Imhofite Divjakovic V, Nowacki W Zeitschrift fur Kristallographie 144 (1976) 323-333 Die kristallstruktur von imhofit, Tl5.6As15S25.3 Locality: synthetic _database_code_amcsd 0010785 CELL PARAMETERS: 8.7550 24.4250 5.7390 90.000 108.280 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 1165.300 Density (g/cm3): 4.389 MAX. ABS. INTENSITY / VOLUME**2: 14.24949322 RIR: 1.057 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.24 18.97 12.2125 0 2 0 2 11.24 1.32 7.8698 1 1 0 4 14.51 6.80 6.1062 0 4 0 2 15.23 20.43 5.8167 1 3 0 4 16.42 6.96 5.3997 -1 0 1 2 16.67 54.36 5.3186 0 1 1 4 16.82 11.48 5.2724 -1 1 1 4 17.82 6.91 4.9764 0 2 1 4 18.02 40.06 4.9213 1 4 0 4 19.60 42.90 4.5286 0 3 1 4 21.09 4.30 4.2117 1 5 0 4 21.69 2.23 4.0977 2 1 0 4 21.83 30.21 4.0708 0 6 0 2 21.86 4.05 4.0658 0 4 1 4 21.97 16.80 4.0450 -1 4 1 4 22.13 56.85 4.0163 1 0 1 2 22.43 6.25 3.9631 1 1 1 4 22.60 100.00 3.9349 2 2 0 4 22.76 31.96 3.9063 -2 1 1 4 23.31 23.06 3.8153 1 2 1 4 23.63 8.78 3.7645 -2 2 1 4 24.35 28.36 3.6560 1 6 0 4 24.47 10.71 3.6374 0 5 1 4 24.57 71.68 3.6226 -1 5 1 4 24.72 6.18 3.6019 1 3 1 4 25.02 89.78 3.5591 -2 3 1 4 25.93 47.77 3.4361 2 4 0 4 26.56 49.99 3.3556 1 4 1 4 26.85 17.56 3.3208 -2 4 1 4 27.35 10.18 3.2613 0 6 1 4 27.44 70.09 3.2506 -1 6 1 4 27.73 41.11 3.2174 1 7 0 4 28.19 83.51 3.1657 2 5 0 4 28.78 5.16 3.1024 1 5 1 4 29.04 1.66 3.0749 -2 5 1 4 30.42 5.63 2.9385 0 7 1 4 30.74 11.23 2.9084 2 6 0 4 31.10 2.88 2.8757 2 1 1 4 31.21 17.64 2.8660 1 8 0 4 31.29 50.49 2.8591 1 6 1 4 31.39 60.85 2.8496 -1 1 2 4 31.51 38.20 2.8394 -3 1 1 4 31.53 5.87 2.8375 -2 6 1 4 31.76 9.47 2.8177 2 2 1 4 32.04 1.00 2.7931 -1 2 2 4 32.52 8.15 2.7534 3 1 0 4 32.83 9.39 2.7284 2 3 1 4 32.87 6.48 2.7247 0 0 2 2 33.08 5.61 2.7079 0 1 2 4 33.10 43.76 2.7061 -1 3 2 4 33.15 18.23 2.7024 3 2 0 4 33.18 2.13 2.6999 -2 0 2 2 33.21 4.95 2.6973 -3 3 1 4 33.39 53.97 2.6835 -2 1 2 4 33.53 99.22 2.6725 2 7 0 4 33.65 1.78 2.6636 0 8 1 4 33.72 1.41 2.6577 -1 8 1 4 34.01 2.45 2.6362 -2 2 2 4 34.04 53.21 2.6341 1 7 1 4 34.18 8.16 2.6233 3 3 0 4 34.26 6.37 2.6172 -2 7 1 4 34.27 7.11 2.6165 2 4 1 4 34.65 4.53 2.5891 -3 4 1 