Heteromorphite Edenharter A Zeitschrift fur Kristallographie 151 (1980) 193-202 Die kristallstruktur von heteromorphit, Pb7Sb8S19 _database_code_amcsd 0010822 CELL PARAMETERS: 13.6280 11.9430 21.2850 90.000 90.920 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 3463.883 Density (g/cm3): 5.816 MAX. ABS. INTENSITY / VOLUME**2: 29.61295143 RIR: 1.658 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.31 3.11 10.6411 0 0 2 2 9.85 1.17 8.9815 1 1 0 4 10.65 14.60 8.3063 -1 1 1 4 12.83 10.79 6.8996 -1 1 2 4 12.97 1.06 6.8280 1 1 2 4 15.33 1.21 5.7801 -2 0 2 2 15.41 4.70 5.7495 0 2 1 4 15.56 2.39 5.6964 2 0 2 2 15.84 26.11 5.5959 -1 1 3 4 16.00 1.20 5.5385 1 1 3 4 16.66 10.42 5.3206 0 0 4 2 17.03 11.82 5.2076 0 2 2 4 19.30 10.45 4.5990 -1 1 4 4 19.43 9.34 4.5684 0 2 3 4 20.25 4.55 4.3846 2 2 1 4 20.92 17.89 4.2454 3 1 0 4 21.02 4.74 4.2264 -2 0 4 2 21.28 3.37 4.1754 -3 1 1 4 21.39 1.62 4.1532 -2 2 2 4 21.40 3.51 4.1515 3 1 1 4 22.38 27.83 3.9725 0 2 4 4 22.67 44.11 3.9230 3 1 2 4 23.03 82.43 3.8622 -1 1 5 4 23.22 1.80 3.8307 1 1 5 4 23.28 71.64 3.8213 1 3 0 4 23.33 3.90 3.8127 -2 2 3 4 23.56 18.43 3.7764 2 2 3 4 23.64 12.18 3.7641 -1 3 1 4 23.67 59.75 3.7582 1 3 1 4 24.60 17.87 3.6191 3 1 3 4 24.72 12.33 3.6016 -1 3 2 4 24.79 8.41 3.5913 1 3 2 4 25.70 4.91 3.4661 0 2 5 4 25.83 23.55 3.4498 -2 2 4 4 26.10 78.25 3.4140 2 2 4 4 26.16 24.22 3.4066 4 0 0 2 26.44 12.49 3.3706 -1 3 3 4 26.93 74.10 3.3111 -1 1 6 4 27.07 65.47 3.2945 3 1 4 4 27.13 1.27 3.2872 1 1 6 4 27.36 81.67 3.2596 -4 0 2 2 27.62 1.93 3.2293 4 0 2 2 28.56 3.67 3.1257 2 0 6 2 28.75 81.81 3.1057 -2 2 5 4 28.83 4.36 3.0971 1 3 4 4 29.06 39.39 3.0731 2 2 5 4 29.84 1.32 2.9938 3 3 0 4 29.95 60.74 2.9836 3 1 5 4 30.10 40.77 2.9690 -3 3 1 4 30.19 13.31 2.9603 3 3 1 4 30.20 16.83 2.9589 4 2 0 4 30.23 4.22 2.9568 0 4 1 4 30.44 2.26 2.9363 -4 2 1 4 30.56 2.23 2.9252 4 2 1 4 30.94 9.29 2.8901 -4 0 4 2 30.94 90.71 2.8899 -3 3 2 4 30.95 4.68 2.8891 -1 1 7 4 31.12 1.32 2.8740 3 3 2 4 31.16 1.21 2.8706 1 1 7 4 31.26 1.53 2.8611 -4 2 2 4 31.49 34.00 2.8406 4 2 2 4 31.99 73.36 2.7979 -2 2 6 4 32.33 