PbGe3O7 Otto H H Zeitschrift fur Kristallographie 149 (1979) 197-205 Die kristallstruktur von PbGe3O7 mit Ge4+ in trigonal-dipyramidaler neben tetraedrischer koordination _database_code_amcsd 0010804 CELL PARAMETERS: 5.2700 14.0970 16.0590 90.000 90.000 90.000 SPACE GROUP: Pcab X-RAY WAVELENGTH: 1.541838 Cell Volume: 1193.042 Density (g/cm3): 5.980 MAX. ABS. INTENSITY / VOLUME**2: 52.15109371 RIR: 2.840 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.02 17.94 8.0295 0 0 2 2 12.56 15.71 7.0485 0 2 0 2 12.69 44.11 6.9771 0 1 2 4 16.74 3.99 5.2971 0 2 2 4 18.81 3.08 4.7185 1 1 1 8 21.05 2.76 4.2207 1 2 0 4 21.13 3.59 4.2052 1 1 2 8 21.77 42.17 4.0821 1 2 1 8 21.92 10.29 4.0556 0 3 2 4 22.14 5.61 4.0148 0 0 4 2 23.03 10.90 3.8612 0 1 4 4 23.82 37.79 3.7360 1 2 2 8 24.53 50.66 3.6289 1 1 3 8 25.27 33.68 3.5243 0 4 0 2 25.53 15.04 3.4885 0 2 4 4 26.00 10.09 3.4265 1 3 1 8 26.90 7.77 3.3144 1 2 3 8 27.64 24.99 3.2271 0 4 2 4 27.76 91.35 3.2140 1 3 2 8 28.66 87.51 3.1147 1 1 4 8 29.26 1.48 3.0524 0 3 4 4 30.47 100.00 2.9337 1 3 3 8 30.51 3.65 2.9295 1 4 0 4 31.03 3.69 2.8820 1 4 1 8 32.53 26.59 2.7521 1 4 2 8 33.28 15.85 2.6921 1 1 5 8 33.48 13.19 2.6765 0 0 6 2 33.69 21.59 2.6602 0 5 2 4 33.94 46.10 2.6413 1 3 4 8 34.02 7.97 2.6350 2 0 0 2 34.10 27.46 2.6295 0 1 6 4 34.49 50.70 2.6002 2 0 1 4 34.91 13.55 2.5699 1 4 3 8 35.09 7.25 2.5571 2 1 1 8 35.11 3.35 2.5559 1 2 5 8 35.89 5.11 2.5022 0 2 6 4 36.45 1.88 2.4651 2 1 2 8 36.58 3.52 2.4567 1 5 1 8 36.84 4.23 2.4395 2 2 1 8 37.99 5.40 2.3687 1 3 5 8 38.02 1.03 2.3665 1 4 4 8 38.25 2.79 2.3529 1 1 6 8 38.31 17.45 2.3495 0 6 0 2 38.62 5.91 2.3315 2 1 3 8 38.72 2.40 2.3257 0 3 6 4 39.04 6.34 2.3073 0 5 4 4 39.61 1.44 2.2751 2 3 1 8 39.88 1.75 2.2603 1 2 6 8 39.98 3.95 2.2549 0 6 2 4 40.24 4.14 2.2414 2 2 3 8 41.73 4.73 2.1644 1 4 5 8 42.41 31.96 2.1315 0 4 6 4 42.82 3.01 2.1119 2 3 3 8 43.02 1.39 2.1026 2 2 4 8 43.24 26.27 2.0924 2 4 1 8 44.47 1.04 2.0371 2 0 5 4 44.96 30.57 2.0162 2 1 5 8 44.97 1.53 2.0156 1 2 7 8 45.17 7.37 