4 34.77 12.28 2.5799 1 9 0 4 35.02 1.07 2.5626 -2 3 2 4 35.58 7.05 2.5234 3 4 0 4 36.10 7.24 2.4882 0 4 2 4 36.41 23.68 2.4673 -3 5 1 4 36.80 23.88 2.4425 0 10 0 2 37.00 14.00 2.4293 0 9 1 4 37.81 9.42 2.3796 0 5 2 4 38.02 4.30 2.3666 1 1 2 4 38.08 3.30 2.3630 -2 5 2 4 38.38 1.53 2.3452 -1 6 2 4 38.41 7.45 2.3434 1 10 0 4 38.48 4.45 2.3395 -3 6 1 4 39.11 3.04 2.3030 -3 2 2 4 39.33 1.49 2.2907 3 6 0 4 39.48 9.33 2.2825 1 3 2 4 39.66 3.44 2.2724 2 9 0 4 39.81 30.77 2.2643 0 6 2 4 40.01 5.20 2.2534 -3 3 2 4 40.07 4.06 2.2500 -2 6 2 4 40.30 1.47 2.2381 -2 9 1 4 40.47 2.93 2.2289 0 10 1 4 40.48 7.99 2.2284 2 7 1 4 40.54 12.42 2.2254 -1 10 1 4 40.71 2.60 2.2162 -1 7 2 4 40.72 6.71 2.2158 1 4 2 4 40.81 7.46 2.2114 -3 7 1 4 40.90 34.03 2.2062 3 0 1 2 41.08 9.09 2.1973 3 1 1 4 41.24 14.03 2.1892 -3 4 2 4 41.53 1.97 2.1745 -4 1 1 4 41.60 8.46 2.1711 3 2 1 4 42.04 3.74 2.1491 -4 2 1 4 42.08 2.11 2.1475 0 7 2 4 42.27 1.15 2.1380 1 5 2 4 42.33 2.38 2.1353 -2 7 2 4 42.77 1.85 2.1141 -3 5 2 4 42.89 1.33 2.1087 -4 3 1 4 42.95 2.77 2.1058 2 10 0 4 43.05 6.03 2.1011 2 8 1 4 43.27 5.84 2.0908 -1 8 2 4 43.36 9.49 2.0869 1 10 1 4 43.36 1.30 2.0868 -3 8 1 4 43.62 1.43 2.0749 3 4 1 4 43.71 6.94 2.0708 4 1 0 4 44.05 5.56 2.0558 -4 4 1 4 44.10 7.71 2.0536 -1 11 1 4 44.21 1.96 2.0488 4 2 0 4 44.51 10.50 2.0354 0 12 0 2 44.57 1.91 2.0329 0 8 2 4 44.59 1.75 2.0320 -3 6 2 4 45.09 3.17 2.0107 3 5 1 4 45.15 1.76 2.0082 2 0 2 2 45.79 1.59 1.9816 2 2 2 4 45.82 4.12 1.9802 2 9 1 4 45.90 3.86 1.9770 1 12 0 4 46.02 6.48 1.9721 -4 1 2 4 46.03 6.88 1.9716 -1 9 2 4 46.20 3.53 1.9649 1 7 2 4 46.36 2.58 1.9585 2 11 0 4 46.50 2.53 1.9531 -4 2 2 4 46.67 2.85 1.9463 -3 7 2 4 46.86 3.20 1.9389 3 9 0 4 47.50 2.35 1.9140 -2 9 2 4 47.55 26.70 1.9124 4 5 0 4 47.67 8.63 1.9077 2 4 2 4 47.78 6.73 1.9035 -1 0 3 2 47.94 3.89 1.8977 -1 1 3 4 48.53 7.35 1.8760 1 8 2 4 48.57 5.65 1.8746 -2 2 3 4 48.78 2.86 1.8671 2 10 1 4 48.84 4.03 1.8647 3 7 1 4 48.98 18.82 1.8598 -3 8 2 4 49.16 1.04 1.8535 -1 3 3 4 49.23 7.19 1.8510 4 6 0 4 49.76 2.78 1.8323 3 10 0 4 49.89 13.21 1.8280 2 12 0 4 50.16 2.35 1.8187 0 10 2 4 50.20 2.80 1.8172 -1 4 3 4 50.25 