5.85 2.7693 2 2 6 4 32.33 39.15 2.7688 -3 3 3 4 32.54 1.87 2.7519 0 4 3 4 32.59 1.30 2.7479 3 3 3 4 32.75 11.15 2.7347 2 4 0 4 32.96 24.10 2.7175 4 2 3 4 33.00 29.42 2.7146 -2 4 1 4 33.05 7.29 2.7102 2 4 1 4 33.15 20.81 2.7021 3 1 6 4 33.90 1.35 2.6445 2 4 2 4 34.44 3.19 2.6038 0 4 4 4 34.90 3.87 2.5708 4 2 4 4 35.25 1.07 2.5462 2 4 3 4 35.48 15.12 2.5301 -2 2 7 4 35.84 4.74 2.5053 2 2 7 4 35.91 1.49 2.5011 -5 1 3 4 36.29 1.63 2.4755 5 1 3 4 36.45 36.83 2.4647 2 0 8 2 36.75 5.01 2.4456 -4 2 5 4 36.86 1.55 2.4386 -2 4 4 4 36.89 4.37 2.4367 3 3 5 4 37.06 1.56 2.4259 2 4 4 4 37.73 2.99 2.3844 -1 3 7 4 37.90 2.24 2.3739 1 3 7 4 38.09 1.03 2.3623 5 1 4 4 38.51 1.89 2.3378 1 5 1 4 39.03 1.35 2.3075 -2 4 5 4 39.18 4.82 2.2995 -2 2 8 4 39.30 2.54 2.2927 -1 1 9 4 39.38 12.07 2.2879 -4 2 6 4 39.45 12.37 2.2842 0 4 6 4 39.51 6.55 2.2808 1 1 9 4 39.60 1.13 2.2760 3 3 6 4 40.10 17.74 2.2488 5 3 0 4 40.16 1.18 2.2454 4 4 0 4 40.27 21.44 2.2394 -5 3 1 4 40.39 2.53 2.2333 5 3 1 4 40.43 16.06 2.2313 1 5 3 4 40.91 5.53 2.2061 -5 3 2 4 41.18 3.27 2.1923 4 4 2 4 41.45 2.44 2.1787 1 3 8 4 41.57 1.12 2.1725 -2 4 6 4 42.03 74.04 2.1495 1 5 4 4 42.08 2.09 2.1472 -4 4 3 4 42.14 1.14 2.1446 -3 3 7 4 42.33 3.69 2.1354 -4 2 7 4 42.35 1.46 2.1342 4 4 3 4 42.43 14.11 2.1303 0 4 7 4 42.59 1.63 2.1227 6 2 0 4 42.61 1.05 2.1220 3 3 7 4 43.03 1.35 2.1022 3 5 1 4 43.04 7.17 2.1015 -2 2 9 4 43.48 5.35 2.0813 -5 3 4 4 43.58 5.25 2.0767 6 0 4 2 43.60 30.37 2.0757 6 2 2 4 43.82 16.90 2.0660 1 1 10 4 43.92 3.46 2.0616 5 3 4 4 43.92 2.92 2.0615 -1 5 5 4 43.93 4.16 2.0609 4 4 4 4 44.03 6.79 2.0567 1 5 5 4 44.39 11.12 2.0408 -2 0 10 2 44.63 3.05 2.0302 -3 5 3 4 44.75 27.74 2.0253 6 2 3 4 44.83 3.16 2.0219 3 5 3 4 44.96 23.97 2.0163 -5 1 7 4 44.99 4.80 2.0149 -1 3 9 4 45.18 3.09 2.0068 1 3 9 4 45.36 1.95 1.9993 -5 3 5 4 45.47 4.91 1.9947 -4 4 5 4 45.68 8.11 1.9862 0 4 8 4 45.87 6.15 1.9782 3 3 8 4 45.89 8.14 1.9774 4 4 5 4 46.08 9.31 1.9697 -3 5 4 4 46.29 2.34 1.9615 6 2 4 4 47.31 7.22 1.9213 7 1 0 4 47.47 6.91 1.9154 2 2 10 4 47.50 1.31 1.9141 -3 1 10 4 47.59 2.22 1.9108 7 1 1 4 47.59 