2.0074 0 0 8 2 45.54 2.78 1.9918 1 6 3 8 45.93 3.65 1.9760 1 4 6 8 46.24 3.30 1.9633 2 4 3 8 46.80 8.82 1.9411 0 5 6 4 47.07 1.96 1.9306 0 2 8 4 47.35 1.35 1.9199 1 3 7 8 47.57 15.32 1.9114 2 5 1 8 48.08 6.05 1.8925 1 6 4 8 48.72 2.25 1.8691 2 3 5 8 48.74 2.09 1.8684 1 7 1 8 48.99 5.34 1.8595 1 1 8 8 49.78 14.35 1.8316 1 7 2 8 50.33 8.14 1.8128 1 2 8 8 50.37 3.98 1.8115 2 5 3 8 50.53 2.22 1.8062 1 4 7 8 50.72 3.46 1.8001 0 7 4 4 51.49 10.23 1.7748 1 7 3 8 51.78 6.86 1.7657 0 6 6 4 51.84 5.96 1.7637 2 4 5 8 52.46 5.63 1.7443 0 4 8 4 52.49 22.14 1.7433 2 6 1 8 52.53 1.30 1.7422 1 3 8 8 52.92 12.33 1.7302 2 0 7 4 53.22 2.74 1.7212 0 8 2 4 53.78 5.01 1.7045 3 2 0 4 53.82 16.27 1.7035 1 7 4 8 54.11 2.46 1.6950 3 2 1 8 54.62 13.15 1.6804 2 2 7 8 54.70 3.28 1.6781 1 1 9 8 54.83 1.16 1.6742 1 6 6 8 54.94 3.54 1.6712 1 8 0 4 55.08 4.39 1.6674 3 2 2 8 55.26 8.19 1.6622 1 8 1 8 55.43 8.63 1.6575 3 1 3 8 55.45 1.45 1.6572 2 4 6 8 55.49 4.34 1.6559 1 4 8 8 55.66 5.60 1.6512 2 5 5 8 55.95 12.43 1.6435 1 2 9 8 56.19 2.44 1.6369 3 3 1 8 56.22 2.82 1.6361 1 8 2 8 56.67 1.09 1.6242 3 2 3 8 56.71 6.10 1.6232 1 7 5 8 57.08 1.31 1.6135 0 8 4 4 57.14 1.54 1.6119 3 3 2 8 57.25 3.67 1.6092 0 7 6 4 57.65 2.58 1.5990 3 1 4 8 57.92 1.98 1.5922 2 7 1 8 57.99 1.92 1.5903 1 3 9 8 58.70 24.88 1.5728 3 3 3 8 58.93 2.92 1.5672 1 6 7 8 59.52 17.83 1.5532 2 4 7 8 59.96 3.48 1.5429 3 4 2 8 60.12 1.04 1.5391 1 7 6 8 60.42 5.37 1.5321 3 1 5 8 60.64 2.33 1.5271 1 1 10 8 60.68 3.73 1.5262 0 6 8 4 60.78 2.90 1.5239 1 4 9 8 60.84 5.33 1.5225 3 3 4 8 61.47 5.38 1.5085 3 4 3 8 61.81 9.63 1.5009 1 2 10 8 62.57 2.07 1.4846 3 5 1 8 62.67 1.35 1.4825 1 8 5 8 62.90 2.27 1.4775 2 0 9 4 63.04 5.34 1.4747 2 5 7 8 63.17 1.02 1.4718 0 8 6 4 63.29 1.02 1.4694 2 1 9 8 63.46 1.23 1.4660 1 6 8 8 63.74 11.64 1.4601 1 3 10 8 63.78 3.12 1.4592 0 9 4 4 63.81 1.07 1.4587 2 8 1 8 64.45 2.44 1.4456 1 9 3 8 64.85 1.43 1.4377 3 2 6 8 65.13 8.08 1.4322 2 7 5 8 65.67 4.01 1.4217 0 7 8 4 66.18 1.81 1.4121 3 4 5 8 66.30 3.75 1.4097 0 10 0 2 