10.07 1.8156 1 12 1 4 50.37 13.11 1.8116 -2 4 3 4 50.69 6.70 1.8010 2 6 2 4 50.72 1.85 1.7999 -3 0 3 2 51.16 1.28 1.7856 4 7 0 4 51.31 3.84 1.7807 -3 2 3 4 51.34 5.78 1.7795 -4 6 2 4 51.45 1.92 1.7762 0 13 1 4 51.46 15.55 1.7759 -4 8 1 4 51.50 3.40 1.7744 -3 9 2 4 51.55 13.48 1.7729 0 3 3 4 51.69 1.37 1.7684 -2 5 3 4 52.16 8.41 1.7536 -3 11 1 4 52.24 2.05 1.7509 -5 0 1 2 52.34 1.49 1.7480 4 2 1 4 52.39 6.42 1.7464 -5 1 1 4 52.45 7.38 1.7446 0 14 0 2 52.58 2.23 1.7405 2 7 2 4 52.82 1.87 1.7332 -5 2 1 4 53.04 1.25 1.7265 -3 4 3 4 53.22 2.13 1.7213 0 11 2 4 53.22 3.18 1.7211 -4 7 2 4 53.27 5.50 1.7195 -2 6 3 4 53.43 5.70 1.7150 -2 11 2 4 53.53 2.63 1.7119 3 9 1 4 53.68 1.86 1.7074 1 14 0 4 54.03 9.41 1.6973 -2 13 1 4 54.22 2.83 1.6916 -3 10 2 4 54.32 7.17 1.6889 -3 5 3 4 54.66 1.04 1.6790 3 2 2 4 55.07 1.46 1.6675 -5 1 2 4 55.10 4.68 1.6667 -2 7 3 4 55.17 3.94 1.6649 1 1 3 4 55.36 2.83 1.6595 3 3 2 4 55.39 1.95 1.6588 0 6 3 4 55.39 1.23 1.6588 5 1 0 4 55.49 10.63 1.6559 -5 2 2 4 55.80 1.32 1.6474 5 2 0 4 56.18 4.55 1.6372 3 10 1 4 56.35 13.71 1.6327 -4 2 3 4 56.49 3.27 1.6290 5 3 0 4 56.54 1.04 1.6277 -4 10 1 4 56.63 1.48 1.6253 -2 12 2 4 57.03 1.14 1.6148 -4 3 3 4 57.05 1.34 1.6143 2 9 2 4 57.14 5.00 1.6121 -5 4 2 4 57.17 4.70 1.6112 0 7 3 4 57.23 1.51 1.6098 1 4 3 4 57.27 4.32 1.6087 2 14 0 4 57.44 6.86 1.6042 5 4 0 4 57.55 1.00 1.6014 3 5 2 4 57.98 1.15 1.5906 -4 4 3 4 58.29 1.74 1.5828 4 10 0 4 58.74 5.25 1.5718 -1 13 2 4 59.02 4.69 1.5650 3 11 1 4 59.19 15.05 1.5611 0 8 3 4 59.27 1.89 1.5590 -1 15 1 4 59.45 4.15 1.5548 -2 9 3 4 59.60 1.34 1.5512 2 10 2 4 59.81 1.01 1.5463 1 12 2 4 59.90 1.73 1.5441 1 6 3 4 59.99 4.14 1.5422 -2 13 2 4 60.20 1.92 1.5372 -3 12 2 4 60.66 8.75 1.5266 0 16 0 2 61.07 6.32 1.5173 4 11 0 4 61.42 4.50 1.5095 0 9 3 4 61.59 5.73 1.5058 -2 15 1 4 61.79 1.85 1.5014 -1 10 3 4 61.93 4.00 1.4982 -2 10 3 4 61.95 8.02 1.4979 2 1 3 4 62.04 5.54 1.4960 3 12 1 4 62.34 2.05 1.4895 2 2 3 4 62.69 2.46 1.4820 3 8 2 4 62.92 2.23 1.4772 -4 11 2 4 62.95 2.79 1.4764 3 14 0 4 62.98 3.46 1.4758 2 3 3 4 63.06 4.72 1.4742 1 13 2 4 63.31 1.24 1.4690 -1 16 1 4 63.45 5.84 1.4661 -5 8 2 4 