1.65 1.9107 -5 3 6 4 47.59 9.55 1.9106 2 6 0 4 47.82 1.30 1.9022 2 6 1 4 47.90 3.08 1.8991 -3 5 5 4 47.91 9.40 1.8988 6 0 6 2 47.98 6.17 1.8959 -7 1 2 4 48.02 21.28 1.8948 -5 1 8 4 48.19 2.70 1.8882 4 4 6 4 48.20 2.64 1.8880 5 3 6 4 48.22 17.13 1.8873 1 1 11 4 48.27 1.96 1.8855 7 1 2 4 48.36 19.21 1.8820 -2 6 2 4 48.44 3.62 1.8791 2 6 2 4 48.82 7.10 1.8654 5 1 8 4 48.88 1.34 1.8632 -1 5 7 4 48.89 6.03 1.8629 -1 3 10 4 48.97 1.32 1.8600 -4 2 9 4 49.02 7.99 1.8582 1 5 7 4 49.15 12.07 1.8537 0 4 9 4 49.34 2.15 1.8471 7 1 3 4 49.34 4.26 1.8470 -2 6 3 4 49.36 8.85 1.8462 3 3 9 4 49.72 6.14 1.8336 -6 2 6 4 50.06 12.97 1.8220 -3 5 6 4 50.23 1.09 1.8163 -7 1 4 4 50.26 4.82 1.8154 -4 4 7 4 50.63 1.83 1.8031 0 6 5 4 50.78 5.05 1.7980 7 1 4 4 50.80 2.08 1.7971 4 4 7 4 50.82 2.80 1.7966 5 3 7 4 50.83 1.97 1.7963 5 5 0 4 50.96 1.42 1.7921 4 0 10 2 51.07 3.71 1.7883 5 5 1 4 51.21 2.33 1.7837 -2 2 11 4 51.32 1.34 1.7803 -5 1 9 4 51.53 1.16 1.7735 0 0 12 2 51.62 9.26 1.7706 -3 1 11 4 51.64 2.48 1.7701 2 2 11 4 51.70 17.33 1.7682 5 5 2 4 51.80 1.78 1.7648 -1 5 8 4 52.05 12.80 1.7570 -6 4 3 4 52.18 10.02 1.7529 -6 2 7 4 52.18 7.99 1.7528 5 1 9 4 52.54 2.40 1.7418 -3 5 7 4 52.73 2.76 1.7359 0 6 6 4 52.83 5.38 1.7330 0 4 10 4 52.94 1.59 1.7296 -7 3 2 4 52.95 8.46 1.7293 -1 3 11 4 53.09 5.89 1.7249 -4 4 8 4 53.16 1.76 1.7230 1 3 11 4 53.32 2.40 1.7182 -6 4 4 4 53.70 11.41 1.7070 4 4 8 4 53.72 1.52 1.7063 5 3 8 4 53.81 6.97 1.7036 -7 3 3 4 54.06 1.53 1.6965 5 5 4 4 54.18 3.50 1.6929 1 7 0 4 54.42 12.66 1.6861 -8 0 2 2 54.94 1.99 1.6714 1 7 2 4 55.04 3.94 1.6685 -7 3 4 4 55.15 2.11 1.6653 0 6 7 4 55.30 1.09 1.6612 -3 5 8 4 55.51 6.79 1.6555 -2 2 12 4 55.55 1.46 1.6542 7 3 4 4 55.76 2.28 1.6487 5 5 5 4 55.80 1.37 1.6474 -1 7 3 4 55.81 2.06 1.6472 6 2 8 4 55.88 4.32 1.6453 -3 1 12 4 56.41 1.65 1.6312 8 2 1 4 56.46 8.53 1.6298 -8 0 4 2 56.73 1.12 1.6227 -8 2 2 4 56.84 9.38 1.6197 4 4 9 4 56.88 1.17 1.6189 5 3 9 4 57.25 1.25 1.6091 4 2 11 4 57.31 3.90 1.6076 1 1 13 4 57.72 4.46 1.5972 3 7 0 4 57.86 1.32 1.5938 0 6 8 4 57.87 3.32 1.5934 -3 7 1 4 57.92 1.34 1.5920 3 7 