66.49 5.09 1.4063 1 9 4 8 67.19 10.97 1.3932 2 6 7 8 67.45 2.34 1.3885 0 10 2 4 69.02 1.70 1.3607 3 6 3 8 69.05 1.16 1.3601 1 9 5 8 69.54 1.53 1.3519 0 9 6 4 69.78 5.80 1.3478 1 3 11 8 70.08 2.17 1.3426 1 10 2 8 70.35 1.19 1.3383 0 0 12 2 70.68 3.04 1.3327 2 8 5 8 70.71 5.67 1.3323 0 1 12 4 71.63 5.52 1.3175 4 0 0 2 71.90 1.15 1.3131 4 0 1 4 72.34 1.06 1.3062 3 7 2 8 72.37 1.39 1.3057 2 9 3 8 72.79 2.54 1.2993 3 2 8 8 73.09 2.11 1.2946 4 1 2 8 73.09 1.03 1.2946 1 7 9 8 73.72 6.14 1.2851 3 7 3 8 73.77 3.42 1.2843 1 8 8 8 74.63 1.59 1.2718 2 1 11 8 75.06 3.53 1.2655 0 11 2 4 75.64 2.09 1.2572 3 7 4 8 76.10 1.52 1.2507 2 6 9 8 76.13 1.42 1.2503 1 3 12 8 76.35 1.62 1.2473 0 10 6 4 76.38 2.58 1.2469 3 1 9 8 76.38 1.52 1.2469 4 1 4 8 76.49 1.78 1.2453 3 6 6 8 76.76 3.87 1.2417 2 9 5 8 76.86 3.28 1.2404 3 8 1 8 76.93 7.67 1.2393 2 10 1 8 77.05 1.03 1.2377 3 4 8 8 77.32 1.95 1.2341 4 4 0 4 77.43 7.78 1.2325 3 2 9 8 77.58 1.49 1.2305 1 11 2 8 77.67 1.55 1.2294 3 8 2 8 78.08 3.25 1.2239 3 7 5 8 78.27 2.95 1.2214 1 7 10 8 78.40 1.62 1.2198 4 4 2 8 78.40 4.11 1.2197 1 8 9 8 78.86 1.45 1.2137 1 10 6 8 79.18 1.16 1.2096 3 3 9 8 79.24 6.44 1.2090 0 5 12 4 80.00 1.62 1.1993 3 6 7 8 80.65 1.01 1.1913 2 7 9 8 80.81 1.86 1.1894 1 11 4 8 81.41 2.52 1.1821 4 0 6 4 81.53 4.66 1.1806 4 5 2 8 81.62 1.33 1.1796 3 4 9 8 81.76 3.73 1.1779 4 1 6 8 82.80 1.14 1.1658 4 2 6 8 83.02 6.89 1.1632 2 5 11 8 83.21 1.94 1.1610 1 11 5 8 83.37 1.93 1.1592 2 10 5 8 83.48 3.98 1.1579 1 8 10 8 83.86 2.55 1.1536 0 10 8 4 83.89 1.73 1.1533 1 7 11 8 84.23 1.68 1.1495 2 11 1 8 84.26 1.53 1.1493 3 3 10 8 84.27 2.95 1.1492 4 6 0 4 84.45 1.44 1.1471 0 0 14 2 84.72 1.99 1.1441 4 5 4 8 84.90 1.47 1.1422 3 9 3 8 86.35 2.20 1.1267 2 11 3 8 86.76 1.22 1.1225 3 9 4 8 86.93 3.61 1.1207 4 4 6 8 87.14 2.60 1.1185 2 0 13 4 87.48 5.74 1.1150 2 1 13 8 88.84 1.73 1.1015 4 0 8 4 89.32 1.09 1.0967 1 9 10 8 89.72 3.13 1.0929 2 10 7 8 89.81 4.61 1.0920 3 3 11 8 89.98 1.07 1.0905 1 7 12 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.