Cl4 K2 O2 Os Hoard J, Grenko J Zeitschrift fur Kristallographie 87 (1934) 100-109 The crystal structure of potassium osmyl chloride K2 Os O2 Cl4 _cod_database_code 1010629 _database_code_amcsd 0017511 CELL PARAMETERS: 6.9900 6.9900 8.7500 90.000 90.000 90.000 SPACE GROUP: I4/mmm X-RAY WAVELENGTH: 1.541838 Cell Volume: 427.526 Density (g/cm3): 3.435 MAX. ABS. INTENSITY / VOLUME**2: 116.6853048 RIR: 11.061 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 16.23 100.00 5.4613 1 0 1 8 17.95 16.75 4.9427 1 1 0 4 20.30 16.09 4.3750 0 0 2 2 25.49 9.31 3.4950 2 0 0 4 27.22 35.67 3.2760 1 1 2 8 30.36 28.89 2.9438 2 1 1 16 32.80 1.59 2.7307 2 0 2 8 33.29 11.91 2.6917 1 0 3 8 36.35 26.06 2.4713 2 2 0 4 40.05 4.29 2.2515 3 0 1 8 40.82 3.58 2.2104 3 1 0 8 41.27 8.44 2.1875 0 0 4 2 41.99 8.03 2.1518 2 2 2 8 42.38 7.86 2.1326 2 1 3 16 45.34 2.44 2.0003 1 1 4 8 46.00 14.26 1.9729 3 1 2 16 48.07 13.78 1.8928 3 2 1 16 49.13 2.43 1.8543 2 0 4 8 50.11 1.45 1.8204 3 0 3 8 52.36 7.26 1.7475 4 0 0 4 54.02 4.22 1.6976 1 0 5 8 55.19 6.42 1.6644 4 1 1 16 56.15 11.05 1.6380 2 2 4 8 56.72 2.86 1.6228 4 0 2 8 57.04 6.15 1.6145 3 2 3 16 59.11 1.77 1.5630 4 2 0 8 59.45 1.82 1.5548 3 1 4 16 60.00 3.50 1.5419 3 3 2 8 60.64 4.11 1.5270 2 1 5 16 63.47 3.08 1.4657 4 1 3 16 66.86 1.00 1.3993 3 0 5 8 66.89 2.44 1.3987 1 1 6 8 67.90 1.63 1.3805 4 3 1 16 67.90 2.60 1.3805 5 0 1 8 68.75 5.04 1.3653 4 0 4 8 72.22 3.38 1.3081 5 1 2 16 72.81 3.68 1.2990 3 2 5 16 74.63 1.27 1.2717 4 2 4 16 75.40 1.53 1.2607 5 0 3 8 75.73 1.40 1.2560 2 2 6 8 77.20 1.64 1.2357 4 4 0 4 78.56 2.16 1.2176 4 1 5 16 78.59 2.58 1.2173 3 1 6 16 83.64 1.47 1.1562 5 3 2 16 85.16 1.09 1.1394 6 1 1 16 88.46 2.07 1.1052 6 2 0 8 89.79 1.19 1.0923 5 0 5 8 89.82 1.04 1.0920 3 3 6 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.