1 4 58.38 2.20 1.5808 -3 7 2 4 58.46 1.60 1.5788 0 2 13 4 58.90 2.79 1.5680 6 2 9 4 59.25 1.34 1.5596 7 3 6 4 59.53 1.46 1.5529 -4 4 10 4 59.86 1.95 1.5451 -8 0 6 2 59.94 1.37 1.5433 -2 2 13 4 60.00 2.92 1.5417 4 6 6 4 60.42 2.27 1.5321 -3 7 4 4 61.31 3.12 1.5119 4 2 12 4 61.56 6.21 1.5065 7 3 7 4 61.94 1.01 1.4982 -3 7 5 4 62.00 3.18 1.4969 6 6 0 4 62.03 2.68 1.4962 1 1 14 4 62.22 2.26 1.4921 6 6 1 4 62.86 2.93 1.4784 0 8 2 4 62.96 3.53 1.4763 -5 3 11 4 63.10 9.19 1.4734 -4 4 11 4 63.11 1.25 1.4732 0 2 14 4 63.52 1.38 1.4645 5 1 12 4 63.70 1.96 1.4609 0 8 3 4 63.77 1.14 1.4594 -3 7 6 4 63.84 1.21 1.4581 4 4 11 4 64.05 3.71 1.4537 0 6 10 4 64.15 2.39 1.4517 7 3 8 4 64.17 1.14 1.4514 -8 2 7 4 64.49 7.33 1.4450 -6 6 4 4 64.52 1.54 1.4443 8 4 3 4 64.53 1.87 1.4441 2 8 2 4 64.60 1.64 1.4428 -3 3 13 4 64.82 2.25 1.4383 4 6 8 4 64.97 1.02 1.4355 0 4 13 4 65.01 5.72 1.4346 -5 7 2 4 65.27 1.40 1.4295 -1 7 8 4 65.36 1.87 1.4279 -7 5 5 4 65.55 1.12 1.4241 8 0 8 2 65.55 2.16 1.4241 4 2 13 4 65.58 2.04 1.4235 -9 1 5 4 65.66 1.28 1.4220 3 5 11 4 65.80 1.74 1.4194 -5 7 3 4 65.93 1.82 1.4168 -6 6 5 4 66.11 1.25 1.4134 -9 3 1 4 66.25 1.88 1.4107 3 7 7 4 66.35 1.95 1.4088 -6 0 12 2 66.53 1.46 1.4055 -9 3 2 4 66.58 1.21 1.4045 -8 2 8 4 66.74 1.04 1.4016 -5 3 12 4 66.82 1.18 1.4000 9 3 2 4 66.87 1.05 1.3992 1 1 15 4 66.88 2.14 1.3990 -4 4 12 4 67.02 1.10 1.3964 7 3 9 4 67.11 2.26 1.3948 -7 5 6 4 67.27 1.62 1.3918 -9 3 3 4 67.51 1.67 1.3874 0 6 11 4 67.65 2.06 1.3849 4 6 9 4 67.69 3.78 1.3841 5 1 13 4 67.92 2.24 1.3800 4 0 14 2 68.03 1.47 1.3781 2 8 5 4 68.04 2.86 1.3778 -1 7 9 4 68.15 2.38 1.3760 0 8 6 4 68.19 2.40 1.3753 9 1 6 4 68.33 1.80 1.3728 -3 7 8 4 68.72 3.40 1.3659 3 7 8 4 68.92 1.28 1.3625 9 3 4 4 69.14 2.30 1.3587 8 4 6 4 69.34 1.06 1.3552 -9 1 7 4 69.35 3.37 1.3551 4 8 2 4 69.54 2.75 1.3518 -3 1 15 4 69.63 1.76 1.3504 -2 8 6 4 69.67 3.09 1.3497 3 3 14 4 69.71 1.29 1.3489 10 0 2 2 69.91 2.03 1.3455 -1 5 13 4 70.35 2.35 1.3382 9 1 7 4 70.74 1.96 1.3318 4 6 10 4 70.84 3.46 1.3301 0 0 16 2 70.94 1.40 1.3285 10 2 0 4 71.07 1.30 1.3264 -4 8 4 4 71.15 1.40 