4 48.40 1.88 1.8806 -4 0 6 2 49.13 5.61 1.8543 -6 2 2 4 49.14 8.29 1.8540 -6 0 4 2 49.28 3.25 1.8492 1 3 5 4 49.52 1.54 1.8408 -3 5 2 4 49.86 1.30 1.8288 0 2 6 4 51.14 2.92 1.7860 -4 4 4 4 51.57 2.11 1.7723 -4 2 6 4 51.60 2.83 1.7712 3 3 4 4 51.73 1.75 1.7671 0 6 0 2 52.15 1.07 1.7540 2 4 4 4 52.15 10.20 1.7538 -1 3 6 4 52.16 2.48 1.7534 0 4 5 4 52.57 4.56 1.7409 4 4 2 4 52.98 5.25 1.7282 -3 3 6 4 53.92 12.12 1.7003 5 3 2 4 54.02 2.87 1.6975 6 2 1 4 54.04 2.47 1.6970 3 5 2 4 54.23 3.15 1.6915 0 6 2 4 55.45 2.25 1.6570 -2 2 7 4 56.98 1.87 1.6161 -7 1 4 4 57.12 1.99 1.6127 -2 4 6 4 58.33 1.15 1.5820 2 4 5 4 58.45 1.57 1.5789 -5 5 1 4 58.82 3.11 1.5699 0 4 6 4 59.95 1.31 1.5430 3 1 6 4 59.98 1.05 1.5423 6 4 0 4 60.50 1.51 1.5303 -7 3 2 4 60.99 1.16 1.5192 -6 4 4 4 61.30 4.46 1.5122 0 6 4 4 61.75 1.06 1.5024 2 6 3 4 61.79 6.68 1.5014 1 7 0 4 61.86 1.10 1.4998 5 5 1 4 62.50 3.50 1.4859 -4 0 8 2 65.41 1.29 1.4267 4 0 6 2 65.65 2.87 1.4222 8 0 0 2 66.20 1.74 1.4117 6 4 2 4 66.29 3.99 1.4100 2 6 4 4 70.34 1.38 1.3384 -1 5 7 4 70.41 1.96 1.3372 -3 5 7 4 71.09 1.16 1.3261 2 0 8 2 74.12 2.72 1.2791 -6 6 4 4 75.78 1.10 1.2553 9 1 0 4 76.06 1.79 1.2513 7 5 1 4 77.80 1.33 1.2277 -9 1 6 4 78.57 1.07 1.2175 3 7 4 4 82.46 1.28 1.1697 4 0 8 2 82.63 1.17 1.1677 6 2 6 4 82.72 1.44 1.1667 -9 3 6 4 84.95 1.50 1.1416 0 2 10 4 88.17 1.53 1.1081 7 7 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.