(V.75Ni.25)SO4*6H2O Kutoglu A Zeitschrift fur Kristallographie 137 (1973) 51-66 Kristallstruktur und wasserstoffbindungen von (V1-x,Nix)SO4*6H2O Note: isotypic with hexahydrite _database_code_amcsd 0010742 CELL PARAMETERS: 9.8900 7.2410 24.1570 90.000 98.350 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1711.629 Density (g/cm3): 1.995 MAX. ABS. INTENSITY / VOLUME**2: 8.556578951 RIR: 1.397 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.83 2.74 5.9752 0 0 4 2 15.22 17.84 5.8206 1 1 0 4 15.35 1.49 5.7711 -1 1 1 4 15.98 3.31 5.5463 1 1 1 4 16.35 23.37 5.4205 -1 1 2 4 17.51 20.76 5.0636 1 1 2 4 18.08 2.16 4.9061 -1 1 3 4 18.13 20.65 4.8926 2 0 0 2 18.57 15.64 4.7776 -2 0 2 2 19.65 4.34 4.5177 1 1 3 4 20.36 100.00 4.3620 -1 1 4 4 20.59 12.40 4.3135 2 0 2 2 21.74 15.57 4.0876 -2 0 4 2 22.22 53.66 4.0002 1 1 4 4 23.03 4.81 3.8613 -1 1 5 4 24.59 12.91 3.6205 0 2 0 2 24.87 2.64 3.5797 0 2 1 4 25.14 14.41 3.5418 2 0 4 2 25.99 7.65 3.4283 -1 1 6 4 26.73 7.40 3.3353 -2 0 6 2 28.22 7.02 3.1625 1 1 6 4 29.16 1.76 3.0628 -1 1 7 4 29.78 1.96 3.0002 -3 1 1 4 29.91 4.49 2.9876 0 0 8 2 29.99 5.48 2.9799 -3 1 2 4 30.05 4.14 2.9739 3 1 0 4 30.62 7.42 2.9194 -2 2 1 4 30.67 6.42 2.9155 -3 1 3 4 30.72 7.05 2.9103 2 2 0 4 30.94 15.32 2.8904 2 0 6 2 30.99 15.80 2.8856 -2 2 2 4 31.28 1.49 2.8595 2 2 1 4 31.79 4.00 2.8152 -3 1 4 4 31.81 2.35 2.8131 -2 2 3 4 32.28 7.66 2.7731 2 2 2 4 32.78 3.86 2.7324 -2 0 8 2 33.05 1.56 2.7103 -2 2 4 4 33.31 2.41 2.6899 -3 1 5 4 33.45 4.71 2.6792 0 2 6 4 33.69 4.00 2.6606 2 2 3 4 34.92 6.29 2.5693 1 1 8 4 35.19 1.26 2.5504 -3 1 6 4 35.46 1.16 2.5318 2 2 4 4 35.94 4.02 2.4990 -1 1 9 4 36.40 3.95 2.4680 -4 0 2 2 36.63 1.80 2.4531 -2 2 6 4 37.66 1.99 2.3888 -4 0 4 2 39.09 4.52 2.3043 0 2 8 4 39.50 2.38 2.2813 -1 1 10 4 39.71 3.97 2.2697 -1 3 3 4 39.84 8.98 2.2628 -3 1 8 4 39.91 1.57 2.2588 2 2 6 4 40.17 2.63 2.2448 3 1 6 4 40.87 5.18 2.2079 -1 3 4 4 41.40 3.04 2.1810 -2 2 8 4 41.90 2.11 2.1563 1 3 4 4 42.36 1.25 2.1337 -1 3 5 4 43.17 1.04 2.0958 -1 1 11 4 44.14 1.36 2.0519 -2 2 9 4 44.32 1.52 2.0438 -4 0 8 2 44.42 1.33 2.0393 -4 2 2 4 44.71 1.61 2.0270 4 2 0 4 45.34 1.71 2.0001 2 2 8 4 45.49 4.44 1.9939 -4 2 4 4 45.59 2.84 1.9898 1 3 6 4 45.81 9.33 1.9807 3 1 8 4 46.51 3.43 1.9525 -4 2 5 4 47.33 1.61 1.9205 3 3 1 4 47.67 1.43 1.9078 -5 1 2 4 48.04 1.93 1.8940 -3 3 4 4 48.17 2.71 1.8892 5 1 0 4 48.45 1.40 1.8786 -5 1 4 4 48.53 2.32 1.8758 -1 3 8 4 49.13 4.51 1.8545 -3 3 5 4 49.17 7.78 1.8529 4 2 4 4 49.64 5.09 1.8365 1 1 12 4 50.18 1.13 1.8180 -2 2 11 4 50.31 1.88 1.8135 1 3 8 4 50.41 1.55 1.8103 0 4 0 2 50.57 2.32 1.8051 0 4 1 4 52.03 3.85 1.7578 2 0 12 2 52.17 2.21 1.7532 -3 3 7 4 52.43 2.95 1.7451 0 2 12 4 52.83 1.08 1.7329 5 1 4 4 53.45 2.32 1.7141 -2 2 12 4 53.64 3.12 1.7086 -5 1 8 4 53.95 1.13 1.6996 -2 4 1 4 54.09 2.54 1.6955 -3 3 8 4 54.71 1.37 1.6778 -2 4 3 4 55.07 3.04 1.6677 -4 0 12 2 58.96 1.19 1.5666 3 3 8 4 60.95 1.75 1.5201 5 3 0 4 61.19 1.40 1.5147 -4 2 12 4 62.14 1.07 1.4938 0 0 16 2 62.46 1.06 1.4870 6 2 0 4 63.16 1.17 1.4721 6 2 1 4 66.18 1.49 1.4120 -3 1 16 4 66.57 1.77 1.4048 1 5 3 4 66.82 1.15 1.4002 6 2 4 4 67.87 1.59 1.3809 0 2 16 4 70.61 1.54 1.3339 5 3 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.