1.3251 2 4 14 4 71.18 1.22 1.3246 10 2 1 4 71.28 1.63 1.3231 8 4 7 4 71.33 2.34 1.3223 4 8 4 4 71.42 1.08 1.3208 1 9 0 4 71.49 3.08 1.3196 -7 5 8 4 71.68 2.68 1.3166 -2 8 7 4 72.04 1.12 1.3109 -1 9 2 4 72.06 1.22 1.3106 5 1 14 4 72.31 1.10 1.3067 -7 3 11 4 72.36 2.05 1.3059 -6 2 13 4 73.50 1.48 1.2884 8 2 10 4 73.64 1.31 1.2864 -4 2 15 4 73.88 3.07 1.2828 8 6 2 4 74.08 1.26 1.2798 4 6 11 4 74.12 2.89 1.2793 -7 5 9 4 74.15 3.10 1.2788 9 5 0 4 74.24 1.32 1.2775 -9 5 1 4 74.26 1.66 1.2771 -9 1 9 4 74.38 1.10 1.2754 -7 7 2 4 74.42 1.66 1.2748 -3 1 16 4 74.47 1.62 1.2740 3 7 10 4 74.91 5.13 1.2676 9 5 2 4 75.08 2.50 1.2652 10 0 6 2 75.16 2.14 1.2641 3 9 2 4 75.25 1.09 1.2627 -2 4 15 4 75.29 1.37 1.2622 -8 4 9 4 75.53 1.14 1.2588 9 1 9 4 75.59 3.14 1.2580 -1 3 16 4 75.72 2.39 1.2561 2 4 15 4 75.73 1.63 1.2559 -7 1 13 4 75.76 2.03 1.2555 9 5 3 4 76.53 1.65 1.2448 -6 2 14 4 76.83 2.44 1.2407 8 2 11 4 76.85 2.04 1.2404 2 6 13 4 76.94 2.41 1.2392 -4 6 12 4 77.00 1.25 1.2384 -5 7 9 4 77.07 1.50 1.2375 3 9 4 4 77.14 1.01 1.2365 -9 1 10 4 77.15 1.60 1.2363 7 3 12 4 77.94 1.08 1.2258 -1 7 12 4 78.06 1.17 1.2242 -10 4 3 4 78.17 2.91 1.2228 -8 4 10 4 78.25 1.68 1.2217 11 1 2 4 78.99 1.94 1.2122 6 8 4 4 79.49 2.64 1.2058 6 4 13 4 79.75 3.31 1.2025 7 7 6 4 79.83 1.90 1.2014 -7 1 14 4 79.88 1.10 1.2009 -5 7 10 4 80.01 1.69 1.1992 -2 4 16 4 80.41 1.30 1.1943 6 8 5 4 80.50 1.23 1.1931 2 4 16 4 80.56 1.55 1.1924 0 10 1 4 80.74 1.27 1.1902 -4 6 13 4 81.01 2.20 1.1870 2 6 14 4 81.03 1.04 1.1866 7 3 13 4 81.78 1.02 1.1777 0 10 3 4 81.78 1.80 1.1777 7 7 7 4 81.80 1.34 1.1774 9 1 11 4 82.73 1.08 1.1665 -5 5 14 4 82.77 1.60 1.1660 -10 2 9 4 82.78 1.21 1.1659 -5 9 4 4 84.05 1.13 1.1516 -5 3 16 4 84.72 2.76 1.1442 -11 3 5 4 84.96 1.38 1.1416 -2 6 15 4 85.29 1.24 1.1380 6 6 12 4 85.60 1.10 1.1346 3 1 18 4 86.50 1.00 1.1252 4 10 1 4 86.73 1.64 1.1227 8 8 0 4 86.75 1.46 1.1226 -4 0 18 2 87.49 1.03 1.1149 -12 2 1 4 87.57 1.21 1.1142 -12 0 4 2 87.58 1.03 1.1140 -4 10 3 4 89.61 1.02 1.0940 -2 6 16 4 89.74 1.24 1.0927 4 2 18 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.