64.03 1.45 1.4542 4 12 0 4 64.24 3.37 1.4499 -4 8 3 4 64.34 3.43 1.4479 4 0 2 2 64.43 1.36 1.4461 -6 2 1 4 64.47 2.97 1.4454 4 1 2 4 65.01 2.01 1.4346 -2 0 4 2 65.27 2.49 1.4295 2 12 2 4 65.28 1.45 1.4294 -6 0 2 2 65.40 5.70 1.4270 1 16 1 4 65.51 1.17 1.4248 -2 2 4 4 65.60 1.38 1.4231 -5 10 1 4 65.96 6.98 1.4162 -1 15 2 4 65.99 1.78 1.4156 -5 5 3 4 66.03 1.11 1.4149 -3 15 1 4 66.03 1.04 1.4148 -1 1 4 4 66.35 1.73 1.4088 4 4 2 4 66.41 3.58 1.4078 -1 2 4 4 66.55 7.36 1.4050 5 5 1 4 66.78 2.50 1.4009 -3 2 4 4 67.49 1.32 1.3878 -2 12 3 4 67.62 1.98 1.3855 6 0 0 2 67.74 1.76 1.3833 6 1 0 4 67.96 1.26 1.3794 -5 10 2 4 68.12 2.39 1.3765 -2 5 4 4 68.21 1.14 1.3749 -5 11 1 4 68.24 1.02 1.3744 5 10 0 4 68.26 3.23 1.3740 -3 4 4 4 68.72 1.03 1.3659 6 3 0 4 68.82 1.04 1.3642 4 6 2 4 68.96 2.87 1.3618 -5 7 3 4 69.18 1.40 1.3579 2 17 0 4 69.41 1.37 1.3539 0 2 4 4 69.51 3.89 1.3523 5 7 1 4 69.73 1.67 1.3487 -6 6 2 4 69.75 2.34 1.3483 -3 12 3 4 70.03 2.36 1.3435 1 15 2 4 70.60 1.42 1.3340 1 11 3 4 71.82 2.05 1.3144 -6 8 1 4 71.89 1.23 1.3133 2 9 3 4 72.36 1.81 1.3059 0 13 3 4 72.40 1.24 1.3053 -4 15 1 4 73.40 1.42 1.2899 2 18 0 4 73.69 1.48 1.2856 1 18 1 4 73.70 2.15 1.2855 -1 8 4 4 73.79 1.29 1.2842 -2 14 3 4 73.81 3.03 1.2838 -3 17 1 4 74.63 2.32 1.2718 3 6 3 4 74.72 1.19 1.2704 1 19 0 4 75.52 1.05 1.2590 -4 7 4 4 75.77 1.32 1.2553 3 16 1 4 75.84 1.20 1.2544 1 4 4 4 76.06 1.01 1.2513 -5 3 4 4 77.34 1.83 1.2338 -6 7 3 4 77.90 2.43 1.2263 -7 3 2 4 79.40 1.77 1.2069 -5 14 2 4 79.69 1.31 1.2032 1 7 4 4 80.12 4.76 1.1978 -4 14 3 4 80.62 1.15 1.1917 0 20 1 4 80.75 1.62 1.1900 -7 6 1 4 81.06 1.22 1.1864 -6 9 3 4 81.43 1.23 1.1818 4 17 0 4 81.80 1.04 1.1775 -7 0 3 2 82.16 1.17 1.1732 -1 19 2 4 82.23 1.40 1.1724 4 4 3 4 82.33 1.08 1.1712 -6 1 4 4 83.39 1.21 1.1590 1 9 4 4 84.87 1.36 1.1425 -3 1 5 4 85.09 1.09 1.1401 -6 5 4 4 85.38 1.41 1.1370 -1 21 1 4 87.23 1.01 1.1175 3 20 0 4 87.36 1.13 1.1163 5 10 2 4 87.73 1.16 1.1125 4 8 3 4 88.30 2.49 1.1068 7 8 0 4 88.63 2.82 1.1035 2 15 3 4 88.87 1.42 1.1011 -3 6 5 4 88.99 1.87 1.1000 -1 14 4 4 89.33 1.42 1.0967 -3 14 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.